Absolute inner-shell cross section determination for EELS analysis

Author(s):  
P.A. Crozier

Absolute inelastic scattering cross sections or mean free paths are often used in EELS analysis for determining elemental concentrations and specimen thickness. In most instances, theoretical values must be used because there have been few attempts to determine experimental scattering cross sections from solids under the conditions of interest to electron microscopist. In addition to providing data for spectral quantitation, absolute cross section measurements yields useful information on many of the approximations which are frequently involved in EELS analysis procedures. In this paper, experimental cross sections are presented for some inner-shell edges of Al, Cu, Ag and Au.Uniform thin films of the previously mentioned materials were prepared by vacuum evaporation onto microscope cover slips. The cover slips were weighed before and after evaporation to determine the mass thickness of the films. The estimated error in this method of determining mass thickness was ±7 x 107g/cm2. The films were floated off in water and mounted on Cu grids.

1988 ◽  
Vol 128 ◽  
Author(s):  
N. R. Parikh ◽  
Z. H. Zhang ◽  
M. L. Swanson ◽  
N. Yu ◽  
W. K. Chu

ABSTRACTElastic scattering of protons with energies from 1.5 MeV to 2 MeV was used to determine the concentration of oxygen in Y-Ba-Cu-O compound, nitrogen in GaN films, and boron in B-Si glass and other materials. Proton scattering from light elements in this energy range exhibits non-Rutherford scattering cross section, which are enhanced by a factor of 3 to 6 or more relative to the Rutherford scattering cross sections. Thus the sensitivity for the light clement detection is considerably larger than that obtained by He ion scattering.Quantitative analysis by proton scattering is discussed and compared with other methods.


2011 ◽  
Vol 10 (3) ◽  
pp. 672-694
Author(s):  
Lorella Fatone ◽  
Maria Cristina Recchioni ◽  
Francesco Zirilli

AbstractAcoustic scattering cross sections of smart furtive obstacles are studied and discussed. A smart furtive obstacle is an obstacle that, when hit by an incoming field, avoids detection through the use of a pressure current acting on its boundary. A highly parallelizable algorithm for computing the acoustic scattering cross section of smart obstacles is developed. As a case study, this algorithm is applied to the (acoustic) scattering cross section of a “smart” (furtive) simplified version of the NASA space shuttle when hit by incoming time-harmonic plane waves, the wavelengths of which are small compared to the characteristic dimensions of the shuttle. The solution to this numerically challenging scattering problem requires the solution of systems of linear equations with many unknowns and equations. Due to the sparsity of these systems of equations, they can be stored and solved using affordable computing resources. A cross section analysis of the simplified NASA space shuttle highlights three findings: i) the smart furtive obstacle reduces the magnitude of its cross section compared to the cross section of a corresponding “passive” obstacle; ii) several wave propagation directions fail to satisfactorily respond to the smart strategy of the obstacle; iii) satisfactory furtive effects along all directions may only be obtained by using a pressure current of considerable magnitude. Numerical experiments and virtual reality applications can be found at the website: http://www.ceri.uniromal.it/ceri/zirilli/w7.


2020 ◽  
Vol 239 ◽  
pp. 14007
Author(s):  
Vaibhav Jaiswal ◽  
Luiz Leal ◽  
Alexander I. Kolesnikov

Thermal neutron scattering cross-section data for light water available in the major nuclear data libraries observes significant differences especially at reactor operating temperatures. During the past few years there has been a renewed interest in reviewing the existing thermal scattering models and generating more accurate and reliable thermal scattering cross sections using existing experimental data and in some cases based on Molecular Dynamics (MD) simulations. There is a need for performing new time-of-flight experiments at high temperatures and pressures, to have a better understanding of the physics involved in the scattering process that could help improve the existing TSL data. Lack of experimental thermal scattering data for light water at high temperatures led to a new measurement campaign within the INSIDER project at the Institut de radioprotection et de sûreté nucléaire (IRSN). Double differential scattering cross section for light water have been measured at the SEQUOIA spectrometer based at the Spallation Neutron Source (SNS), Oak Ridge National Laboratory, United States. Several measurements have been carried out at different temperatures and pressures corresponding to liquid light water. Measurements at five different incident neutron energies Ei (8, 60, 160, 280 and 800 meV) have been carried out to help exploring different regions of the frequency spectrum. This paper presents the analysis of the dynamic structure factor and the derived frequency spectrum of light water. The analysis of the experimental data would provide one with better confidence, the behavior of thermal scattering cross sections for light water at high temperatures, knowledge of which is very important for the design of novel reactors as well as existing pressurized water reactors.


1968 ◽  
Vol 46 (24) ◽  
pp. 2755-2763 ◽  
Author(s):  
Chin-Lin Chen

The problem of the scattering of a plane wave by a long, thin, perfectly conducting wire is studied. The scatterer is loaded at its center by a lumped element. The effects of the loading on the scattering of waves are investigated. Numerical results are obtained for the case of normal incidence. The results show that for relatively short wires, the back-scattering cross sections may be modified effectively by central loading, while for longer wires, the modification is rather difficult to achieve. To nullify the back-scattering cross section completely, it is necessary to use active loading if kh > 3.6. A physical explanation is also presented.


2019 ◽  
Vol 73 (12) ◽  
Author(s):  
Lilian Ellis-Gibbings ◽  
Francisco Blanco ◽  
Gustavo García

Abstract Positron scattering cross sections, used for modelling particle transport in various media, are difficult to gather experimentally. As such, various cross section calculation methods have been developed to varying accuracy. The IAM-SCAR+I method has been improved upon recently to fulfil the optical theorem and the results for two important simple molecules, N2 and O2, are presented here. These results are compared to literature and our findings are comparable in most impact energy ranges. Graphical abstract


1982 ◽  
Vol 60 (5) ◽  
pp. 632-635 ◽  
Author(s):  
P. Gabriel ◽  
J. M. Robson

The sum of the absorption, incoherent, and thermal inelastic scattering cross sections of natural titanium has been measured at 293 K for three neutron velocities in the range 6–8 m/s. They agree with values to be expected on the basis of an inverse velocity extrapolation from measurements near thermal neutron velocities.


1995 ◽  
Vol 04 (01) ◽  
pp. 163-179
Author(s):  
S.L. MINTZ ◽  
M. POURKAVIANI

The unpolarized and parity violating polarized inclusive inelastic electron scattering cross-sections are calculated for incident electrons from threshold to 100 MeV, for the 12C nucleus. The relationship between these cross-sections and the inclusive neutrino cross-section on this same nucleus is discussed. The possibility of using the parity violating polarized electron scattering interaction to obtain the average nuclear excitation is also discussed.


2015 ◽  
Vol 11 (A29B) ◽  
pp. 739-739
Author(s):  
Allan D Ernest ◽  
Matthew P. Collins

AbstractWe show that as equilibrium is approached in deep gravity wells, such as those of galactic halos, gravitational quantum theory predicts that radial particle densities ρ(r) tend toward 1/r2 profiles, and photon-baryon scattering cross sections are significantly reduced.


Open Physics ◽  
2012 ◽  
Vol 10 (4) ◽  
Author(s):  
Igor Sharf ◽  
Andrii Tykhonov ◽  
Grygorii Sokhrannyi ◽  
Maksym Deliyergiyev ◽  
Natalia Podolyan ◽  
...  

AbstractWe demonstrate a new method to calculate inelastic scattering cross-sections, which in contrary to the Regge-based methods takes into account the energy momentum conservation law. It is shown that the main contribution to integral expressing inelastic scattering cross-sections does not come from the multi-Regge domain. In particular, accounting for the longitudinal momenta contribution to virtualities is sufficient and results in the new mechanism of cross-section growth. The reasons for taking into account the sufficiently high number of interference contributions are shown and the approximate method for this purpose is developed. By fitting single free parameter of the model achieved a qualitative agreement of the total and inelastic cross sections with experimental data.


2021 ◽  
Vol 247 ◽  
pp. 15010
Author(s):  
D. Kent Parsons ◽  
Scott A. Turner ◽  
Peter J. Jaegers

With the recent release of ENDF/B VIII.0 data, additional covariance data was provided for many isotopes, including O16. The detail of elastic scattering and mubar covariance data for O16 increased dramatically between ENDF/B VII.1 and ENDF/B VIII.0. This new covariance data has been processed with NJOY2016 and investigation has begun on the effects of these new uncertainty data. The uncertainties are applied to multi-group scattering cross sections and P1 Legendre components in deterministic neutron transport. A simple but typical application of shielding fission neutrons with concrete has been used to assess the practical effects of the new covariance data for O16. A somewhat surprising result is that the mubar uncertainty can have a significant effect on the calculated shielding and criticality results.


Sign in / Sign up

Export Citation Format

Share Document