Rapid determination of methanol content in paper materials by alkaline extraction, coupled with headspace analysis

2014 ◽  
Vol 1350 ◽  
pp. 10-14 ◽  
Author(s):  
Chun-Yun Zhang ◽  
Ling-Ling Li ◽  
Xin-Sheng Chai ◽  
Donald G. Barnes
2015 ◽  
Vol 69 (5) ◽  
Author(s):  
Qing-Qing Guan ◽  
Xiao-Dian Huang ◽  
Yan-Hua Zeng ◽  
Chao-Hai Wei ◽  
Ping Ning ◽  
...  

AbstractThis paper reports a headspace analysis technique for the determination of products, i.e., cyclohexanone (CE) and cyclohexanol (CL), of phenol hydrogenation in a supercritical water reaction system (SWRS) with water removal by hydrate formation. An addition of anhydrous calcium chloride leads to water absorption resulting in crystal water; thus, the samples can be quantitatively measured without the influence of water. After achieving equilibrium at 150­°C and maintaining it for 5 min, the obtained results showed a relative standard deviation of less than 5.3 % and the recovery ranged from 93 % to 104 %. The presented method is simple and accurate for the analysis of CL, CE and phenol in samples from phenol conversion in SWRS.


2014 ◽  
Vol 8 (4) ◽  
pp. 893-897 ◽  
Author(s):  
Chun-Yun Zhang ◽  
Neng-Biao Lin ◽  
Xin-Sheng Chai ◽  
Zhong Li ◽  
Donald G. Barnes

Author(s):  
T. Y. Tan ◽  
W. K. Tice

In studying ion implanted semiconductors and fast neutron irradiated metals, the need for characterizing small dislocation loops having diameters of a few hundred angstrom units usually arises. The weak beam imaging method is a powerful technique for analyzing these loops. Because of the large reduction in stacking fault (SF) fringe spacing at large sg, this method allows for a rapid determination of whether the loop is faulted, and, hence, whether it is a perfect or a Frank partial loop. This method was first used by Bicknell to image small faulted loops in boron implanted silicon. He explained the fringe spacing by kinematical theory, i.e., ≃l/(Sg) in the fault fringe in depth oscillation. The fault image contrast formation mechanism is, however, really more complicated.


2017 ◽  
Vol 45 (2) ◽  
pp. 455-464
Author(s):  
T.T. Xue ◽  
J. Liu ◽  
Y.B. Shen ◽  
G.Q. Liu

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