Crystal structure of the self condensation product of (3R,4R)-3,4-dihydroxyhexane-2,5-dione

Author(s):  
Mark A. Briggs ◽  
Alan H. Haines ◽  
Trevor J. King
Structure ◽  
2010 ◽  
Vol 18 (1) ◽  
pp. 138-147 ◽  
Author(s):  
Eri Sakata ◽  
Tadashi Satoh ◽  
Shunsuke Yamamoto ◽  
Yoshiki Yamaguchi ◽  
Maho Yagi-Utsumi ◽  
...  

CrystEngComm ◽  
2021 ◽  
Author(s):  
Jarosław Chojnacki ◽  
Michał Mońka ◽  
Illia E. Serdiuk ◽  
Piotr Bojarski ◽  
Tadeusz Połoński ◽  
...  

The influence of ligand chirality on the self-assembly and spectroscopic properties of copper(i) halide coordination polymers was investigated.


Crystals ◽  
2020 ◽  
Vol 10 (4) ◽  
pp. 269 ◽  
Author(s):  
Rosita Diana ◽  
Ugo Caruso ◽  
Luigi Di Costanzo ◽  
Gelsomina Bakayoko ◽  
Barbara Panunzi

We developed a new benzodifuran derivative as the condensation product between 2,6-diamino-4-(4-nitrophenyl)benzo[1,2-b:4,5-b’]difuran-3,7-dicarboxylate and 3-hydroxy-2-naphthaldehyde. The intramolecular hydrogen-bond interactions in the terminal half-salen moieties produce a sterically encumbered highly conjugated main plane and a D-A-D (donor-acceptor-donor) T-shaped structure. The novel AIEgen (aggregation-induced enhanced emission generator) fulfils the requirement of RIR (restriction of intramolecular rotation) molecules. DR/NIR (deep red/near infrared) emission was recorded in solution and in the solid state, with a noteworthy photoluminescence quantum yield recorded on the neat crystals which undergo some mechanochromism. The crystal structure study of the probe from data collected at a synchrotron X-ray source shows a main aromatic plane π-stacked in a columnar arrangement.


1968 ◽  
Vol 16 (9) ◽  
pp. 1835-1837 ◽  
Author(s):  
TETSUZO KATO ◽  
HIROSHI YAMANAKA ◽  
JUNSHI KAWAMATA ◽  
TETSUICHI SHIBATA

2008 ◽  
Vol 63 (3) ◽  
pp. 345-348 ◽  
Author(s):  
Artem A. Babaryk ◽  
Igor V. Zatovsky ◽  
Nikolay S. Slobodyanik ◽  
Ivan V. Ogorodnyk

A new complex phosphate K1.84Fe1.42Nb0.58(PO4)3 has been synthesized by the self-flux technique. The X-ray single crystal structure and magnetic properties were studied. The compound crystallizes in the cubic system with space group P213 (a = 9.9404(10) Å ) and belongs to the langbeinite structure type. The structure contains [M2P3O18] building units. “Closed” fragments [M8P9O60] provide space for location of two potassium atoms. Antiferromagnetic interactions were detected at low temperatures which originate from superexchange through a M(1)-O-P-O-M(2) pathway with corresponding J = −5.5(1) cm−1. The relationship between the UV/vis absorption and the structure is discussed.


2005 ◽  
Vol 175 (2) ◽  
pp. 977-984 ◽  
Author(s):  
Barbara Giabbai ◽  
Stèphane Sidobre ◽  
M. D. Max Crispin ◽  
Yovan Sanchez-Ruìz ◽  
Angela Bachi ◽  
...  

1990 ◽  
Vol 68 (1) ◽  
pp. 69-73 ◽  
Author(s):  
Wolfgang Kliegel ◽  
Mahmood Tajerbashi ◽  
Steven J. Rettig ◽  
James Trotter

Reaction of oxybis(diphenylborane) with the condensation product of salicylohydroxamic acid and cyclopentanone gives the title compound in good yield. Crystals of 2,2-diphenyl-4,4-tetramethylene-1,3,5-trioxa-3a-azonia-2-borata-2,3,4,5-tetrahydro-1H-cyclopenta[a]naphthalene are monoclinic, a = 12.521(1), b = 12.409(1), c = 12.975(1) Å, β = 93.784(8)°, Z = 4, space group P21/n. The structure was solved by direct methods and was refined by full-matrix least-squares procedures to R = 0.043 and Rw = 0.044 for 1502 reflections with I ≥ 2σ(I). The molecule has a typical diphenylboron hydroxamate structure featuring a five-membered COBON chelate ring. The O,O-chelating ligand is weakly bound to the diphenylboron moiety. Bond lengths (corrected for libration) include: (N)O—B = 1.558(4), (C=)O—B = 1.578(4), and C—B = 1.589(5) and 1.603(5) Å. Keywords: crystal structure, boron compound, organoboron compound.


Author(s):  
Karl Peters ◽  
Eva-Maria Peters ◽  
Hans Georg von Schnering ◽  
Gerhard Bringmann ◽  
Christiana Hesselmann ◽  
...  

AbstractThe title compound is the condensation product of the aminoacid


Author(s):  
M. G. Derebe ◽  
N. Retta ◽  
A. G. G. Moliterni ◽  
F. Capitelli

AbstractDiaquabis(diketohydrindene-diketohydrindamine)manganese(II), Mn(II) complex of Ruhemann's purple, a condensation product of ninhydrin and


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