Physicochemical characterization, water sorption and solubility of adhesive systems incorporated with titanium tetrafluoride, and its influence on dentin permeability

Author(s):  
Ruthinea Faria de Moraes Cardoso ◽  
Rosanna Tarkany Basting ◽  
Fabiana Mantovani Gomes França ◽  
Flávia Lucisano Botelho do Amaral ◽  
Roberta Tarkany Basting
2015 ◽  
Vol 34 (1) ◽  
pp. 1-6 ◽  
Author(s):  
Saryta ARGOLO ◽  
Paula MATHIAS ◽  
Thaiane AGUIAR ◽  
Adriano LIMA ◽  
Sara SANTOS ◽  
...  

2021 ◽  
Author(s):  
JMMS Cruz ◽  
ALGBM Silva ◽  
RMRF Eira ◽  
BMPR Sousa ◽  
MMN Lopes ◽  
...  

Clinical Relevance Universal adhesives do not seem to have the ability to effectively seal dentin, regardless of the mode of application. SUMMARY Purpose: This study evaluates the reduction in dentin permeability (P) and the expression of nanoleakage in resin-dentin interfaces made with universal adhesives, comparing the self-etch mode of application with the etch-and-rinse mode of application. Methods and Materials: To measure dentin P at the baseline and after adhesive polymerization, 80 extracted noncarious human third molars (N=80) were sectioned to obtain 0.7-mm-thick midcoronal dentin disks. The specimens were randomly assigned to 8 groups according to the different adhesive systems and application modes used: Scotchbond Universal (SBU; etch-and-rinse [ER] mode vs self-etch [SE] mode), OptiBond XTR (OPT; etch-and-rinse mode vs self-etch mode), Clearfil Universal Bond Quick (CL; etch-and-rinse mode vs self-etch mode), and Adhese Universal (ADH; etch-and-rinse mode vs self-etch mode). A two-way analysis of variance with interaction was used to evaluate the P reduction differences among the groups (α=0.05). Sixteen additional 0.7-mm-thick dentin disks were similarly prepared and treated, immersed in 50 wt% ammoniacal silver nitrate, and then processed according to conventional methods for analysis under transmission electron microscopy. Results: The differences in P reduction among the adhesives were significant (p=0.029). For OPT and ADH (p=0.0304 and p=0.0120, respectively), the P reduction was higher in the ER mode than in the SE mode. For CL and SBU, no differences in P reduction was observed between the two application modes (p>0.05). All the groups showed some pattern of nanoleakage. Conclusions: No adhesive system completely reduced dentin P. Dentin sealing was higher for OPT and ADH in the ER mode, while for SBU and CL, there was no difference between the two modes. All the adhesive systems showed nanoleakage.


2013 ◽  
Vol 2013 ◽  
pp. 1-5 ◽  
Author(s):  
Lívia Andrade Vitória ◽  
Thaiane Rodrigues Aguiar ◽  
Poliana Ramos Braga Santos ◽  
Andrea Nóbrega Cavalcanti ◽  
Paula Mathias

Aim. To evaluate the effect of cigarette smoke on water sorption and solubility of four adhesive systems. Materials and Methods. Sixteen disks of each adhesive system were prepared (Adper Scotchbond Multipurpose Adhesive (SA); Adper Scotchbond Multipurpose Adhesive System (Adhesive + Primer) (SAP); Adper Single Bond Plus (SB); Adper Easy One (EO)). Specimens were desiccated until a constant mass was obtained and divided into two groups (n=8). One-half of the specimens were immersed in deionized water, while the other half were also immersed, but with daily exposure to tobacco smoke. After 21 days, disks were measured again and stored in desiccators until constant mass was achieved. Data were calculated according to ISO specifications and statistically analyzed. Results. The tobacco smoke only significantly affected the water sorption and solubility of EO. There were significant differences in both analyses among materials tested. The SB exhibited the highest water sorption, followed by EO, which demonstrated significantly higher solubility values than SB. The SA and SAP showed low water sorption and solubility, and there were no significant differences between the two. Conclusion. Regardless of smoke exposure, both simplified adhesive systems presented an inferior performance that could be related to the complex mixture of components in such versions.


2014 ◽  
Vol 22 (4) ◽  
pp. 294-301 ◽  
Author(s):  
Talita Baumgratz Cachapuz CHIMELI ◽  
Paulo Henrique Perlatti D'ALPINO ◽  
Patrícia Nóbrega PEREIRA ◽  
Leandro Augusto HILGERT ◽  
Vinicius DI HIPÓLITO ◽  
...  

2014 ◽  
Vol 39 (4) ◽  
pp. 427-432 ◽  
Author(s):  
M Calabria ◽  
R Porfirio ◽  
S Fernandes ◽  
L Wang ◽  
M Buzalaf ◽  
...  

SUMMARY Dentin hypersensitivity (DH) is related to an increase in dentin permeability. This study tested the effect of titanium tetrafluoride (TiF4) compared with sodium fluoride (NaF) and potassium oxalate gel on reducing hydraulic conductance (Lp) from the perspective of diminishing dentin permeability. The Lp of the dentin disks (1.0 ± 0.2 mm) was evaluated using Flodec. The maximum Lp values of each disk were taken after phosphoric acid etching (15 seconds) and randomly allocated to seven groups (n=8) according to the treatments. The minimum (smear layer) and the maximum (after acid etching) Lp values were recorded. Treatments were performed for 4 minutes as follows: 1) NaF varnish 2) and solution (2.45% F, pH 5.0), 3) TiF4 varnish and 4) solution (2.45% F, pH 1.0), 5) 3% potassium oxalate gel, 6) free fluoride varnish (placebo, pH 5.0), 7) and no treatment (control). The Lp after each treatment was assessed. Samples were exposed to an erosive challenge (6% citric acid, pH 2.1, 1 minute), and the final Lp was recorded. The data were statistically analyzed using repeated measures two-way analysis of variance (p<0.05). All treatments were effective in reducing dentin Lp compared with the control immediately after the application. However, only potassium oxalate and NaF varnish significantly differed from placebo varnish (p<0.0001). The same results were found after the erosive challenge. Therefore, the TiF4 was less effective than the NaF varnish and potassium oxalate gel in reducing dentin permeability. Using this experimental model, both NaF varnish and potassium oxalate gel reduced the Lp similarly to the presence of smear layer.


2021 ◽  
Vol 34 (1) ◽  
pp. 10-17
Author(s):  
Fábia Roma ◽  
Karla Penha ◽  
Carlos Torres ◽  
Etevaldo Maia-Filho ◽  
Leily Firoozmand

Dentin hypersensitivity is caused by increased dentinal permeability due to total or partial exposure of dentinal tubules, which in turn can be produced by alterations of dental structures or failure of restorative procedures. The purpose of this in vitro study was to evaluate the efficacy of the application of different kinds of adhesive systems to prevent dentin permeability before and after an erosive challenge. Fifty bovine dentin discs (6x1 mm) were prepared and the specimens were divided into 5 groups (n=10): (SB2) Single Bond 2, (SBU) Universal Single Bond, (CSB) Clearfil SE Bond, (SM) Scotchbond Multipurpose and (C) Control. Hydraulic conductance of dentin was recorded after adhesive application (HC-1) and after erosive challenge (HC-2). Dentin surface images of post-treatment and post-erosive challenge were obtained by scanning electron microscopy (SEM). Data were analyzed using Kruskal Wallis, Mann-Whitney with Bonferroni correction and Wilcoxon tests (p<0.05). Reduction in dentin permeability was observed with the application of adhesive systems (p<0.05). After the erosive challenge, dentin permeability increased for SBU and CSB (p<0.05), while SB2 and SM did not differ in HC-1 or HC-2 (p>0.05). The conventional, self-etching and universal adhesive systems reduce dentinal permeability by more than 80%, and dentin demineralization may contribute to the increased permeability of universal and self-etching systems.


2015 ◽  
Vol 43 (12) ◽  
pp. 1491-1497 ◽  
Author(s):  
Eduardo Moreira da Silva ◽  
Carolina Ullmann Fernandes de Sá Rodrigues ◽  
Marcos Paulo de Oliveira Matos ◽  
Thais Rodrigues de Carvalho ◽  
Glauco Botelho dos Santos ◽  
...  

Author(s):  
Miguel Salvador- Figueroa ◽  
Dafne Castillo- López ◽  
Lourdes Adriano- Anaya ◽  
Didiana Gálvez- López ◽  
Raymundo Rosas- Quijano ◽  
...  

The main objectives of this study were; first formulate and evaluate some properties of chitosan composite films enriched with essential oils of cinnamon, thyme, clove, and lime alone or in combination; and second select the most appropriate formulation and evaluate their effect on physiological properties and fungal incidence of papaya Maradol stored at environmental tropical conditions. Breaking strength, thickness, color, moisture, water vapor permeability, solubility and water sorption of films were measured. Furthermore, in vitro activity was evaluated against Colletotrichum gloeosporioides Penz. Using multivariate analysis and based on the most desirable characteristics (low water sorption values, water vapor permeability, solubility, and greater inhibition of C. gloeosporioides), three formulations of films were used lately for coated fruit of papaya Maradol and stored at 28 ± 2 °C and 85 % RH. Two control treatments were included: one uncoated and other treated with Mancozeb® fungicide. At six days of storage, the fruit of both control treatments showed evident signs of ripening; contrary to the treatments wherein fruit were coated, and had low respiration, other attributes as firmness, little change in the external color of the fruit were manifested. Similarly, the use of composite films reduced the fungus C. gloeosporioides by 30-50 %. The use of film enriched with essential oil of 1 % cinnamon- 1 % thyme improved the characteristics of fruit quality, increased shelf life and reduced by 50 % the incidence of fungus in papaya Maradol stored under humid tropic environmental conditions. This coating can be an alternative to potentially reduce the need for cold storage during postharvest handling.


2014 ◽  
Vol 39 (6) ◽  
pp. 637-643 ◽  
Author(s):  
MRL Vale ◽  
FAC Afonso ◽  
BCD Borges ◽  
AC Freitas ◽  
A Farias-Neto ◽  
...  

SUMMARY Objective This study evaluated the degree of conversion (DC) and the water sorption/solubility of preheated single-bottle adhesive systems. Methods and Materials Five adhesive systems were tested: Adper Easy One and Adper Single Bond 2 (3M ESPE), Excite and Tetric N-Bond (Ivoclar/Vivadent), and XP Bond (Dentsply/Caulk). After storage for two hours at 25°C or 60°C, 50 samples (n=5) were prepared for all adhesive systems and stored dry in lightproof containers at 37°C for 24 hours. Fourier transform infrared/attenuated total reflectance spectroscopy was used to evaluate the DC, and water sorption/solubility was measured by means of mass loss and gain after water storage. The data were analyzed by two-way analysis of variance followed by Tukey's test (p&lt;0.05). Results Preheated adhesive systems showed statistically significantly higher DC than those kept at 25°C. Except for XP Bond, preheated adhesive systems presented statistically significantly lower water sorption/solubility means. Conclusions Preheating improved the DC for all tested adhesive systems. Also, it promoted a decrease of water sorption/solubility, except for the XP Bond adhesive system.


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