Microwave-assisted synthesis of carbon nanotubes threaded core-shell CoP /Co-N -C@CNT and its performance as an efficient bifunctional oxygen catalyst for the rechargeable zinc-air battery

2019 ◽  
Vol 9 ◽  
pp. 100132 ◽  
Author(s):  
X. Wu ◽  
S. Chen ◽  
Y. Feng ◽  
Q. Yuan ◽  
J. Gao ◽  
...  
2017 ◽  
Vol 2017 ◽  
pp. 1-4 ◽  
Author(s):  
N. Kure ◽  
M. N. Hamidon ◽  
S. Azhari ◽  
N. S. Mamat ◽  
H. M. Yusoff ◽  
...  

In this work, a quick and effective method to synthesize carbon nanotubes (CNTs) is reported; a commercial microwave oven of 600 W at 2.45 GHz was utilized to synthesize CNTs from plasma catalytic decomposition of polyethylene. Polyethylene and silicon substrate coated with iron (III) nitrate were placed in the reaction chamber to form the synthesis stock. The CNTs were synthesized at 750°C under atmospheric pressure of 0.81 mbar. Raman spectroscopy and field emission scanning electron microscope revealed the quality and entangled bundles of mixed CNTs from which the diameters of the CNTs were calculated to be between 1.03 and 25.00 nm. High resolution transmission electron microscope further showed that the CNTs obtained by this method are graphitized. Energy dispersive X-ray analysis and thermogravimetric analysis revealed above 98% carbon purity.


RSC Advances ◽  
2016 ◽  
Vol 6 (116) ◽  
pp. 115317-115325 ◽  
Author(s):  
Yaru Yan ◽  
Qitong Huang ◽  
Chan Wei ◽  
Shirong Hu ◽  
Hanqiang Zhang ◽  
...  

Cyclic voltammetry of HQ and CC recorded on Nafion/CDs–ZnO/MWCNTs/GCE.


2012 ◽  
Vol 2012 ◽  
pp. 1-15 ◽  
Author(s):  
Sarah C. Motshekga ◽  
Sreejarani K. Pillai ◽  
Suprakas Sinha Ray ◽  
Kalala Jalama ◽  
Rui. W. M. Krause

The study of coating carbon nanotubes with metal/oxides nanoparticles is now becoming a promising and challenging area of research. To optimize the use of carbon nanotubes in various applications, it is necessary to attach functional groups or other nanostructures to their surface. The combination of the distinctive properties of carbon nanotubes and metal/oxides is expected to be applied in field emission displays, nanoelectronic devices, novel catalysts, and polymer or ceramic reinforcement. The synthesis of these composites is still largely based on conventional techniques, such as wet impregnation followed by chemical reduction of the metal nanoparticle precursors. These techniques based on thermal heating can be time consuming and often lack control of particle size and morphology. Hence, there is interest in microwave technology recently, where using microwaves represents an alternative way of power input into chemical reactions through dielectric heating. This paper covers the synthesis and applications of carbon-nanotube-coated metal/oxides nanoparticles prepared by a microwave-assisted method. The reviewed studies show that the microwave-assisted synthesis of the composites allows processes to be completed within a shorter reaction time with uniform and well-dispersed nanoparticle formation.


2016 ◽  
Vol 40 (9) ◽  
pp. 7986-7995 ◽  
Author(s):  
Zohre Zarnegar ◽  
Javad Safari

The microwave-assisted synthesis of the first ionic liquid stabilized CNTs–Fe3O4as a novel nanocatalyst for the synthesis of 2-amino-chromenesviaa multicomponent reaction is reported.


2011 ◽  
Vol 2011 ◽  
pp. 1-3
Author(s):  
Manuel Ramos ◽  
Karina Castillo ◽  
Domingo A. Ferrer ◽  
Rurik J. Farias ◽  
Sergio Flores ◽  
...  

Core-Shell (Fe3O4/Au) nanoparticles were synthesized using iron II chloride tetrahydrate (FeCl2H2O) and potassium tetrachloroaurate III (AuCl4K) precursors under microwave-assisted conditions. Products were analyzed using field emission gun electron microscope in transmission and scanning modes; energy disperse X-ray spectroscopy performed during STEM measurements indicated a signal for gold K and M signals at 9 keV and 13 keV, respectively, confirming Au atoms at nanoparticle's perimeter and Fe-L signal at 8 keV to be at the center.


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