Investigation on mechanical properties and microstructure of silicon nitride ceramics fabricated by spark plasma sintering

2018 ◽  
Vol 731 ◽  
pp. 595-602 ◽  
Author(s):  
Liyan Cao ◽  
Zhenhua Wang ◽  
Zengbin Yin ◽  
Kui Liu ◽  
Juntang Yuan
Materials ◽  
2020 ◽  
Vol 13 (22) ◽  
pp. 5221
Author(s):  
Jaroslaw Wozniak ◽  
Mateusz Petrus ◽  
Tomasz Cygan ◽  
Artur Lachowski ◽  
Bogusława Adamczyk-Cieślak ◽  
...  

This paper discusses the influence of Ti3C2 (MXene) addition on silicon nitride and its impact on the microstructure and mechanical properties of the latter. Composites were prepared through powder processing and sintered using the spark plasma sintering (SPS) technic. Relative density, hardness and fracture toughness, were analyzed. The highest fracture toughness at 5.3 MPa·m1/2 and the highest hardness at HV5 2217 were achieved for 0.7 and 2 wt.% Ti3C2, respectively. Moreover, the formation of the Si2N2O phase was observed as a result of both the MXene addition and the preservation of the α-Si3N4→β-Si3N4 phase transformation during the sintering process.


2014 ◽  
Vol 13 (1) ◽  
Author(s):  
Eszter Bódis ◽  
Orsolya Tapasztó ◽  
Zoltán Károly ◽  
Péter Fazekas ◽  
Szilvia Klébert ◽  
...  

AbstractMulitlayer graphene reinforced silicon nitride composites were prepared by spark plasma sintering to investigate the effect of the graphene addition on mechanical properties. The composites contained multilayer graphene (MLG) in various (0, 1, 3 and 5 wt%) content. Significantly higher fracture toughness of 8.0 MPa m


2015 ◽  
Vol 644 ◽  
pp. 159-170 ◽  
Author(s):  
N. Azeggagh ◽  
L. Joly-Pottuz ◽  
J. Chevalier ◽  
M. Omori ◽  
T. Hashida ◽  
...  

2011 ◽  
Vol 31 (4) ◽  
pp. 645-652 ◽  
Author(s):  
Helen Reveron ◽  
Laurent Blanchard ◽  
Yann Vitupier ◽  
Emmanuelle Rivière ◽  
Guillaume Bonnefont ◽  
...  

Author(s):  
Aqib Hussain Mir ◽  
SN Ahmad

The present study provides an overview of the fabrication of silicon nitride (Si3N4)-based advanced ceramic materials using spark plasma sintering. Being an excellent engineering ceramic material, silicon nitride is extensively being used in tribological components, aerospace, and automotive industries due to its unique blend of thermo-mechanical, tribological, and chemical properties. The selection of the sintering process, as well as sintering aids, strongly affects the properties of silicon nitride ceramics. Several conventional sintering techniques have been utilized in the past to optimize the structure and properties of silicon nitride ceramics such as hot pressing. However, spark plasma sintering, a relatively new, non-conventional, powder consolidating technique has recently gained significant attention to fabricate silicon nitride ceramic due to high heating rates, extremely short sintering time, and relatively low sintering temperatures which renders it an ideal technique for mass production. Both the composition and concentration of sintering additives during processing play a vital part in achieving the final desired properties of the bulk silicon nitride ceramic materials. In this review, the critical aspects like the effects of additive composition, additive concentration, and sintering parameters on microstructure and bulk properties of silicon nitride ceramics fabricated via spark plasma sintering are presented. The review may come in handy for scientists and engineers concerned with fabricating future silicon nitride composites with desired properties and performance for different engineering applications.


2011 ◽  
Vol 49 (01) ◽  
pp. 40-45 ◽  
Author(s):  
Hyun-Kuk Park ◽  
Seung-Min Lee ◽  
Hee-Jun Youn ◽  
Ki-Sang Bang ◽  
Ik-Hyun Oh

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