[43] Preparation of trimethylsilyl derivatives of nucleic acid components for analysis by mass spectrometry

1990 ◽  
pp. 791-796 ◽  
Author(s):  
Karl H. Schram
Keyword(s):  
Mass Spectrometry ◽  
Nucleic Acid ◽  
Trimethylsilyl Derivatives ◽  
Derivatives Of

Mass spectrometry of nucleic acid components. Trimethylsilyl derivatives of nucleotides

1971 ◽  
Vol 93 (4) ◽  
pp. 1014-1023 ◽  
Author(s):  
James A. McCloskey ◽  
A. M. Lawson ◽  
Richard N. Stillwell ◽  
M. M. Tacker ◽  
K. Tsuboyama
Keyword(s):  
Mass Spectrometry ◽  
Nucleic Acid ◽  
Trimethylsilyl Derivatives ◽  
Derivatives Of

ChemInform Abstract: MASS SPECTROMETRY OF NUCLEIC ACID CONSTITUENTS. TRIMETHYLSILYL DERIVATIVES OF NUCLEOSIDES

1983 ◽  
Vol 14 (8) ◽  
Author(s):  
H. PANG ◽  
K. H. SCHRAM ◽  
D. L. SMITH ◽  
S. P. GUPTA ◽  
L. B. TOWNSEND ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Nucleic Acid ◽  
Trimethylsilyl Derivatives ◽  
Derivatives Of

Mass spectrometry of nucleic acid constituents. Trimethylsilyl derivatives of nucleosides

1982 ◽  
Vol 47 (20) ◽  
pp. 3923-3932 ◽  
Author(s):  
Henrianna Pang ◽  
Karl H. Schram ◽  
David L. Smith ◽  
S. P. Gupta ◽  
Leroy B. Townsend ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Nucleic Acid ◽  
Trimethylsilyl Derivatives ◽  
Derivatives Of

Mass spectrometry of nucleic acid components. Trimethylsilyl derivatives of nucleotides, nucleosides, and bases

1968 ◽  
Vol 90 (15) ◽  
pp. 4182-4184 ◽  
Author(s):  
James A. McCloskey ◽  
A. M. Lawson ◽  
K. Tsuboyama ◽  
P. M. Krueger ◽  
R. N. Stillwell
Keyword(s):  
Mass Spectrometry ◽  
Nucleic Acid ◽  
Trimethylsilyl Derivatives ◽  
Derivatives Of

Massenspektrometrische Fragmentierung von Trimethylsilylderivaten (TMS) des Thyrotropin-„Releasing“-Hormons (TRH) und dessen Teilstrukturen / Mass Spectroscopy of Trimethylsilyl Derivatives of Thyrotropin-releasing Hormone and its Constituents

1973 ◽  
Vol 28 (11-12) ◽  
pp. 820-823 ◽  
Author(s):  
W. A. König ◽  
S. Fuchs ◽  
K. Zech ◽  
W. Voelter
Keyword(s):  
Mass Spectrometry ◽  
Mass Spectroscopy ◽  
Peptide Hormones ◽  
Thyrotropin Releasing Hormone ◽  
Mass Spectral Fragmentation ◽  
Releasing Hormone ◽  
Mass Spectral ◽  
Trimethylsilyl Derivatives ◽  
Fragmentation Patterns ◽  
Derivatives Of

The mass spectral fragmentation patterns of trimethylsilyl derivatives of TRH and its constituents are discussed. The utility of these derivatives for the control of the synthesis of peptide hormones by mass spectrometry is obvious.

Mass spectrometry of the trimethylsilyl derivatives of some cardiac aglycones and monoglycosides

1973 ◽  
Vol 7 (2) ◽  
pp. 141-153 ◽  
Author(s):  
Fred C. Falkner ◽  
Jürgen Frölich ◽  
J. Throck Watson
Keyword(s):  
Mass Spectrometry ◽  
Trimethylsilyl Derivatives ◽  
Derivatives Of

Use of High-Resolution Open Tubular Glass Capillary Columns to Separate Acidic Metabolites in Urine

1975 ◽  
Vol 21 (7) ◽  
pp. 888-891 ◽  
Author(s):  
Brian A Knights ◽  
Mary Legendre ◽  
John L Laseter ◽  
James S Storer
Keyword(s):  
Mass Spectrometry ◽  
High Resolution ◽  
Capillary Columns ◽  
General Purpose ◽  
Gas Chromatography Mass Spectrometry ◽  
Glass Capillary ◽  
Glass Capillary Columns ◽  
Trimethylsilyl Derivatives ◽  
Derivatives Of ◽  
Urine Specimens

Abstract We used high-resolution glass capillary columns to study the trimethylsilyl derivatives of some acidic metabolites found in pooled urine specimens from control and postpartum subjects. About 30 compounds were identified by gas chromatography—mass spectrometry—computer techniques. In general, open tubular capillary columns effect better resolution of trimethylsilyl derivatives of organic acids than do conventional packed columns. GE SE-30 proved to be a good general-purpose stationary phase, whereas OV-17 offered certain advantages in resolving aromatic acid components.

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