Effectiveness of pretreatment with phosphoric acid, sodium hypochlorite and sulfinic acid sodium salt on root canal dentin resin bonding

Objective: To evaluate the effect of different irrigation solutions prior to post cementation on the resin bonding to bovine root dentine. Material and Methods: 60 bovine roots (16 mm) were prepared to 12 mm with specific drill of a double-tapered fiber post system, included in PMMA, and divided into 6 groups, considering the irrigation solutions (IS) prior to cementation: Gr1- saline solution (control), Gr2- NaOCl 0.5 %, Gr3- NaOCl 1 %, Gr4- NaOCl 2.5 %, Gr5- NaOCl 5 %, Gr6- Chlorexidine 2 % (solution). The root canals were irrigated with IS 20 ml during 10 min. Then they were rinsed with 20 ml of distilled water and dried with paper points. One fiber post was molded with polyvinylsiloxane and 60 posts made of resin cement (PRC) were obtained moments before the cementation. The root canal dentin was etched with H2PO3 37 %/15 s + washing/drying, a multi-bottle etch&rinse adhesive system was applied and the PRC were resin luted with dual resin cement (DuolinkTM, Bisco). Each specimen was cut into 4 slices of ±1.8mm in thickness and submitted to push-out test (1 mm/min). Results: ANOVA showed that bond strength was significantly affected by IS (P<0.0001). The highest bond strengths (MPa) were those for the groups 4 (3.51 ± 1.52) and 5 (3.0 ± 1.16). The groups 1 (0.70 ± 0.30), 2 (0.80 ± 0.24), 3 (1.26 ± 0.57) and 6 (0.90 ± 0.41) were statistically similar to each other. Conclusion: The resin bonding to the root dentine was higher when higher concentrations of hypochlorite solutions were used.KeywordsBond strength; Irrigation solutions; Push-out test; Resin cement; Root canal dentin.

Download Full-text

Pengaruh Konsentrasi dan Lama Aplikasi Sodium Hipoklorit (NaOCL) sebagai Bahan Irigasi Saluran Akar terhadap Kekuatan Geser Perlekatan Siler Berbahan Dasar Resin Pada Dentin Saluran Akar

Majalah Kedokteran Gigi Indonesia ◽

10.22146/majkedgiind.15646 ◽

2012 ◽

Vol 19 (1) ◽

pp. 21

Author(s):

Tunjung Nugraheni

Keyword(s):

Bond Strength ◽

Sodium Hypochlorite ◽

Root Canal ◽

Shear Bond Strength ◽

Testing Machine ◽

Universal Testing Machine ◽

Root Canal Irrigation ◽

Universal Testing ◽

Group I ◽

Root Canal Dentin

Latar belakang. Salah satu tahap penting perawatan saluran akar yaitu preparasi saluran akar. Pada preparasi saluran akar digunakan bahan Irigasi sodium hipoklorit (NaOCI), dengan konsentrasi 0,5%-5.25%. Penggunaan NaOCL berpengaruh pada struktur permukaan dentin saluran akar, yang selanjutnya mempengaruhi perlekatan dentin saluran akar dengan bahan pengisi saluran akar. Penelitian ini bertujuan untuk mengetahui pengaruh konsentrasi dan lama aplikasi NaOCI terhadap kekuatan geser perlekatan siler berbahan dasar resin pada dentin saluran akar. Metode Penelitian. Tiga puluh gigi premolar dipotong arah bukolingual, jaringan pulpa dibersihkan dan permukaan dentin saluran akar diratakan. Gigi difiksasi resin akrilik, sisi dentin saluran akar menghadap ke atas. Sampel dibagi menjadi 2 kelompok masing-masing 15 gigi, kelompok 1 di rendam dalam 6ml NaOCI 2,5%. Kelompok II direndam dalam 6 ml NaOCI 5%. Kelompok I dan II dibagi menjadi 3 sub kelompok lama perendaman, yaitu sub kelompok a direndam selama 5 menit, sub kelompok diremdam selama 10 menit, sub kelompok direndam selama 15 menit. Cetakan siler difiksasi pada akar gigi, dilakukan insersi siler ke dalam cetakan kemudian dimasukkan inkubaror pada suhu 370 C selama 72 jam. Pengujian kekuatan geser perlekatan menggunakan Universal Testing Machine. Hasil penelitian. Hasil uji statistik AVANA dua jalur menunjukkan kekuatan geser perlekatan siler berbahan dasar resin pada dentin saluran akar setelah diirigasi dengan konsentrasi NaOCI dan lama irigasi yang berbeda terdapat perbedaan yang bermakna (p=0,007). Uji LSD menunjukkan bahwa kekuatan geser perlekatan siler berbahan dasar resin berbeda bermakna pada kelompok yang diirigasi NaOCI 2,5% selama 5 menit dengan 15 menit,, pada kelompok yang diirigasi NaOCI 2,5% selama 10 menit dengan 15 menit, pada kelompok yang diirigasi NaOCI 5% selama 15 menit dengan kelompok yang diirigasi NaOCI 2,5% selama 15 menit serta pada kelompok yang diirigasi NaOCI 5% selama 5 menit dengan kelompok yang diirigasi NaOCI 5% selama 10 menit. Kesimpulan. Kekuatan geser perlekatan siler berbahan dasar resin pada dentin saluran akar berbeda setelah diirigasi NaOCI dengan konsentrasi dan waktu irigasi yang berbeda. Background. Biomechanichal preparationin of root canal treatment used 0,5-5,25% sodium Hypochlorite as root canal irrigation, that may effect to physical properties of dentin. The purpose of this study was to find out the effect of concentration and duration application of sodium hypochlorite to shear bond strength of sealer resin based to root canal dentin. Methods. Thirthy premolar were splitted buccolingual then pulp tissue were cleaned out, smoothed and fixed into acrylic resin cast. They were devided into 2 group, group I were soaking into NaOCI 2,5% group II were soaking into NaOCI 5%. Group I and II were devided into 3 subgroup, group a were soaking 5 minutes, group b were soaking 10 minutes. Group c were soaking 15 minutes. Then sealer cast were fixed and filled with sealer resin-based, and incubated for 74 hours. They were tested for shear bond strength with Universal Testing Machine. The data were analyzed with two way Anava and LSD. Result. Two way Avana show that shear bond strength of sealer resin-based to root canal after irrigation with different concentration and duration application of sodium hypochlorite are significant. Conclusion. Shear bond strength of sealer resin-based to root canal dentin after irrigation with different concentration and duration application of sodium hypochlorite are different.

Download Full-text