Abnormal growth of columnar grains and formation of Σ3 grain boundaries in non-oriented electrical steels

2020 ◽  
Vol 269 ◽  
pp. 127671
Author(s):  
Li Xie ◽  
Mingtao He ◽  
Jiangtao Wang ◽  
Jian Wang ◽  
Yalin Lu ◽  
...  
2013 ◽  
Vol 753 ◽  
pp. 173-176
Author(s):  
Ping Yang ◽  
Yuan Yuan Shao ◽  
Ning Zhang ◽  
Ling Cheng ◽  
Wei Min Mao

The crystallographic and topographic anisotropies of columnar grains can exert strong influence on the subsequently hot rolled, cold rolled and annealed microstructures, textures and properties. The single type tilting grain boundaries among columnar grains will behave differently depending on grain orientations, rolling direction and stress state due to hot rolling and thus affect in return the microstructure and texture to some extents. This work aims to reveal the effects of grain boundaries and their neighboring grain orientation gradients in three types of Fe-3Si in differently processed samples using EBSD technique.


2011 ◽  
Vol 702-703 ◽  
pp. 738-741
Author(s):  
H. Qian ◽  
Ping Yang ◽  
G.H. Zheng ◽  
Wei Min Mao

To identify the relationship between grain orientation and precipitation of MnS/AlN particles during hot deformation, cylinder samples containing columnar grains in electrical steels were prepared with different angles between columnar grain axis and sample axis. They were heated at 1360°C and compressed at 1100°C for 50%. Grain orientations and the precipitation states are determined using XRD, EBSD, EDS and SEM. Results indicate a general behavior of less precipitates in <100> and more precipitates in <111> grains. In addition, more precipitates were observed in samples with grain boundaries perpendicular to compression axis.


2010 ◽  
Vol 1249 ◽  
Author(s):  
Murata Naokazu ◽  
Kinji Tamakawa ◽  
Ken Suzuki ◽  
Hideo Miura

AbstractMicro-texture dependence of both the mechanical and electrical properties of electroplated copper thin films was discussed experimentally considering the change of their micro texture caused by thermal history after the electroplating. Both the static and fatigue strength of the films changed drastically depending on the micro texture and it was found that there were two fatigue fracture modes in the films. One was a typical ductile intragranular fracture and the other was brittle intergranular one. The reason for the variation of the strength of the electroplated copper thin films was attributed to the variation of the average grain size and the characteristics of grain boundaries. In addition, the electrical reliability of the electroplated copper interconnections was discussed under electromigration tests. Though abrupt fracture mode due to the local fusion appeared in the as-electroplated films, the life of the interconnections was improved significantly after the annealing at temperatures high than 200°C. Typical change of the surface morphology of the film, i.e., the formation of voids and hillocks were observed on their surfaces after the annealing. This was also caused by the change of the micro texture from fine grains with porous grain boundaries to coarsened columnar grains with rigid grain boundaries. However, the stress-induced migration appeared in the annealed narrow interconnections, in particular. This was because of high tensile residual stress occurred in the film due to the constraint of the shrinkage of the films by rigid oxide around them. These results clearly indicated that the control of both the micro-texture and residual stress is indispensable for improving the reliability of the interconnectins.


1994 ◽  
Vol 343 ◽  
Author(s):  
S. J. Townsend ◽  
C. S. Nichols

ABSTRACTDuring grain growth, shrinking columnar grains in thin-film polycrystalline microstructures eventually reach sizes comparable to the film thickness. Due to surface drag, the sides of such grains may bow inward rather than remaining fiat through the bulk of the film. The grain boundaries delimiting such small shrinking grains may become unstable long before the surface of the shrinking grain reaches zero area. We report simulation results demonstrating such an instability in the limit of infinite surface drag. This may lead to extremely rapid disappearance of 4- or 5- sided grains, such as have been recently observed in in situ hot-stage TEM experiments on aluminum thin film polycrystals.


2016 ◽  
Vol 254 ◽  
pp. 97-101
Author(s):  
Sergiu Barbos ◽  
Andrei Novac ◽  
Roxana Sprincenatu ◽  
Madalin Condel ◽  
Ion Mitelea ◽  
...  

Ti-Ta films were deposited out of Ti and Ta targets on glass and kapton substrates. The co-deposition leaded to the formation of a compositional spread in the Ti-Ta system, a continuous variation of the Ta/Ti ratio along the full range of the film. The typical microstructure observed for the films deposited at RT consisted of columnar grains with dotted Ta-rich particles, reflecting a relatively nonhomogenous structure. Annealing at 400 °C leaded to the individualization of grain boundaries and to a coalescence of the Ta-rich particles. Annealing at 500 °C further reduced the amount of particles, but also appeared to be associated with the cracking in the stressed area of the film/kapton structure.


2011 ◽  
Vol 702-703 ◽  
pp. 754-757 ◽  
Author(s):  
Ping Yang ◽  
Y.Y. Shao ◽  
W.M. Mao ◽  
Q.W. Jiang ◽  
W.X. Jin

The texture evolution in the surface and center layer of hot rolled electrical steel containing initial columnar grains with their <100> nearly along ND, RD and TD of sheets were determined by EBSD technique. The transition from Goss to Brass or Copper orientation in surface was analyzed. The difference in texture of center layers in these samples was compared. In particular, orientation evolutions within grains and at grain boundaries of different types of orientations were explored. The results are discussed in terms of the special alignments of grain boundaries among columnar grains.


Author(s):  
Naokazu Murata ◽  
Kinji Tamakawa ◽  
Ken Suzuki ◽  
Hideo Miura

Electroplated copper thin films have been used for interconnection of semiconductor devices. Both the mechanical and electrical properties of the films were found to be quite different from those of bulk material, and thus, the reliability of the devices is not so high as to be expected. The main reason for the difference was found to be their micro texture. When the films consist of fine columnar grains with weak grain boundaries, their mechanical properties show strong anisotropy and complicated fracture mode. Thus, the fatigue strength of the electroplated copper thin films was measured under uniaxial stress. The mechanical properties such as the yield stress, fracture elongation and Young’s modulus of each film were quite different from those of bulk copper due to their unique micro structure. The micro texture of each film was observed by using SEM (Scanning Electro Microscope) and SIM (Scanning Ion Microscope). The low-cycle fatigue strength varied drastically depending on their micro texture, while the high-cycle fatigue strength was almost same. The fracture surfaces were observed by SEM after the fatigue test. It was found that there were two fracture modes under the fatigue test. One was a typical ductile fracture, and the other was brittle one even under the fatigue load higher than its yield stress. The crack seemed to propagate in the grains when the ductile fracture occurred since typical striations and dimples were observed clearly on the fractured surfaces. On the other hand, the crack seemed to propagate along grain boundaries of columnar grains when the brittle fracture occurred. No striations or dimples remained on the fractured surfaces. One of the reasons for this brittle fracture can be explained by cooperative grain boundary sliding of the films which consist of fine columnar grains with weak grain boundaries. These results clearly indicated that the fatigue strength of the electroplated copper thin films varies depending on their micro structure. Since the initial micro texture was found to change significantly even after the annealing at temperatures lower than 300°C, the effect of the thermal history of them after electroplating on both their micro texture and fatigue strength was investigated quantitatively. Not only the average grain size, but also the crystallographic structure of the films changed significantly depending on their thermal history, and thus, the fatigue strength of the films varied drastically. It is important, therefore, to control the micro texture of the films for assuring their reliability.


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