Computed crystal structure images for high resolution electron microscopy

Nature ◽  
1978 ◽  
Vol 274 (5669) ◽  
pp. 322-324 ◽  
Author(s):  
M. A. O'Keefe ◽  
P. R. Buseck ◽  
S. Iijima
2013 ◽  
Vol 456 ◽  
pp. 533-536
Author(s):  
Yan Zhi Lou

In this paper, high resolution electron microscopy (HREM) was used to observe nanosized Fe2M precipitates in M50NiL steel, and crystal structure of which was also investigated by selected area electron diffraction (SAED). At the same time, the orientation relationship between the Fe2M and the martensite matrix was also studied. The results suggested that crystal structure of Fe2M is close-packed hexagonal, and lattice parameters about a=b=0.473nm, c=0.772nm, α=β=90°, γ=120°. The orientation relationship between the nanoprecipitates Fe2M and martensite is and .


2009 ◽  
Vol 1184 ◽  
Author(s):  
Fanghua Li ◽  
Chunyan Tang

AbstractImage deconvolution is introduced as an effective tool to enhance the determination of crystal structures and defects in high-resolution electron microscopy. The essence is to transform a single image that does not intuitively represent the examined crystal structure into the structure image. The principle and method of image deconvolution together with the related image contrast theory, the pseudo weak phase object approximation (pseudo WPOA), are briefly described. The method has been applied to different types of dislocations, twin boundaries, stacking faults, and one-dimensional incommensurate modulated structures. Results on the semiconducting epilayers Si0.76Ge0.24/Si and 3C-SiC/Si are given in some detail. The results on other compounds including AlSb/GaAs, GaN, Y0.6Na0.4Ba2Cu2.7Zn0.3O7-δ, Ca0.28Ba0.72Nb2O6 and Bi2.31Sr1.69CuO6+δ are briefly summarized. It is also shown how to recognize atoms of Si from C based on the pseudo WPOA, when the defect structures in SiC was determined at the atomic level with a 200 kV LaB6 microscope.


1988 ◽  
Vol 38 (16) ◽  
pp. 11952-11954 ◽  
Author(s):  
H. Ihara ◽  
R. Sugise ◽  
K. Hayashi ◽  
N. Terada ◽  
M. Jo ◽  
...  

2007 ◽  
Vol 46 (2) ◽  
pp. 712-715 ◽  
Author(s):  
Kunio Yubuta ◽  
Yuh-ki Hasegawa ◽  
Yuzuru Miyazaki ◽  
Tsuyoshi Kajitani

1977 ◽  
Vol 30 (6) ◽  
pp. 1195 ◽  
Author(s):  
AN Bagshaw ◽  
BH Doran ◽  
AH White ◽  
AC Willis

The crystal structure of a mineral with the stoichiometry (K0.58Ba0.36)2(Ti0.93FeIII0.06)6O13 has been determined by X-ray diffraction and refined by full-matrix least squares to a residual of 0.076 for 1688 ?observed? reflections. Crystals are monoclinic, C2/m, a = 15.453(2), b = 3.8368(7), c = 9.123(2) Ǻ,β = 99.25(1)�, Z = 2, and are isostructural with the (Na,K,Rb)2Ti6O13 family. High-resolution electron microscopy has confirmed that the Ba and FeIII species (the latter in a high-spin state) are randomly substituted for K and Ti respectively.


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