Electrophoretic deposition of tetracycline hydrochloride loaded halloysite nanotubes chitosan/bioactive glass composite coatings for orthopedic implants

2017 ◽  
Vol 327 ◽  
pp. 146-157 ◽  
Author(s):  
Namir S. Radda'a ◽  
Wolfgang H. Goldmann ◽  
Rainer Detsch ◽  
Judith A. Roether ◽  
Luis Cordero-Arias ◽  
...  
2015 ◽  
Vol 654 ◽  
pp. 189-194 ◽  
Author(s):  
S. Borjas ◽  
E.J. Gil ◽  
L. Cordero ◽  
J.J. Pavón ◽  
J.A. Rodriguez-Ortiz ◽  
...  

Porous titanium samples of cp Ti grade IV were obtained by space-holder technique (50%vol of NH4HCO3, 800 MPa, 1250 oC during 2h in high vacuum), producing a good balance between stiffness and mechanical strength. The samples were coated with chitosan/45S5 bioactive glass composite by electrophoretic deposition. Homogeneity, infiltration efficiency, and coatings integrity (cracking and adhesion) were evaluated in order to establish correlations with processing parameters. SEM, FTIR, and contact profilometry were performed for detailed characterization of the coatings; and micro-mechanical properties (P-h curves and scratch testing) were set-up as well. Optimum EPD parameters were 25V, 7 min and suspension containing 0.5 g/L chitosan and 1.5 g/L BG a titanium structure with pore sizes greater than 200 μm are required.


Author(s):  
Marta Miola ◽  
Enrica Verné ◽  
Francesca Elisa Ciraldo ◽  
Luis Cordero-Arias ◽  
Aldo R. Boccaccini

2017 ◽  
Vol 232 ◽  
pp. 456-464 ◽  
Author(s):  
Svenja Heise ◽  
Michael Höhlinger ◽  
Yadir Torres Hernández ◽  
Juan José Pavón Palacio ◽  
Jose Antonio Rodriquez Ortiz ◽  
...  

2015 ◽  
Vol 654 ◽  
pp. 165-169 ◽  
Author(s):  
Marta Miola ◽  
Enrica Verné ◽  
Antonella Piredda ◽  
Sigrid Seuss ◽  
Sandra Cabanas-Polo ◽  
...  

Three different glasses were synthesized by doping 45S5 bioactive glass with B2O3. The bioactivity of the glasses was evaluated by immersion in simulated body fluid (SBF) up to 3 days; all glasses showed the precipitation of hydroxyapatite (HAp) after one day of soaking in SBF. Electrophoretic deposition (EPD) was used to prepare PEEK/B2O3-doped 45S5 glass composite coatings on stainless steel substrates. The coatings were characterized by means of tape test (ASTM D3359-B), scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR), contact angle measurements, thermogravimetric analysis and in vitro bioactivity test. All composite coatings exhibited a porous and homogenous structure with a hydrophobic surface, according to the wettability test. The in vitro test in SBF demonstrated that the coatings were highly bioactive.


2010 ◽  
Vol 36 (1) ◽  
pp. 307-312 ◽  
Author(s):  
M. Charlotte Schausten ◽  
Decheng Meng ◽  
Rainer Telle ◽  
Aldo R. Boccaccini

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