Design and optimization of sensitive analytical spectrophotometric method for micro determination of copper(II) from e-waste by using of novel chromogenic extractant

Author(s):  
Sangram B. Kharade ◽  
Rajvardhan K. Chougale ◽  
Umesh B. Barache ◽  
Kallappa R. Sanadi ◽  
Kishan C. Rathod ◽  
...  
1967 ◽  
Vol 50 (2) ◽  
pp. 338-339
Author(s):  
Duane H Strunk ◽  
A A Andreasen

Abstract A collaborative study was conducted on the 'atomic absorption spectrophotometric method for measuring the concentration of copper in alcoholic products. In this method, the samples are aspirated directly into the burner of the instrument, and the absorhance values are converted to ppm copper by reference to a standard curve. Data show good precision and are comparable to those obtained by the ZDBT method. It is recommended that the atomic absorption method be adopted as official, first action.


2011 ◽  
Vol 8 (2) ◽  
pp. 587-593 ◽  
Author(s):  
Maliheh Barazandeh Tehrani ◽  
Effat Souri

A simple and sensitive derivative spectrophotometric method for simultaneous determination of nickel and copper using 6-(2- naphthyl)-2,3-dihydro-1,2,4-triazine-3-thione (NDTT) as a selective analytical reagent was developed. The complexes of metal ions with NDTT were formed immediately in basic media and extracted with chloroform. The zero-crossing measurement technique was found suitable for the direct measurement of the third-derivative value of Ni-NDTT and Cu-NDTT at 501 and 472 nm respectively. Beer’s law is obeyed in the concentration range 1-30 μg/mL for both cations with different ratios. The limit of detection was 0.26 μg/mL and 0.13 μg/mL for copper and nickel respectively. The within day and between day variations showed coefficient of variation (CV%) values less than 2.80 and 2.97 for copper and nickel respectively. The error of the determination method did not exceed 6.50%. Analysis of alloy sample showed that this method can be successfully used for simultaneous determination of Cu and Ni in real samples.


2017 ◽  
Vol 58 (2) ◽  
Author(s):  
Carlos Andrés Galán-Vidal ◽  
Araceli Castañeda-Ovando ◽  
Ma. Elena Páez-Hernández ◽  
Elizabeth Contreras-López

<p>With the purpose of obtaining the main factors in the nitrite quantification by bleaching Roselle anthocyanins, an experimental design (2<sup>3</sup>) was carried out. The control factors were ultrasound, time and temperature at two levels (−, +). Results for sausages analysis were obtained by the colorimetric method of AOAC 973.31, and the proposed spectrophotometric method. Statistical analysis show that results do not differ significantly. A better linear calibration range is obtained using this new method. The main advantage is the reagents that are used are cheaper.</p>


1980 ◽  
Vol 61 (6) ◽  
pp. 58-59
Author(s):  
N. A. Roshina

The principle of our proposed method consists in the sorption of copper-containing urine compounds on an ion-exchange resin (Elgostat type) with the subsequent liberation of the free metal and its spectrophotometry determination in the form of a diethyldithio-carbamate complex.


2014 ◽  
Vol 6 (21) ◽  
pp. 8494-8504 ◽  
Author(s):  
Piyawan Phansi ◽  
Camelia Henríquez ◽  
Edwin Palacio ◽  
Duangjai Nacapricha ◽  
Víctor Cerdà

An automated in-chip-catalytic–spectrophotometric method for determination of copper(ii) using a multisyringe flow injection analysis-multipumping flow system (Chip–MSFIA–MPFS).


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