Pilot-scale extraction of zinc from the spent catalyst of vinyl acetate synthesis by microwave irradiation

2008 ◽  
Vol 92 (1-2) ◽  
pp. 79-85 ◽  
Author(s):  
Wei Li ◽  
Jinghui Peng ◽  
Libo Zhang ◽  
Zebiao Zhang ◽  
Lei Li ◽  
...  
Keyword(s):  
Microwave Irradiation ◽  
Vinyl Acetate ◽  
Pilot Scale ◽  
Spent Catalyst ◽  
Vinyl Acetate Synthesis

Structural Characterization of ZnO/AC Composite Prepared from Spent Catalyst of Vinyl Acetate Synthesis

2012 ◽  
Vol 518-523 ◽  
pp. 3483-3487
Author(s):  
Wen Wen Qu ◽  
Wen Jin ◽  
Jin Hui Peng ◽  
Shu Yang
Keyword(s):  
Thermal Treatment ◽  
Vinyl Acetate ◽  
Operating Conditions ◽  
Carbon Surface ◽  
X Ray Diffraction ◽  
Spent Catalyst ◽  
Activation Temperature ◽  
Vinyl Acetate Synthesis ◽  
Ft Ir ◽  
Co2 Flow

ZnO/AC composite was prepared from spent catalyst of vinyl acetate synthesis by using conventional thermal treatment under CO2 atmosphere. The final composite was obtained with the operating conditions of activation temperature of 950°C, activation time of 120min and the CO2 flow rate of 600ml/min. The structure and surface properties of the ZnO/AC composite were observed and characterized by scanning electron microscope (SEM-EDX), X-ray diffraction (XRD), fourier transform infrared spectroscopy (FT-IR) and the UV diffuse reflectance spectra. It was found that the zinc acetate present in the spent catalyst is transformed to zinc oxide (ZnO) after thermal treatment. ZnO particles were well adhered and uniformly distributed onto the carbon surface, forming ZnO/AC composite. The thermal treatment of the spent catalyst gives rise to a material with excellent adsorptive and photocatalytic properties.

Regeneration of spent catalyst from vinyl acetate synthesis as porous carbon: Process optimization using RSM

2014 ◽  
Vol 92 (7) ◽  
pp. 1249-1256 ◽  
Author(s):  
Xinhui Duan ◽  
Zebiao Zhang ◽  
C. Srinivasakannan ◽  
Fei Wang ◽  
Jinsheng Liang
Keyword(s):  
Vinyl Acetate ◽  
Process Optimization ◽  
Porous Carbon ◽  
Spent Catalyst ◽  
Vinyl Acetate Synthesis

Mechanistic Framework and Effects of High Coverage in Vinyl Acetate Synthesis

ACS Catalysis ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 1841-1857
Author(s):  
Zhaoru Zha ◽  
Prashant Deshlahra
Keyword(s):  
Vinyl Acetate ◽  
High Coverage ◽  
Vinyl Acetate Synthesis

Vinyl Acetate Synthesis on Homogeneous and Heterogeneous Pd-Based Catalysts: A Theoretical Analysis on the Reaction Mechanisms#

2009 ◽  
Vol 113 (43) ◽  
pp. 11758-11762 ◽  
Author(s):  
José J. Plata ◽  
Mónica García-Mota ◽  
Ataualpa A. C. Braga ◽  
Núria López ◽  
Feliu Maseras
Keyword(s):  
Theoretical Analysis ◽  
Vinyl Acetate ◽  
Reaction Mechanisms ◽  
Vinyl Acetate Synthesis
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