scholarly journals Electrochemical application of cobalt nanoparticles-polypyrrole composite modified electrode for the determination of phoxim

2021 ◽  
Vol 9 ◽  
pp. 100077
Author(s):  
Molla Tefera ◽  
Merid Tessema ◽  
Shimelis Admassie ◽  
Meryck Ward ◽  
Lisebo Phelane ◽  
...  
RSC Advances ◽  
2014 ◽  
Vol 4 (89) ◽  
pp. 48522-48534 ◽  
Author(s):  
A. T. Ezhil Vilian ◽  
Muniyandi Rajkumar ◽  
Shen-Ming Chen ◽  
Chi-Chang Hu ◽  
Shakkthivel Piraman

This paper describes the two-step synthesis of a nitrogen-doped reduced graphene oxide–ZnO (N-doped RGO–ZnO) nanocomposite and its photo electrochemical application.


2018 ◽  
Vol 14 (3) ◽  
pp. 271-276 ◽  
Author(s):  
Isaac Yves Lopes de Macedo ◽  
Morgana Fernandes Alecrim ◽  
Luane Ferreira Garcia ◽  
Aparecido Ribeiro de Souza ◽  
Wallans Torres Pio dos Santos ◽  
...  

2014 ◽  
Vol 2014 ◽  
pp. 1-10 ◽  
Author(s):  
Gen Liu ◽  
Wei Ma ◽  
Yan Luo ◽  
Deng-ming Sun ◽  
Shuang Shao

Poly(methylene blue) and electrochemically reduced graphene oxide composite film modified electrode (PMB-ERGO/GCE) was successfully fabricated by electropolymerization and was used for simultaneous determination of uric acid (UA) and xanthine (Xa). Based on the excellent electrocatalytic activity of PMB-ERGO/GCE, the electrochemical behaviors of UA and Xa were studied by cyclic voltammetry (CV) and square wave voltammetry (SWV). Two anodic sensitive peaks at 0.630 V (versus Ag/AgCl) for UA and 1.006 V (versus Ag/AgCl) for Xa were given by CV in pH 3.0 phosphate buffer. The calibration curves for UA and Xa were obtained in the range of 8.00 × 10−8~4.00 × 10−4 M and 1.00 × 10−7~4.00 × 10−4 M, respectively, by SWV. The detection limits for UA and Xa were3.00×10-8 M and5.00×10-8 M, respectively. Finally, the proposed method was applied to simultaneously determine UA and Xa in human urine with good selectivity and high sensitivity.


2012 ◽  
Vol 48 (4) ◽  
pp. 639-649 ◽  
Author(s):  
Kellen Heloizy Garcia Freitas ◽  
Orlando Fatibello-Filho ◽  
Ivanildo Luiz de Mattos

A carbon composite electrode modified with copper (II) phosphate immobilized in a polyester resin (Cu3(PO4)2-Poly) for the determination of rutin in pharmaceutical samples by square-wave voltammetry is described herein. The modified electrode allows the determination of rutin at a potential (0.20 V vs. Ag/AgCl (3.0 mol L-1 KCl)) lower than that observed at an unmodified electrode. The peak current was found to be linear to the rutin concentration in the range from 9.9 × 10-8 to 2.5 × 10-6 mol L-1, with a detection limit of 1.2×10-8 mol L-1. The response of the electrode was stable, with no variation in baseline levels within several hours of continuous operation. The surface morphology of the modified electrode was characterized by scanning electron microscopy (SEM) and energy dispersive X-ray (EDX) system. The results obtained are precise and accurate. In addition, these results are in agreement with those obtained by the chromatographic method at a 95% confidence level.


Talanta ◽  
2020 ◽  
Vol 212 ◽  
pp. 120788 ◽  
Author(s):  
Jenjira Saichanapan ◽  
Kiattisak Promsuwan ◽  
Warakorn Limbut

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