Application of direct atmospheric pressure chemical ionization tandem mass spectrometry for on-line analysis of gas phase of cigarette mainstream smoke

2013 ◽  
Vol 353 ◽  
pp. 42-48 ◽  
Author(s):  
Cheng-Yong Jiang ◽  
Shi-Hao Sun ◽  
Qi-Dong Zhang ◽  
Yu-Ping Ma ◽  
Hui Wang ◽  
...  
2001 ◽  
Vol 56 (7-8) ◽  
pp. 526-530 ◽  
Author(s):  
Nikolay Youhnovski ◽  
Christa Werner ◽  
Manfred Hesse

A new hydroxycinnamoyl polyamine derivative, N,N′,N″-triferuloylspermidine (= (E)-N-(4-aminobutyI)-3,3′,3″-tris(4-hydroxy-3-methoxyphenyl)-N,N′,N″-(butane-1,4-diyl)tris [prop-2-enamide]) (1) was detected in the H2O /MeOH extract of pollen from Hippeastrum × hortorum. The compound was identified by on-line-coupled high-performance liquid chromatography and atmospheric-pressure chemical-ionization mass spectrometry (HPLC-UV(DAD)/ APCI-MS and MS/MS). The structure was proven by comparing the HPLC/MS data after UV-induced (E) ⇄ (Z) photoisomerization and catalytic hydrogenation of the natural compound and the synthetic reference compound. This is the first report of a triferuloylspermidine in nature


2008 ◽  
Vol 80 (8) ◽  
pp. 2646-2653 ◽  
Author(s):  
Francisco J. Andrade ◽  
Jacob T. Shelley ◽  
William C. Wetzel ◽  
Michael R. Webb ◽  
Gerardo Gamez ◽  
...  

Sign in / Sign up

Export Citation Format

Share Document