A rapid gas chromatographic method for the quantitation of volatile fatty acids in urine

1973 ◽  
Vol 81 (1) ◽  
pp. 65-69 ◽  
Author(s):  
B.F. Gibbs ◽  
K. Itiaba ◽  
J.C. Crawhall ◽  
B.A. Cooper ◽  
O.A. Mamer
1965 ◽  
Vol 48 (2) ◽  
pp. 433-437
Author(s):  
G R Higginbotham

Abstract The microcoulometric gas chromatographic method for detection of chick edema factor in fats and fatty acids was suhjected to a second collaborative study. Results were satisfactory, and it is recommended that the method be adopted as official, first action.


2011 ◽  
Vol 51 (No. 5) ◽  
pp. 181-188 ◽  
Author(s):  
M. Pešek ◽  
E. Samková ◽  
J. Špička

In 2003, 2004 and 2005 milk fat composition was determined three times in 55 dairy cows of Czech Pied cattle housed in a byre with stanchions and fed under conditions usual on Czech production farms. Fatty acids were determined by a gas chromatographic method, 26 acids out of the total 37 acids observed in chromatograms were identified. The highest proportions were observed for palmitic acid (29.25 ± 2.98%), oleic acid (24.47 ± 3.27%), myristic acid (12.14 ± 1.80%) and stearic acid (8.91 ± 2.44%). The proportions of saturated, unsaturated and monounsaturated fatty acids were 64.71 ± 4.18, 31.96 ± 4.20 and 27.45 ± 3.42% of total acids, respectively. The total proportion of nutritionally undesirable lauric, myristic and palmitic acid was 45.26 ± 4.77%, while that of the desirable group of polyunsaturated fatty acids was 4.51 ± 1.09%. The observed relatively wide ranges of the individual groups of fatty acids indicate that it is possible to improve the milk fat composition in Czech Pied cows.  


2004 ◽  
Vol 524 (1-2) ◽  
pp. 191-200 ◽  
Author(s):  
A. Sanches-Silva ◽  
J. López-Hernández ◽  
P. Paseiro-Losada ◽  
J. Simal-Lozano

1988 ◽  
Vol 25 (2) ◽  
pp. 87-90 ◽  
Author(s):  
M. C. Martin-Hernández ◽  
L. Alonso ◽  
M. Juárez ◽  
J. Fontecha

Author(s):  
Mirela JIMBOREAN ◽  
Dorin Å¢IBULCÄ‚ ◽  
Adriana PÄ‚UCEAN ◽  
Claudiu Dan S Ä‚LÄ‚GEAN

The transformations of cheese components during ripening, especially the evolution of free fatty acids were studied using the gas-chromatographic method. The proteolitic and lypolitic enzymes were added in semi-hard cheese assortment for cheese quality improvment. Three types of semi-hard cheese were taken into study: blank (M), cheese with lypolitic enzymes (Bl) and cheese with proteolytic enzymes (Bp). Samples from these cheeses were collected at three different moment of times: at obtaining, at 25 day of ripening and at 50 day of ripening. The content of saturated fatty acids (SFA), monounsaturated fatty acids (MUFA) and polyunsaturated fatty acids (PUFA) was determined for each sample.


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