Preparation and Characterization of Nanometer Iron Oxide by Sol-Gel Method and Supercritical Fluid Drying Technology

Author(s):  
Yu Zhang ◽  
Jian Xin Cao ◽  
Deng Pan Nie ◽  
Fei Liu ◽  
Yong Gang Dong
2008 ◽  
Vol 368-372 ◽  
pp. 617-619 ◽  
Author(s):  
Yu Zhang ◽  
Jian Xin Cao ◽  
Deng Pan Nie ◽  
Fei Liu ◽  
Yong Gang Dong

Iron oxide nanometer powders were prepared by using sol-gel method and the supercritical fluid drying technology (SCFD) from inorganic salts. The characteristics of the iron oxide nanometer powders were characterized systematically. The results showed that the drying and crystallization of the production could be achieved in one step by SCFD method; furthermore, a highly dispersed, size uniformed and with better crystallization magnetite (Fe3O4) nanoparticles can be obtained. Phase transformation of the as-synthesized powders occurs at about 80°C, and only hematite (α-Fe2O3) can be obtained when being heated at temperatures higher than 400°C. The production synthesized by SCFD exhibits significant magnetic properties. As the heat-treated temperature increase, the magnetic properties of the sample decrease gradually.


RSC Advances ◽  
2015 ◽  
Vol 5 (16) ◽  
pp. 11738-11744 ◽  
Author(s):  
Dongman Guo ◽  
Yun Lu ◽  
Yibo Zhao ◽  
Xuetong Zhang

Graphene/ZrO2 composite aerogels with large BET areas have been synthesized using a sol–gel method together with a supercritical fluid drying process.


2018 ◽  
Vol 09 (04) ◽  
Author(s):  
Rasheed RT ◽  
Al-Algawi SD ◽  
Kareem HH ◽  
Mansoor HS
Keyword(s):  
Sol Gel ◽  

1998 ◽  
Vol 10 (2) ◽  
pp. 495-502 ◽  
Author(s):  
G. Ennas ◽  
A. Musinu ◽  
G. Piccaluga ◽  
D. Zedda ◽  
D. Gatteschi ◽  
...  

1991 ◽  
Vol 26 (2) ◽  
pp. 497-504 ◽  
Author(s):  
N. Takahashi ◽  
N. Kakuta ◽  
A. Ueno ◽  
K. Yamaguchi ◽  
T. Fujii ◽  
...  

ChemInform ◽  
2010 ◽  
Vol 29 (18) ◽  
pp. no-no
Author(s):  
G. ENNAS ◽  
A. MUSINU ◽  
G. PICCALUGA ◽  
D. ZEDDA ◽  
D. GATTESCHI ◽  
...  

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