Influence of Co substitution for Fe on magnetic properties and crystal structure of soft magnetic Fe81.3Mo0.2Cu0.5Si4B14 alloy

2020 ◽  
Vol 512 ◽  
pp. 166681 ◽  
Author(s):  
L. Hawelek ◽  
M. Polak ◽  
P. Wlodarczyk ◽  
P. Zackiewicz ◽  
A. Radon ◽  
...  
2015 ◽  
Vol 1112 ◽  
pp. 19-22
Author(s):  
Umi Nuraini ◽  
Lita Amalia ◽  
Kurniawati C. Rosyidah ◽  
M. Zainuri

Synthesis of Zn doped Barium M-Hexaferrite (BaFe12-xZnxO19) has been performed by co-precipitation method. The purified iron sand from Tulungagung is used as a precursor of Fe3O4. Synthesis of Zn doped Barium M-Hexaferrite (BaFe12-xZnxO19) with variations of x = 0.3, 0.5, and 0.7 wt % has been calcined at temperatures of 1000°C for 5 hours. Ion Zn2+ (with 0 ≤ x ≤ 0.7 wt %) does not change the crystal structure of Barium M-Hexaferrite (BaM), but give a slight displacement of the peak position of the diffraction pattern. SEM figures showed that Zn doped Barium M-Hexaferrite (BaFe12-xZnxO19) have a hexagonal structure, similar to BaM structure. Doping of Zn has changed the magnetic properties of Barium M-Hexaferrit (BaM), from hard magnetic become soft magnetic. Barium M-Hexaferrit (BaM) has a value of Coercivity Field (Hc) and Remanence Magnetization (Mr) is 0.03734 T and 8.334 emu/g. At variation x = 0.3, the Remanence Magnetization (Mr) reaches the highest value. At this point, a value of Coercivity Field (Hc) and Remanence Magnetization (Mr) is 0.0506 T and 14.782 emu/gram respectively.


2021 ◽  
Vol 3 (1) ◽  
pp. 21-28
Author(s):  
Nining S Asri

The synthesis of soft magnetic NixZn1-xFe2O4 with variations in composition (x = 0,2 – 0,8) by the co-precipitation method has been carried out. The research objective was to determine the effect of x variation on the crystal structure, microstructure, magnetic properties, and density. The samples were characterized by their crystal structure using XRD, microstructure using FE-SEM, magnetic properties using VSM, and physical properties (True Density). The XRD analysis results obtained two phases, the major phase is nickel-zinc ferrite, and Fe2O3 shows as the minor phase. The crystal size increased and the lattice parameters decreased with the increase in nickel content. The results of FE-SEM analysis at x = 0.2 are spherical in shape with an average particle size found about 47.07 nm. The results of VSM analysis showed that the increase in nickel content, the higher the magnetization saturation value, and the super-paramagnetic properties of all samples obtained. The results of the analysis of physical properties show that true density decreases with an increase of nickel content in each sample.


1991 ◽  
Vol 30 (Part 1, No. 8) ◽  
pp. 1687-1691 ◽  
Author(s):  
Noriaki Taneko ◽  
Yutaka Shimada ◽  
Kazuaki Fukamichi ◽  
Akira Yoshihara ◽  
Chyoji Miyakawa

Author(s):  
Kaoru Sato

Sendust (Fe-9.6wt%Si-5.5wt%Al) is a well-known soft magnetic material. Attempts have been made recently to improve the corrosion resistance of this alloy by adding a fourth and/or a fifth element. Since the excellent magnetic properties of Sendust have been reported to be deeply related to its crystal structure, the DO3 structure, it is of vital importance to determine the crystallographic sites those additional elements occupy. In the present work I will report the results obtained for the site occupation of Ti, Cr and Co in Sendust alloys using the ALCHEMI method.Sendust containing 4.0%Cr, 3.0%Co+0.5%Nb and 2.0%Ti alloys were arc melted, then furnace-cooled from 1250°C. TEM specimens were prepared in a twin jet electropolisher using 5% perchrolic-acetic acid and the final thinning was done using an ion milling machine. The ALCHEMI experiment was performed in a Philips EM420T equipped with an EDAX 9900 system.All the specimens observed exhibited the diffraction spots which are associated with the DO3 structure (Fig. 1).


2009 ◽  
Vol 321 (5) ◽  
pp. 442-445 ◽  
Author(s):  
L. Peng ◽  
Q.H. Yang ◽  
H.W. Zhang ◽  
Y.Q. Song ◽  
J. Shen

Author(s):  
June D. Kim

Iron-base alloys containing 8-11 wt.% Si, 4-8 wt.% Al, known as “Sendust” alloys, show excellent soft magnetic properties. These magnetic properties are strongly dependent on heat treatment conditions, especially on the quenching temperature following annealing. But little has been known about the microstructure and the Fe-Si-Al ternary phase diagram has not been established. In the present investigation, transmission electron microscopy (TEM) has been used to study the microstructure in a Sendust alloy as a function of temperature.An Fe-9.34 wt.% Si-5.34 wt.% Al (approximately Fe3Si0.6Al0.4) alloy was prepared by vacuum induction melting, and homogenized at 1,200°C for 5 hrs. Specimens were heat-treated in a vertical tube furnace in air, and the temperature was controlled to an accuracy of ±2°C. Thin foils for TEM observation were prepared by jet polishing using a mixture of perchloric acid 15% and acetic acid 85% at 10V and ∼13°C. Electron microscopy was performed using a Philips EM 301 microscope.


1998 ◽  
Vol 22 (4_1) ◽  
pp. 186-189
Author(s):  
M. Matsumoto ◽  
A. Morisako ◽  
Y. Mutoh

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