Ceramic Powder Bed Laser Sintering (CPBLS) on copper-doped hydroxyapatite: creation of thin (5 – 50 micron thick) consolidated ceramic patterns

Author(s):  
Tiphaine Bazin ◽  
François Rouzé-l’Alzit ◽  
Alain Demourgues ◽  
I. Julien ◽  
C. Bertrand ◽  
...  
Author(s):  
Kevin Florio ◽  
Dario Puccio ◽  
Giorgio Viganò ◽  
Stefan Pfeiffer ◽  
Fabrizio Verga ◽  
...  

AbstractPowder bed fusion (PBF) of ceramics is often limited because of the low absorptance of ceramic powders and lack of process understanding. These challenges have been addressed through a co-development of customized ceramic powders and laser process capabilities. The starting powder is made of a mix of pure alumina powder and alumina granules, to which a metal oxide dopant is added to increase absorptance. The performance of different granules and process parameters depends on a large number of influencing factors. In this study, two methods for characterizing and analyzing the PBF process are presented and used to assess which dopant is the most suitable for the process. The first method allows one to analyze the absorptance of the laser during the melting of a single track using an integrating sphere. The second one relies on in-situ video imaging using a high-speed camera and an external laser illumination. The absorption behavior of the laser power during the melting of both single tracks and full layers is proven to be a non-linear and extremely dynamic process. While for a single track, the manganese oxide doped powder delivers higher and more stable absorptance. When a full layer is analyzed, iron oxide-doped powder is leading to higher absorptance and a larger melt pool. Both dopants allow the generation of a stable melt-pool, which would be impossible with granules made of pure alumina. In addition, the present study sheds light on several phenomena related to powder and melt-pool dynamics, such as the change of melt-pool shape and dimension over time and powder denudation effects.


Author(s):  
Arash Gobal ◽  
Bahram Ravani

The process of selective laser sintering (SLS) involves selective heating and fusion of powdered material using a moving laser beam. Because of its complicated manufacturing process, physical modeling of the transformation from powder to final product in the SLS process is currently a challenge. Existing simulations of transient temperatures during this process are performed either using finite-element (FE) or discrete-element (DE) methods which are either inaccurate in representing the heat-affected zone (HAZ) or computationally expensive to be practical in large-scale industrial applications. In this work, a new computational model for physical modeling of the transient temperature of the powder bed during the SLS process is developed that combines the FE and the DE methods and accounts for the dynamic changes of particle contact areas in the HAZ. The results show significant improvements in computational efficiency over traditional DE simulations while maintaining the same level of accuracy.


Author(s):  
Nilabh Roy ◽  
Anil Yuksel ◽  
Michael Cullinan

The development of micro and nanoscale additive manufacturing methods in metals and ceramics is important for many applications in the aerospace, medical device, and electronics industries. Unfortunately, most commercially available metal additive manufacturing tools have feature-size resolutions of greater than 100 μm, which is too large to precisely control the microstructure of the parts they produce. A few research-grade metal additive manufacturing tools do exist, but their build rate is generally too slow for commercial applications. Therefore, this paper presents a new microscale selective laser sintering (μ-SLS) that can be used to improve the minimum feature-size resolution of metal additively manufactured parts by up to two orders of magnitude, while still maintaining the throughput of traditional additive manufacturing processes. In order to achieve this goal, several innovative design features like the use of (1) ultra-fast lasers, (2) a micro-mirror based optical system, (3) nanoscale powders, and (4) a precision spreader mechanism, have been implemented. The micro-SLS system is capable of achieving build rates of approximately 1 cm3/hr while achieving a feature-size resolution of approximately 1 μm. This paper will also present new molecular scale models that have been developed for the micro-SLS to quantify and certify the micro-SLS build process. Modeling of the micro-SLS process is challenging, because most macroscale models of the SLS process contain assumptions that are no longer valid when the size of the particles that are being sintered is smaller than the wavelength of the laser being used to sinter them. Therefore, in modeling the micro-SLS process we must account for the wave nature of light and can no longer rely on the ray tracing models commonly used to model the SLS process. Also, heat transfer in the micro-SLS process is dominated by near-field radiation due to the diffraction of the light off the nanoparticles in the powder bed and the ultrafast lasers that are used in the micro-SLS system. This means that the assumptions of heat transfer by conduction and far-field radiation in the macroscale SLS systems are no longer valid for the micro-SLS system. Finally, the agglomeration of nanoparticles in the powder bed must be accurately modeled in order to precisely predict the formation of defects in the final parts produced. Overall, the goal of this modeling effort is to be able to predict the quality of a part produced using any given processing conditions, in order to produce parts that are “born certified” and do not need to be tested post fabrication.


Author(s):  
Sachin Alya ◽  
Chaitanya Vundru ◽  
Ramesh Singh ◽  
Khushahal Thool ◽  
Indradev Samajdar ◽  
...  

Abstract Additive manufacturing (AM) technology is gaining enormous popularity in the manufacturing industries. The continuous improvements made in the AM processes features development of 3D metallic prototypes as well as fully functional end-use components. Direct Metal Laser Sintering (DMLS) is a pre-placed powder bed based technique, in which a thin layer of powder is place over the build tray and the areas need to be sintered are exposed to the laser. In the current work the microstructural and mechanical behavior of Inconel 718 parts produced by DMLS are investigated. As the DMLS produces parts in a layer by layer fashion, the orientation of parts with respect to the build direction is an important criterion. Microstructure and mechanical properties of the produce differs depending upon the orientation. This paper emphasize on the variation of grain sizes and grain orientations developed in the components built with different orientations. Another common issue with the additive manufacturing is the development of the residual stresses in the components arising due to the differential thermal gradients experienced during processing. The variation of the residual stress generated in the produced parts has also been characterized and modeled.


Author(s):  
Onome Scott-Emuakpor ◽  
Casey Holycross ◽  
Tommy George ◽  
Kevin Knapp ◽  
Joseph Beck

Vibratory bending fatigue behavior of titanium 6Al–4V plate specimens manufactured via direct metal laser sintering (DMLS), powder bed fusion additive manufacturing (AM), is assessed. Motivation for the work is based on unprecedented performance demands for sixth-generation gas turbine engine technology that requires complex, lightweight components. Due to cost, schedule, and feasibility limitations associated with conventional manufacturing, AM aims to address ubiquitous component concepts. Though AM has promise in the engine community, process controls necessary for consistent material properties remain an enigma. The following manuscript compares variability of DMLS fatigue and strength to cold-rolled data. Results show discrepancies between DMLS and cold-rolled for fatigue and microstructure characteristics.


Author(s):  
Lan Zhang ◽  
M'hamed Boutaous ◽  
Shihe Xin ◽  
Dennis A. Siginer

Abstract This work focusses on studying multiphysical transient phenomena in polymer powders occurring during selective laser sintering in polymers powders. Multiple phenomena stemming from the interaction of the laser with the polymer powder bed and the transfer of the laser power to the powder bed including laser scattering and absorption, polymer heating, melting, coalescence, densification, and the variation of the material parameters with the temperature are simulated via the modified Monte Carlo-ray tracing method coupled with the Mie theory. A finite volume method is adopted for the heat transfer. The model couples heat diffusion, melting, coalescence and densification of the polymer grains, and the crystallization kinetics during the cooling steps. Laser intensity is concentrated on the surface of the material contrary to the predictions of the Beer-Lambert law. Laser acting on thermoplastic material cause the polymer powder melt, coalescence between melted grains, air diffusion versus densification, crystallization and volume shrinkage. All these processes are simulated by a series of multiphysical models. The reliability of the modeling is tested by comparison with experiments in the literature, and a parametric analysis is performed, based on the process characteristics such as laser sweep speed, its intensity and shape, polymeric grain size among others. Several recommendations to optimize the process are proposed.


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