Conformation of platinum-trinucleotide adduct Pt(dien)[d(ApGpA)-N7(2)] in the solid state and in aqueous solution, as determined with single-crystal x-ray diffraction and high-resolution NMR spectroscopy in solution

1992 ◽  
Vol 114 (3) ◽  
pp. 930-938 ◽  
Author(s):  
Gert Admiraal ◽  
Maarten Alink ◽  
Cornelis Altona ◽  
Fransje J. Dijt ◽  
Carla J. Van Garderen ◽  
...  
Keyword(s):  
Aqueous Solution ◽  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Single Crystal ◽  
X Ray Diffraction ◽  
X Ray ◽  
High Resolution Nmr

X-ray diffraction and high resolution NMR spectroscopy analysis of methyl β-d-glucofuranosidurono-6,3-lactone

1998 ◽  
Vol 308 (3-4) ◽  
pp. 431-433 ◽  
Author(s):  
Janusz Madaj ◽  
Anna Trynda ◽  
Antoni Konitz ◽  
Andrzej Nowacki ◽  
Andrzej Wiśniewski
Keyword(s):  
Nmr Spectroscopy ◽  
High Resolution ◽  
X Ray Diffraction ◽  
Spectroscopy Analysis ◽  
X Ray ◽  
High Resolution Nmr

Preparation, single-crystal X-ray diffraction and high-resolution NMR spectroscopic analyses of N-[(1,4-anhydro-5-deoxy-2,3-O-isopropylidene-d,l-ribitol)-5-yl]trimethylammonium iodide

2006 ◽  
Vol 341 (11) ◽  
pp. 1916-1921 ◽  
Author(s):  
Barbara Dmochowska ◽  
Eugenia Skorupa ◽  
Lucyna Pellowska-Januszek ◽  
Monika Czarkowska ◽  
Artur Sikorski ◽  
...  
Keyword(s):  
High Resolution ◽  
Single Crystal ◽  
X Ray Diffraction ◽  
X Ray ◽  
Spectroscopic Analyses ◽  
High Resolution Nmr

scholarly journals Order in disorder: solution and solid-state studies of [MIII2MII5] wheels (MIII = Cr, Al; MII = Ni, Zn)

2018 ◽  
Vol 47 (34) ◽  
pp. 11834-11842 ◽  
Author(s):  
Hector W. L. Fraser ◽  
Gary S. Nichol ◽  
Dušan Uhrín ◽  
Ulla Gro Nielsen ◽  
Marco Evangelisti ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Solid State ◽  
Nmr Spectroscopy ◽  
Single Crystal ◽  
Solid State Nmr ◽  
Squid Magnetometry ◽  
X Ray Diffraction ◽  
X Ray ◽  
Solid State Nmr Spectroscopy ◽  
Esi Mass Spectrometry

Heterometallic species with Anderson-like structures are characterised by single-crystal X-ray diffraction, solution- and solid-state NMR spectroscopy, ESI mass spectrometry and SQUID magnetometry.

Dimeres Di(N-lithium–tert–butylamino)bis(dimethylamino)silan - [Si(N(CH3)2)2(NLiC(CH3)3)2]2 – Darstellung und Kristallstruktur / Dimeric Di(N -lithio-tert-butylamino)bis(dimethylamino)silane - [Si(N(CH3)2)2(NLiC(CH3)3)2]2 – Synthesis und Crystal Structure

2001 ◽  
Vol 56 (1) ◽  
pp. 90-94 ◽  
Author(s):  
Josef Engering ◽  
Eva-Maria Peters ◽  
Martin Jansen
Keyword(s):  
Crystal Structure ◽  
Mass Spectrometry ◽  
Solid State ◽  
Nmr Spectroscopy ◽  
Single Crystal ◽  
Title Compound ◽  
Solution Nmr ◽  
X Ray Diffraction ◽  
X Ray ◽  
Solution Nmr Spectroscopy

Abstract [Si(N(CH3)2)2(NLiC(CH3)3)2]2 results from the reaction of silicon tetrachloride with excess terf-butylamine, followed by halogen substitution with LiN(CH3)2, and treatment with n-butyllithium in hexane. The title compound, found to be dimeric in the solid state, was characterised by single crystal X-ray diffraction (triclinic, Pi , a = 10.208(2), b = 12.140(2), c = 15.658(3) Å , a = 79.02(3), ß = 82.80(3), γ = 67.19(3)°, Z = 2, C24H60Li4N8Si2 ), and by solid state and solution NMR-spectroscopy and mass spectrometry.

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