Synthesis and physicochemical properties of graphene/ZrO2 composite aerogels

RSC Advances ◽  
2015 ◽  
Vol 5 (16) ◽  
pp. 11738-11744 ◽  
Author(s):  
Dongman Guo ◽  
Yun Lu ◽  
Yibo Zhao ◽  
Xuetong Zhang

Graphene/ZrO2 composite aerogels with large BET areas have been synthesized using a sol–gel method together with a supercritical fluid drying process.

2008 ◽  
Vol 368-372 ◽  
pp. 617-619 ◽  
Author(s):  
Yu Zhang ◽  
Jian Xin Cao ◽  
Deng Pan Nie ◽  
Fei Liu ◽  
Yong Gang Dong

Iron oxide nanometer powders were prepared by using sol-gel method and the supercritical fluid drying technology (SCFD) from inorganic salts. The characteristics of the iron oxide nanometer powders were characterized systematically. The results showed that the drying and crystallization of the production could be achieved in one step by SCFD method; furthermore, a highly dispersed, size uniformed and with better crystallization magnetite (Fe3O4) nanoparticles can be obtained. Phase transformation of the as-synthesized powders occurs at about 80°C, and only hematite (α-Fe2O3) can be obtained when being heated at temperatures higher than 400°C. The production synthesized by SCFD exhibits significant magnetic properties. As the heat-treated temperature increase, the magnetic properties of the sample decrease gradually.


2017 ◽  
Vol 91 (8) ◽  
pp. 1486-1492 ◽  
Author(s):  
A. I. Ivanets ◽  
V. G. Prozorovich ◽  
E. F. Krivoshapkina ◽  
T. F. Kuznetsova ◽  
P. V. Krivoshapkin ◽  
...  

Ionics ◽  
2008 ◽  
Vol 15 (2) ◽  
pp. 177-182 ◽  
Author(s):  
Ting-Feng Yi ◽  
Yan-Rong Zhu ◽  
Rong-Sun Zhu ◽  
Li Zhou ◽  
Peng Li ◽  
...  

2006 ◽  
Vol 32 (4) ◽  
pp. 460-470 ◽  
Author(s):  
I. V. Smirnova ◽  
O. A. Shilova ◽  
V. A. Moshnikov ◽  
M. F. Panov ◽  
V. V. Shevchenko ◽  
...  

2017 ◽  
Vol 13 (4) ◽  
pp. 690-692
Author(s):  
Nur Izzati Abu Bakar ◽  
Sheela Chandren ◽  
Nursyafreena Attan ◽  
Leaw Wai Loon ◽  
Hadi Nur

This paper describes the approach by using a magnetic field as a technique in order to synthesize well-aligned materials. The magnetic field technique could be a potential method because it has advantage that all of the materials could be aligned by magnetic field as long as they have magnetic anisotropy. The aim of this research is to explore the effects of magnetic field and magnetic line in the synthesis of well-aligned material, namely titania (TiO2).  The synthesis of well-aligned titania with liquid crystal as the structure-aligning agent is demonstrated under magnetic field in the presence of liquid crystal, 4′-pentyl-4-biphenylcarbonitrile (5CB), tetra-n-butyl orthotitanate (TBOT), 2-propanol and water. The mixture underwent slow hydrolysis and drying process under magnetic field (0.3 T) in ambient condition. The use of magnetic field and 5CB liquid crystal as the structure aligning agent has led to the successful formation of well-aligned TiO2-5CB via sol-gel method. When no magnetic field was applied, the TiO2-5CB obtained was spherical in shape and no alignment can be observed. This study demonstrated that magnetic field can play an important role in the synthesis of well-aligned TiO2-5CB.


RSC Advances ◽  
2019 ◽  
Vol 9 (40) ◽  
pp. 22942-22949 ◽  
Author(s):  
Ya Zhong ◽  
Gaofeng Shao ◽  
Xiaodong Wu ◽  
Yong Kong ◽  
Xue Wang ◽  
...  

Monolithic polymer(resorcinol-formaldehyde) reinforced alumina (RF/Al2O3) aerogel composites were prepared using a sol–gel method and supercritical fluid CO2 drying.


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