One-Pot Synthesis of Regular Rhombic Titanium Dioxide Supracolloidal Submicrometer Sheet via Sol–Gel Method

Langmuir ◽  
2013 ◽  
Vol 30 (1) ◽  
pp. 35-40 ◽  
Author(s):  
Ting Huang ◽  
Dong Qiu
2018 ◽  
Vol 479 ◽  
pp. 105-112 ◽  
Author(s):  
Robert E. Przekop ◽  
Piotr Marciniak ◽  
Bogna Sztorch ◽  
Agnieszka Czapik ◽  
Mikołaj Stodolny ◽  
...  

2013 ◽  
Vol 13 (11) ◽  
pp. 7717-7722 ◽  
Author(s):  
Abid Hussain ◽  
Abhijit P. Jadhav ◽  
Yeon Kyung Baek ◽  
Hul Jin Choi ◽  
Jaeho Lee ◽  
...  

2018 ◽  
Vol 226 ◽  
pp. 03014
Author(s):  
Vitaly A. Tarala ◽  
Alexander A. Dolgalev ◽  
Alexander A. Kravtsov ◽  
Irina S. Chikulina ◽  
Boris V. Bukhalov

Within the framework of the study, TiO2 coatings were obtained by sol-gel method via dip-coating. For the films obtaining, manual drawing the substrate from the solution at a relatively high rate of 30 mm / min and automated drawing from the solution at low drawing rates (from 1 to 10 mm / min) were used. The morphology of coatings has been studied by scanning electron microscopy. The influence of the mode and the rate of drawing of the substrate from the solution on the films morphology was demonstrated. Analysis of the data showed, that the surface morphology of the coatings obtained at lower drawing rates by an automated method is much more homogeneous - the titanium dioxide films completely repeats the topography of the substrate surface, there are practically no fissures. Qualitative coatings of titanium dioxide, completely replicating the surface relief of the substrate, can be obtained by this method. Selection of the substrate drawing rate allows reducing the influence of the substrate topography and avoiding the appearance of crystallization centers, and as a consequence, the appearance of defects in the morphology of coatings, such as fissures or microparticles.


2018 ◽  
Vol 5 (1) ◽  
pp. 49-58 ◽  
Author(s):  
Yu.S. Demidova ◽  
I.L. Simakova ◽  
E.V. Suslov ◽  
K.P. Volcho ◽  
N.F. Salakhutdinov ◽  
...  

Abstract In the current work gold catalysts supported on both commercial oxides and oxides synthesized by the sol-gel method were used for the one-pot alcohol amination of myrtenol. In general, utilization of metal oxides synthesized by the sol-gel method as the gold catalyst support enhanced the knowledge regarding key parameters determining catalytic behavior. Synthesized alumina was characterized by stronger acid sites favoring primary amine accumulation on the catalyst surface, as compared to the commercial oxide. Utilization of mixed metal oxides synthesized by the sol-gel method resulted in the non-additive behavior of different oxides enhancing the catalytic activity. Introduction of ceria into alumina modified the support basicity resulting in more efficient alcohol activation.


2011 ◽  
Vol 58 (2) ◽  
pp. 535-538 ◽  
Author(s):  
Marauo Davis ◽  
Cenk Gümeci ◽  
Courtney Kiel ◽  
Louisa J. Hope-Weeks

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