A new synthetic route to quadruply bonded tungsten-tungsten and molybdenum-tungsten compounds of the type MM'X4(PR3)4, X = Cl or Br. Structural characterization of quadruply bonded WWBr4(.mu.-dppm)2 and MoWBr4(PMe2Ph)4 and phosphorus-31{proton} NMR spectra of these and related compounds

1993 ◽  
Vol 32 (5) ◽  
pp. 681-686 ◽  
Author(s):  
F. A. Cotton ◽  
Judith L. Eglin ◽  
Chris A. James
Keyword(s):  
Structural Characterization ◽  
Nmr Spectra ◽  
Proton Nmr ◽  
Synthetic Route ◽  
Related Compounds

Structural Characterization of Glass from the Inversion of23Na and27Al 3Q-MAS NMR Spectra

1999 ◽  
Vol 103 (47) ◽  
pp. 10356-10364 ◽  
Author(s):  
F. Angeli ◽  
T. Charpentier ◽  
P. Faucon ◽  
J.-C. Petit
Keyword(s):  
Structural Characterization ◽  
Nmr Spectra ◽  
Mas Nmr

A new synthetic route to cyclophosphadithiatriazenes: synthesis and X-ray structural characterization of the first spirocycle containing thiadiazaphosphetidine and phosphadithiatriazene heterocycles

2006 ◽  
Vol 20 (12) ◽  
pp. 880-885 ◽  
Author(s):  
Janarthanan Gopalakrishnan ◽  
Babu Varghese ◽  
Adinarayana Doddi ◽  
M. N. Sudheendra Rao
Keyword(s):  
Structural Characterization ◽  
Synthetic Route ◽  
X Ray

Structural characterization of octahedral metal complexes of [MX3(py)3] type with three pyridines as revealed by 2H NMR spectra

1994 ◽  
Vol 218 (1-2) ◽  
pp. 179-184 ◽  
Author(s):  
Sumio Kaizaki ◽  
J. Ivan Legg
Keyword(s):  
Metal Complexes ◽  
Structural Characterization ◽  
Nmr Spectra ◽  
2H Nmr

Characterization of Novel Aminobenzylcantharidinimides and Related Imides by Proton NMR Spectra and Their Effects on NO Induction

2014 ◽  
Vol 62 (1) ◽  
pp. 59-63 ◽  
Author(s):  
Ing-Jy Tseng ◽  
Pen-Yuan Lin ◽  
Shiow-Yunn Sheu ◽  
Wan-Ni Tung ◽  
Ching-Tung Lin ◽  
...  
Keyword(s):  
Nmr Spectra ◽  
Proton Nmr

Proton NMR studies on bovine cyclophilin: preliminary structural characterization of its complex with cyclosporin A

Biochemistry ◽  
1990 ◽  
Vol 29 (18) ◽  
pp. 4466-4478 ◽  
Author(s):  
S. L. Heald ◽  
M. W. Harding ◽  
R. E. Handschumacher ◽  
I. M. Armitage
Keyword(s):  
Cyclosporin A ◽  
Structural Characterization ◽  
Proton Nmr ◽  
Nmr Studies

Proton NMR structural characterization of a recombinant kringle 2 domain from human tissue-type plasminogen activator

Biochemistry ◽  
1989 ◽  
Vol 28 (24) ◽  
pp. 9350-9360 ◽  
Author(s):  
In Ja L. Byeon ◽  
Robert F. Kelley ◽  
Miguel Llinas
Keyword(s):  
Plasminogen Activator ◽  
Structural Characterization ◽  
Human Tissue ◽  
Proton Nmr ◽  
Tissue Type ◽  
Tissue Type Plasminogen Activator ◽  
Type Plasminogen Activator ◽  
Kringle 2

Sequence-specific proton NMR assignments and structural characterization of bovine seminal fluid protein PDC-109 domain b

Biochemistry ◽  
1991 ◽  
Vol 30 (6) ◽  
pp. 1663-1672 ◽  
Author(s):  
Keith L. Constantine ◽  
Vasudevan Ramesh ◽  
Laszlo Banyai ◽  
Maria Trexler ◽  
Laszlo Patthy ◽  
...  
Keyword(s):  
Structural Characterization ◽  
Nmr Assignments ◽  
Seminal Fluid ◽  
Proton Nmr ◽  
Seminal Fluid Protein

A New Synthetic Route to High-Valent Half-Sandwich Group 4 Metallacarborane Alkyls. Synthesis and Structural Characterization of [η1:η6-(Me2NCH2CH2)C2B10H11]Hf(CH2SiMe3)2

2005 ◽  
Vol 24 (13) ◽  
pp. 3037-3039 ◽  
Author(s):  
Mak-Shuen Cheung ◽  
Hoi-Shan Chan ◽  
Zuowei Xie
Keyword(s):  
Structural Characterization ◽  
Synthetic Route ◽  
Group 4 ◽  
High Valent ◽  
Half Sandwich

Synthesis and characterization of a series of 3-methyl-3-{3-[1-methyl-3-aryl-2-triazenyl]propyl}-1-aryl-1-triazenes and related compounds

2006 ◽  
Vol 84 (6) ◽  
pp. 831-842
Author(s):  
Jeff D Clarke ◽  
Shasta L Moser ◽  
Keith Vaughan
Keyword(s):  
Secondary Amine ◽  
Nmr Spectra ◽  
High Resolution Mass Spectrometry ◽  
Coupling Reaction ◽  
H Nmr ◽  
Methylene Groups ◽  
Related Series ◽  
Diazonium Coupling ◽  
Related Compounds

A series of diazonium salts has been coupled to both secondary nitrogen atoms of the bis-secondary amine, N,N′-dimethyl-1,3-propanediamine (MeNHCH2CH2CH2NHMe), to afford the new bistriazene series, the 3-methyl-3-{3-[1-methyl-3-aryl-2-triazenyl]propyl}-1-aryl-1-triazenes (9). These compounds have been fully characterized by IR and NMR spectroscopy, with supporting data from elemental analysis and high-resolution mass spectrometry. A limited number of model compounds in the N,N-dimethyl-N-{3-[1-methyl-3-aryl-2-triazenyl]propyl}amine series (10) have been synthesized to aid in the interpretation of the NMR spectra of the bistriazenes (9). A series of related compounds, the 3-ethyl-3-{(E)-4-[1-ethyl-3-aryl-2-triazenyl]-2-butenyl}-1-aryl-1-triazenes (11), have been synthesized by diazonium coupling with the bis-secondary amine N,N′-diethyl-2-butene-1,4-diamine (15), and the diazonium coupling reaction with trans-N,N′-dimethycyclohexane-1,2-diamine (19) has been used to prepare another related series of bistriazenes, the 3-methyl-3-{2-[1-methyl-3-aryl-2-triazenyl]cyclohexyl}-1-aryl-1-triazenes (12). The 1H NMR spectra of these compounds are complex because of the presence of two chiral centres in the cyclohexanediamine moiety; the diastereotopic protons of the methylene groups in the cyclohexane ring are clearly distinguished in the 500 MHz spectra of these compounds.Key words: triazene, bistriazene, synthesis, nuclear magnetic resonance, propanediamine, 1,4-diamino-2-butene, cyclohexanediamine.

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