Strain analysis with nanometer resolution using a conventional transmission electron microsopy technique: electron diffraction contrast imaging revisited

Author(s):  
Koenraad G F Janssens ◽  
Omer Van der Biest ◽  
Jan Vanhellemont ◽  
Herman E Maes ◽  
Robert Hull

There is a growing need for elastic strain characterization techniques with submicrometer resolution in several engineering technologies. In advanced material science and engineering the quantitative knowledge of elastic strain, e.g. at small particles or fibers in reinforced composite materials, can lead to a better understanding of the underlying physical mechanisms and thus to an optimization of material production processes. In advanced semiconductor processing and technology, the current size of micro-electronic devices requires an increasing effort in the analysis and characterization of localized strain. More than 30 years have passed since electron diffraction contrast imaging (EDCI) was used for the first time to analyse the local strain field in and around small coherent precipitates1. In later stages the same technique was used to identify straight dislocations by simulating the EDCI contrast resulting from the strain field of a dislocation and comparing it with experimental observations. Since then the technique was developed further by a small number of researchers, most of whom programmed their own dedicated algorithms to solve the problem of EDCI image simulation for the particular problem they were studying at the time.

1995 ◽  
Vol 405 ◽  
Author(s):  
J. Vanhellemont ◽  
K. G. F. Janssens ◽  
S. Frabboni ◽  
P. Smeys ◽  
R. Balboni ◽  
...  

AbstractAn overview is given of transmission electron microscopy techniques to address strain with nm scale spatial resolution. In particular the possibilities and limitations of (large angle) convergent beam electron diffraction ((LA)CBED) and electron diffraction contrast imaging (EDCI) techniques are discussed in detail. It will be shown by a few case studies that unique and quantitative information on local strain distributions can be obtained by the combined use of both (LA)CBED and EDCI in correlation with three dimensional finite element simulations of the strain distributions in the thinned specimen.


1995 ◽  
Vol 406 ◽  
Author(s):  
J. Vanhellemont ◽  
K. G. F. Janssens ◽  
S. Frabboni ◽  
P. Smeys ◽  
R. Balboni ◽  
...  

AbstractAn overview is given of transmission electron microscopy techniques to address strain with nm scale spatial resolution. In particular the possibilities and limitations of (large angle) convergent beam electron diffraction ((LA)CBED) and electron diffraction contrast imaging (EDCI) techniques are discussed in detail. It will be shown by a few case studies that unique and quantitative information on local strain distributions can be obtained by the combined use of both (LA)CBED and EDCI in correlation with three dimensional finite element simulations of the strain distributions in the thinned specimen.


2013 ◽  
Vol 1510 ◽  
Author(s):  
Takanori Kiguchi ◽  
Yusuke Hoshi ◽  
Takeshi Tayagaki ◽  
Noritaka Usami

AbstractThe local strain field and the intermixing of a Ge nano-islands (NIs)/Si spacer stacked structure in a novel solar cell with a p-i-n type Si single crystal with two-dimensional photonic nanocrystals connecting to the vertically aligned NIs were analyzed using electron microscopy. High-angle annular dark field-scanning transmission electron microscope (HAADF-STEM) images show intermixing between Ge and Si clearly and reveal that the surface segregation of Ge becomes advanced. The average composition of the NIs is Ge0.42Si0.58, which is almost constant in a row of vertically aligned NIs. The local strain analysis results obtained from the high-resolution transmission electron microscope (HRTEM) images show that the strain state is partially relaxed after the elastic relaxation of NIs.


1997 ◽  
Vol 69 (3) ◽  
pp. 151-167 ◽  
Author(s):  
Koenraad G.F. Janssens ◽  
Omer Van der Biest ◽  
Jan Vanhellemont ◽  
Herman E. Maes

1996 ◽  
Vol 86 (2-3) ◽  
pp. 191-191
Author(s):  
Bruce SHILLITO ◽  
Jean-Pierre LECHAIRE ◽  
Franc¸oise GAILL

1993 ◽  
Vol 8 (2) ◽  
pp. 286-290 ◽  
Author(s):  
Yanfa Yan ◽  
Renhui Wang

The electron diffraction contrast of two types of rectangular dislocation networks in an Al70Co15Ni15 decagonal quasicrystal has been analyzed. One type of dislocation network consists of two dislocation sets whose Burgers vectors are parallel to the tenfold axis A10 and a twofold axis A2D. The other type of dislocation network consists of two dislocation sets whose Burgers vectors are parallel to the A10 and the other twofold axis of A2P. The characteristics of the diffraction contrast of the dislocation networks in the Al–Co–Ni decagonal phase are similar to those in conventional crystals.


Author(s):  
Charles F. Tufts

In order to make a critical study of the crystallography in tungsten wires by transmission electron diffraction contrast microscopy, thin sections should be prepared without pressing the wire into ribbon or without using mechanical polishing procedures which can modify the crystallographic character. This paper describes a method that employs electrolytic and chemical polishing to form thin sections in tungsten wires of 0.010 inch diameter.


Author(s):  
Henri CHANZY ◽  
Francoise Gaill ◽  
Marie-Madeleine Giraud-Guille ◽  
Jan Persson ◽  
Junji Sugiyama ◽  
...  

Chitin the poly β (1-4)-N Acetyl D glucosamine is widespread in nature and occurs normally as a crystalline fibrillar substance. As opposed to most of the crystalline polysaccharides, chitin is quite resistant to the electron beam. In particular, at room temperature, accumulated doses as high as 200 elec/nm2 at 120 kV can be used to record successful images showing crystalline details. For this reason, chitin can be studied without too much difficulty by electron diffraction (ED), diffraction contrast transmission electron microscopy (DCTEM) and lattice imaging. This study presents some of the diversity of chitin morphology.Several chitin rich specimens were studied. They include : 1) cross sections of an ovipositor from an ichneumon fly Rhyssa persuosaria ; 2) cross sections of fragments of demineralized crab cuticle ; 3) cross sections of a tube from the vestimentiferan worm Tevnia jerichonana ; 4) bundles of chitin microfibrils isolated from Tevnia tube fragments after deproteinization.


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