Controllable synthesis of porous TiO2with a hierarchical nanostructure for efficient photocatalytic hydrogen evolution

2015 ◽  
Vol 3 (7) ◽  
pp. 3710-3718 ◽  
Author(s):  
Lin Wang ◽  
Zhongyuan Nie ◽  
Chuanbao Cao ◽  
Muwei Ji ◽  
Li Zhou ◽  
...  

A one-pot hydrothermal method was used to fabricate porous TiO2hierarchical microspheres with controllable size of nanorods building units, based on controlling the hydrolysis rate of the precursor and the aggregation of surfactant.

2018 ◽  
Vol 6 (7) ◽  
pp. 2895-2899 ◽  
Author(s):  
Shuangshuang Kai ◽  
Baojuan Xi ◽  
Xiaolei Liu ◽  
Lin Ju ◽  
Peng Wang ◽  
...  

An innovative CdS/ZnS-RGO hybrid is synthesizedviaan one-pot hydrothermal method. The further introduction of Au nanoparticles enables the composite with the merits of heterostructured semiconductor/semiconductor junction benefiting the hole transfer, as well as graphene and noble metal favorable for electron transportation.


Author(s):  
Huihui Li ◽  
Fuchun Ning ◽  
Xiaofei Chen ◽  
Anye Shi

Porous carbon nitride nanosheets with carbon and nitrogen double vacancies have been synthesized by soft template-supported one-pot method. Besides a highly defined and unambiguous structure, it also shows minimal thickness...


2011 ◽  
Vol 2011 (35) ◽  
pp. 5384-5389 ◽  
Author(s):  
Ramesh Rajendran ◽  
Rajalakshmi Muralidharan ◽  
Ramya Santhana Gopalakrishnan ◽  
Muthamizhchelvan Chellamuthu ◽  
Suruttaiya U. Ponnusamy ◽  
...  

2018 ◽  
Vol 6 (42) ◽  
pp. 20947-20955 ◽  
Author(s):  
Lulu Wu ◽  
Qiaodan Li ◽  
Chaofan Yang ◽  
Xiaoqing Ma ◽  
Zefan Zhang ◽  
...  

TiO2/γ-graphyne nanocomposites were successfully synthesizedviaa simple hydrothermal method, and demonstrated as a promising photocatalyst for hydrogen evolution.


Nanomaterials ◽  
2019 ◽  
Vol 9 (2) ◽  
pp. 273 ◽  
Author(s):  
Leilei Xu ◽  
Yuwei Ao ◽  
Bin Guan ◽  
Yun Xiang ◽  
Jianguo Guan

Hierarchical nanostructures (HNs) are possibly endowed with novel properties due to their complex three-dimensional (3D) structures. Here, we provide a novel stepwise growth strategy of Coordination Complex Transformation-Assisted Growth for fabricating HNs. By using this, we prepare a new wurtzite ZnS HNs-hollow chestnut-like hierarchical microspheres (HCHMs), which are mesoporous hollow microspheres with single crystalline nanorods arrayed densely and radially from the centre. The HCHMs formation depends on the stepwise decomposition of the two Zn2+ complexes ([Zn(en)m(H2O)2(3−m)]2+ and [Zn(en)m(NH3)2(3−m)]2+, natural number m < 3). As the reaction proceeds, [Zn2+] has been distinctly reduced due to the transformation from [Zn(en)m(H2O)2(3−m)]2+ to [Zn(en)m(NH3)2(3−m)]2+ with a high stability constant, leading to a low crystal growth rate to obtain single crystalline nanorods. Additionally, the generated bubbles (CO2, NH3) acting as a template can induce the generation of hollow structure. The as-prepared ZnS HCHMs show an enhanced photocatalytic hydrogen evolution activity due to the single crystalline wurtzite phase and the high surface area contributed by the hollow hierarchical structures, as well as the mesoporosity. The versatility of the coordination complex transformation-assisted growth strategy will open up new possibilities for fabricating HNs, especially for those transition metal ions with excellent complex capabilities.


2020 ◽  
Vol 8 (26) ◽  
pp. 13299-13310 ◽  
Author(s):  
Cheng-Qun Xu ◽  
Wei-De Zhang ◽  
Kenzo Deguchi ◽  
Shinobu Ohki ◽  
Tadashi Shimizu ◽  
...  

A facile “one-pot” method to improve the utilization of visible light using organic chemistry protocols is reported.


2021 ◽  
Author(s):  
Shengming Xu ◽  
Jing Xu ◽  
Linying Hu ◽  
Ye Liu ◽  
Lijun Ma

In this paper, NiCo2S4 was coated on the surface of WS2 of 1T/2H mixed phase by two step hydrothermal method to form a in-situ core-shell structure. The unique S-Scheme heterojunction...


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