Structural determination of oligosaccharides derived from lipooligosaccharide of Neisseria gonorrhoeae F62 by chemical, enzymic, and two-dimensional NMR methods

Biochemistry ◽  
1991 ◽  
Vol 30 (43) ◽  
pp. 10566-10575 ◽  
Author(s):  
Ryohei Yamasaki ◽  
Bradley E. Bacon ◽  
Wade Nasholds ◽  
Herman Schneider ◽  
J. M. Griffiss
Keyword(s):  
Neisseria Gonorrhoeae ◽  
Structural Determination ◽  
Two Dimensional ◽  
Nmr Methods

Structural determination of oligosaccharides derived from lipooligosaccharide of Neisseria gonorrhoeae F62 by chemical, enzymic, and two-dimensional NMR methods [Erratum to document cited in CA115(21):229924v]

Biochemistry ◽  
1992 ◽  
Vol 31 (1) ◽  
pp. 316-316
Author(s):  
Ryohei Yamasaki ◽  
Bradley E. Bacon ◽  
Wade Nasholds ◽  
Herman Schneider ◽  
J. M. Griffiss
Keyword(s):  
Neisseria Gonorrhoeae ◽  
Structural Determination ◽  
Two Dimensional ◽  
Nmr Methods

Structural determination of the capsular polysaccharide of Neisseria meningitidis group I: a two-dimensional NMR analysis

Biochemistry ◽  
1985 ◽  
Vol 24 (20) ◽  
pp. 5592-5598 ◽  
Author(s):  
Francis Michon ◽  
Jean Robert Brisson ◽  
Rene Roy ◽  
Fraser E. Ashton ◽  
Harold J. Jennings
Keyword(s):  
Neisseria Meningitidis ◽  
Capsular Polysaccharide ◽  
Structural Determination ◽  
Two Dimensional ◽  
Nmr Analysis ◽  
Group I

ChemInform Abstract: SYNTHESIS AND STRUCTURAL DETERMINATION OF A NEW TWO-DIMENSIONAL COMPOUND: P2NB4S21

1983 ◽  
Vol 14 (34) ◽  
Author(s):  
R. BREC ◽  
M. EVAIN ◽  
P. GRENOUILLEAU ◽  
J. ROUXEL
Keyword(s):  
Structural Determination ◽  
Two Dimensional

Structural determination of geometrical isomers of microcystins LR and RR from cyanobacteria by two-dimensional NMR spectroscopic techniques

1990 ◽  
Vol 3 (5) ◽  
pp. 473-481 ◽  
Author(s):  
Kenichi Harada ◽  
Kiyoshi Ogawa ◽  
Kenji Matsuura ◽  
Hideaki Murata ◽  
Makoto Suzuki ◽  
...  
Keyword(s):  
Spectroscopic Techniques ◽  
Structural Determination ◽  
Two Dimensional ◽  
Geometrical Isomers

Structural determination of the O-antigenic polysaccharide of enteropathogenicEscherichia coliO103:H2

2010 ◽  
Vol 56 (5) ◽  
pp. 367-372 ◽  
Author(s):  
Evgeny Vinogradov ◽  
Leann L. MacLean ◽  
Malcolm B. Perry
Keyword(s):  
Periodate Oxidation ◽  
Enterohemorrhagic Escherichia Coli ◽  
Structural Determination ◽  
Two Dimensional ◽  
Methylation Analysis ◽  
Polysaccharide Antigen ◽  
Antigenic Polysaccharide ◽  
Oxidation Degradation ◽  
C Nmr

The structure of the antigenic O-polysaccharide isolated from the lipopolysaccharide produced by enterohemorrhagic Escherichia coli O103:H2 was determined and shown to be composed of d-glucose (1 part), 2-acetamido-2-deoxy-d-glucose (2 parts), 2-acetamido-2-deoxy-d-galactose (1 part), and 3-deoxy-3-(R)-3-hydroxybutyramido-d-fucose (1 part). From the results of methylation analysis, Smith-type periodate oxidation degradation studies, and the use of one- and two-dimensional1H and13C NMR spectroscopy, the O-polysaccharide antigen was found to be an unbranched polymer of a repeating pentasaccharide unit having the following structure: →2)-β-d-Glcp-(1→2)-β-d-Fucp3NBu-(1→6)-α-d-GlcpNAc-(1→4)-α-d-GalpNAc-(1→3)-β-d-GlcpNAc-(1→, where Bu is (R)-3-hydroxybutyramido.

scholarly journals STRUCTURAL DETERMINATION OF CYCLOALIPHATIC EPOXY MONOMERS BY TWO-DIMENSIONAL NMR SPECTROSCOPY AND QUANTUM CHEMICAL CALCULATION

1991 ◽  
Vol 7 (Supple) ◽  
pp. 425-428 ◽  
Author(s):  
ATSUSHI UDAGAWA ◽  
YASUHIKO YAMAMOTO ◽  
YOSHIO INOUE ◽  
RIICHIRO CHUJO
Keyword(s):  
Nmr Spectroscopy ◽  
Quantum Chemical Calculation ◽  
Quantum Chemical ◽  
Chemical Calculation ◽  
Structural Determination ◽  
Two Dimensional ◽  
Cycloaliphatic Epoxy

New NMR Methods that Probe the Structure of Glasses

1990 ◽  
Vol 215 ◽  
Author(s):  
Robert Tycko ◽  
Gary Dabbagh
Keyword(s):  
Crystal Structures ◽  
Short Range ◽  
Two Dimensional ◽  
Structure Of Glasses ◽  
Orientational Ordering ◽  
Nmr Methods

AbstractTwo-dimensional NMR methods allow a determination of the relative orientations of nearby molecules in polycrystalline and noncrystalline solids. We describe these methods and present applications to the determination of the crystal structures of two forms of polycrystalline methanol and to the investigation of short range molecular orientational ordering in methanol glass and in atactic PMMA.

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