Small-angle X-ray scattering and low-frequency Raman scattering study of liquid phase separation and crystallization in titania-containing glasses of the ZnO–Al2O3–SiO2 System

2005 ◽  
Vol 351 (8-9) ◽  
pp. 711-721 ◽  
Author(s):  
V.V. Golubkov ◽  
O.S. Dymshits ◽  
V.I. Petrov ◽  
A.V. Shashkin ◽  
M.Ya. Tsenter ◽  
...  
2013 ◽  
Vol 1518 ◽  
pp. 47-52
Author(s):  
S.V. Stefanovsky ◽  
B.S. Nikonov ◽  
B.I. Omelyanenko ◽  
K.M. Fox ◽  
J.C. Marra

ABSTRACTGlasses in the Al2O3-B2O3-Fe2O3-Na2O-SiO2 system were produced at a temperature of 1150 °C, annealed, and examined using XRD and SEM/EDX. Surfaces of same samples were additionally heat-treated and etched with HCl. The pristine samples were X-ray amorphous and rather homogeneous except the B1 sample that contained trace crystalline phases of carnegieite/nepheline and spinel. Corrosion of these glasses via an etching treatment proceeds by a conventional mechanism with damage of their surface layers, however, the B2 glass exhibits a “drop-type” microstructure after etching that suggests occurrence of liquid-liquid phase separation.


1972 ◽  
Vol 43 (4) ◽  
pp. 1636-1641 ◽  
Author(s):  
I. S. Patel ◽  
Paul W. Schmidt ◽  
Stanley M. Ohlberg

Soft Matter ◽  
2019 ◽  
Vol 15 (30) ◽  
pp. 6160-6170 ◽  
Author(s):  
Amélie Banc ◽  
Justine Pincemaille ◽  
Salvatore Costanzo ◽  
Edouard Chauveau ◽  
Marie-Sousai Appavou ◽  
...  

We investigate by time-resolved synchrotron ultra-small X-ray scattering the dynamics of liquid–liquid phase-separation of gluten protein suspensions following a temperature quench and show that viscous and gel samples exhibit distinctive features.


2020 ◽  
Vol 4 (10) ◽  
pp. 1888-1894
Author(s):  
Chris J. Benmore ◽  
Oliver L. G. Alderman ◽  
Sophie R. Benmore ◽  
Stephen K. Wilke ◽  
Richard J. K. Weber

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