Solvothermal synthesis of uniform hexagonal-phase ZnS nanorods using a single-source molecular precursor

2006 ◽  
Vol 41 (10) ◽  
pp. 1817-1824 ◽  
Author(s):  
Yong Cai Zhang ◽  
Gui Yun Wang ◽  
Xiao Ya Hu ◽  
Wei Wei Chen
Keyword(s):  
Solvothermal Synthesis ◽  
Hexagonal Phase ◽  
Single Source ◽  
Molecular Precursor

Solvothermal Synthesis of Mn-Doped CdS Nanorods Using Single-Source Molecular Precursors

2011 ◽  
Vol 284-286 ◽  
pp. 667-670
Author(s):  
Zhen Ni Du ◽  
Zhi You Xu ◽  
Yong Cai Zhang ◽  
Ming Zhang
Keyword(s):  
Electron Microscopy ◽  
Solvothermal Synthesis ◽  
Hexagonal Phase ◽  
Single Source ◽  
X Ray Diffraction ◽  
X Ray ◽  
Molecular Precursors ◽  
Cds Nanorods ◽  
Transmission Electron ◽  
Mn Doped

The synthesis of hexagonal phase Mn-doped CdS (Cd1-xMnxS) nanorods was achieved by solvothermal treatment of a class of easily obtained, air-stable single-source molecular precursors (cadmium manganese diethyldithiocarbamates, Cd1-xMnx-(DDTC)2) in ethylenediamine at 180 °C for 12 h. The structures and compositions of the as-synthesized products were characterized by X-ray diffraction, energy dispersive X-ray spectroscopy and transmission electron microscopy.

Solvothermal Synthesis of Phase-Pure CuInS2 Hierachical Nanostructure Using Single-Source Molecular Precursor

2011 ◽  
Vol 266 ◽  
pp. 9-12
Author(s):  
Jing Li ◽  
Yong Cai Zhang ◽  
Ming Zhang
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Solvothermal Synthesis ◽  
Single Source ◽  
X Ray Diffraction ◽  
X Ray ◽  
Molecular Precursor ◽  
Copper Indium ◽  
Phase Pure ◽  
Scanning Electron

The synthesis of phase-pure CuInS2 microclusters comprising nanoflakes was achieved by solvothermal treatment of copper indium diethyldithiocarbamates (compositionally CuIn-(DDTC)5) in ethanol at 190 °C for 36 h. The obtained product was characterized by X-ray diffraction, Raman, energy dispersive X-ray spectroscopy and field emission scanning electron microscopy. Besides, contrast synthesis tests using multi-source precursors were also conducted.

Facile and selective synthesis of zeolites L and W from a single-source heptanuclear aluminosilicate precursor

CrystEngComm ◽  
2020 ◽  
Vol 22 (35) ◽  
pp. 5862-5870
Author(s):  
Akira Imaizumi ◽  
Akinobu Nakada ◽  
Takeshi Matsumoto ◽  
Ho-Chol Chang
Keyword(s):  
Selective Synthesis ◽  
Single Source ◽  
Molecular Precursor ◽  
First Time

Zeolites L and W were synthesized for the first time from a heptanuclear aluminosilicate complex as a single-source molecular precursor, highlighting the potential versatility of this approach toward the synthesis of a variety of zeolites.

Hydrothermal Synthesis of Hexagonal Phase Zn1-XMnxS (x = 0–0.05) Nanorods Using Single-Source Precursors

2010 ◽  
Vol 663-665 ◽  
pp. 100-103
Author(s):  
Zhen Ni Du ◽  
Yong Cai Zhang ◽  
Zhi You Xu ◽  
Ming Zhang
Keyword(s):  
Electron Microscopy ◽  
Aqueous Solution ◽  
Transmission Electron Microscopy ◽  
Hydrothermal Synthesis ◽  
Diffuse Reflectance ◽  
Hexagonal Phase ◽  
Single Source ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron

The synthesis of hexagonal phase Zn1-xMnxS (x = 0–0.05) nanorods was achieved by hydrothermal treatment of zinc manganese diethyldithiocarbamates (Zn1-xMnx-(DDTC)2, x=0–0.05) in 40 mass % hydrate hydrazine aqueous solution at 180 °C for 12 h. The structure, composition and optical property of the obtained products were characterized by X-ray diffraction, energy dispersive X-ray spectroscopy, transmission electron microscopy and UV-vis diffuse reflectance spectra.

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