Use of gas chromatography–mass spectrometry combined with resolution methods to characterize the essential oil components of Iranian cumin and caraway

2007 ◽  
Vol 1143 (1-2) ◽  
pp. 215-226 ◽  
Author(s):  
Mehdi Jalali-Heravi ◽  
Behrooz Zekavat ◽  
Hassan Sereshti
2019 ◽  
Vol 14 (5) ◽  
pp. 1934578X1984270
Author(s):  
Ysbelia Obregón-Díaz ◽  
Alida Pérez-Colmenares ◽  
Karelys Obregón-Alarcón ◽  
Rosa Aparicio-Zambrano ◽  
Luis Rojas-Fermín ◽  
...  

The essential oil from the leaves of Kalanchoe pinnata (Lam.) Pers. (Crassulaceae), collected in the Venezuelan Andes, was obtained by hydrodistillation and its composition determined by gas chromatography (GC) and gas chromatography/mass spectrometry (GC/MS). Nineteen compounds were identified, representing 95.2% of the oil. The most abundant components were α-curcumene (44.7%), 1-octen-3-ol (18.1%), β-curcumene (4.9%), and β-caryophyllene (3.7%).


2010 ◽  
Vol 5 (8) ◽  
pp. 1934578X1000500
Author(s):  
Yuan Zhang ◽  
Zhezhi Wang

Gas chromatography (GC) and gas chromatography–mass spectrometry (GC–MS) were used to compare between the essential oil components from needles of Pinus armandii Franch versus P. tabulaeformis Carr., growing on the same site at Taibai Mountain, China. Under optimum extraction and analysis conditions, 65 and 66 constituents each were identified in P. armandii and P. tabulaeformis, which accounted for 87.9% and 87.1%, respectively, of their oils. Based on their terpene compositions, we concluded that these species belong to a high-caryophyllene chemotype, with sesquiterpenes comprising 54.4% to 54.8% of the total contents. We also determined minor qualitative and major quantitative variations in some compounds. Compared with that from P. tabulaeformis, P. armandii oil had more γ-muurolene (7.5%), terpinolene (5.8%), and longifolene (5.7%). In contrast, α-pinene (8.6%) and caryophyllene oxide (7.4%) were the dominant compounds in P. tabulaeformis.


2014 ◽  
Vol 2014 ◽  
pp. 1-9 ◽  
Author(s):  
Deribachew Bekana ◽  
Tesfahun Kebede ◽  
Mulugeta Assefa ◽  
Habtemariam Kassa

Oleogum resins of B. papyrifera, B. neglecta, and B. rivae were collected from northwestern, southern, and southeastern Ethiopia, and their respective methanol extracts and essential oils were extracted and analyzed by gas chromatography (GC) and gas chromatography-mass spectrometry (GC-MS). The investigation on essential oils led to the identification of 6, 7, and 8 constituents for B. papyrifera, B. neglecta, and B. rivae, respectively. The essential oil of B. papyrifera is mainly characterized by the presence of octyl acetate (57.1–65.7%) and n-octanol (3.4–8.8%). B. neglecta is rich in α-pinene (32.6–50.7%) followed by terpinen-4-ol (17.5–29.9%) and α-thujene (12.7–16.5%), whereas B. rivae was predominated by α-pinene (32.5–66.2%) followed by p-cymene (5.7–21.1%) and limonene (1.1–19.6%). Methanol extracts of the three Boswellia species were found to consist of diterpines (incensole, incensyl acetate and verticilla-4(20),7,11-triene), triterpenes (β-amyrin, α-amyrin, β-amyrenone, and α-amyrenone), nortriterpenes (24-noroleana-3,12-diene and 24-norursa-3,12-diene), and α-boswellic acid. The investigation on the methanol extract showed that only B. papyrifera contains diterpenes and nortriterpenes, whereas B. rivae and B. neglecta consist of only triterpenes. The results indicate that the three Boswellia species were characterized by some terpenes and these terpenoic constituents could be recognized as chemotaxonomical markers for each species.


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