Rapid synthesis of polyimide precursors by solution polymerization using Continuous-flow microreactors

2020 ◽  
Vol 397 ◽  
pp. 125361 ◽  
Author(s):  
Wenhua Xu ◽  
Yuanhai Su ◽  
Minjing Shang ◽  
Xueming Lu ◽  
Qinghua Lu
2018 ◽  
Vol 6 (11) ◽  
pp. 15425-15433 ◽  
Author(s):  
Yanbiao Liu ◽  
Xiang Liu ◽  
Shengnan Yang ◽  
Fang Li ◽  
Chensi Shen ◽  
...  

Author(s):  
Anming Yang ◽  
Xia Yang ◽  
Jincai Yue ◽  
Shiqing Zheng ◽  
Litao Qin

2019 ◽  
Vol 9 (5) ◽  
pp. 1189-1200 ◽  
Author(s):  
Michelle P. van der Helm ◽  
Paula Bracco ◽  
Hanna Busch ◽  
Katarzyna Szymańska ◽  
Andrzej B. Jarzębski ◽  
...  

Enzymes are supreme catalysts when it comes to high enantiopurities and their immobilization will pave the way for continuous operation.


2016 ◽  
Vol 45 (1) ◽  
pp. 83-117 ◽  
Author(s):  
Hannes P. L. Gemoets ◽  
Yuanhai Su ◽  
Minjing Shang ◽  
Volker Hessel ◽  
Rafael Luque ◽  
...  

This review gives an exhaustive overview of the engineering principles, safety aspects and chemistry associated with liquid phase oxidation in continuous-flow microreactors.


Catalysts ◽  
2018 ◽  
Vol 8 (5) ◽  
pp. 221 ◽  
Author(s):  
Katarzyna Maresz ◽  
Agnieszka Ciemięga ◽  
Julita Mrowiec-Białoń

In this work, the kinetics of Meerwein–Ponndorf–Verley chemoselective reduction of carbonyl compounds was studied in monolithic continuous-flow microreactors. To the best of our knowledge, this is the first report on the MPV reaction kinetics performed in a flow process. The microreactors are a very attractive alternative to the batch reactors conventionally used in this process. The proposed micro-flow system for synthesis of unsaturated secondary alcohols proved to be very efficient and easily controlled. The microreactors had reactive cores made of zirconium-functionalized silica monoliths of excellent catalytic properties and flow characteristics. The catalytic experiments were carried out with the use of 2-butanol as a hydrogen donor. Herein, we present the kinetic parameters of cyclohexanone reduction in a flow reactor and data on the reaction rate for several important ketones and aldehydes. The lack of diffusion constraints in the microreactors was demonstrated. Our results were compared with those from other authors and demonstrate the great potential of microreactor applications in fine chemical and complex intermediate manufacturing.


2013 ◽  
Vol 149 ◽  
pp. 367-374 ◽  
Author(s):  
Jun Wang ◽  
Shuang-Shuang Gu ◽  
Hong-Sheng Cui ◽  
Liu-Qing Yang ◽  
Xiang-Yang Wu

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