scholarly journals Ball-free mechanochemistry: in situ real-time monitoring of pharmaceutical co-crystal formation by resonant acoustic mixing

2018 ◽  
Vol 54 (32) ◽  
pp. 4033-4036 ◽  
Author(s):  
Adam A. L. Michalchuk ◽  
Karl S. Hope ◽  
Stuart R. Kennedy ◽  
Maria V. Blanco ◽  
Elena V. Boldyreva ◽  
...  
Keyword(s):  
Real Time ◽  
Powder Diffraction ◽  
Crystal Formation ◽  
Real Time Monitoring ◽  
X Ray ◽  
Resonant Acoustic Mixing ◽  
First Time

Co-crystal formation by resonant acoustic mixing was followed for the first time by in situ real-time X-ray powder diffraction.

scholarly journals Mechanisms of mechanochemical salt formation by in situ real time X-ray powder diffraction

2016 ◽  
Vol 72 (a1) ◽  
pp. s394-s394
Author(s):  
Adam A. L. Michalchuk ◽  
Ivan A. Tumanov ◽  
Simon A. J. Kimber ◽  
Elena V. Boldyreva ◽  
Colin R. Pulham
Keyword(s):  
Real Time ◽  
Powder Diffraction ◽  
Salt Formation ◽  
X Ray

In situ and real-time monitoring of mechanochemical milling reactions using synchrotron X-ray diffraction

2013 ◽  
Vol 8 (9) ◽  
pp. 1718-1729 ◽  
Author(s):  
Ivan Halasz ◽  
Simon A J Kimber ◽  
Patrick J Beldon ◽  
Ana M Belenguer ◽  
Frank Adams ◽  
...  
Keyword(s):  
Real Time ◽  
X Ray Diffraction ◽  
Real Time Monitoring ◽  
X Ray ◽  
Mechanochemical Milling

In Situ Soldering Process Technique by Synchrotron X-Ray Imaging

2015 ◽  
Vol 754-755 ◽  
pp. 508-512
Author(s):  
M.A.A. Mohd Salleh ◽  
A. Sugiyama ◽  
Hideyuki Yasuda ◽  
Stuart D. McDonald ◽  
Kazuhiro Nogita
Keyword(s):  
Real Time ◽  
Void Formation ◽  
In Situ Observation ◽  
Cu Substrate ◽  
X Ray ◽  
Soldering Process ◽  
X Ray Imaging ◽  
Free Solder ◽  
First Time

This paper demonstrates the development of an experimental technique of in-situ observation for soldering of Sn-0.7wt%Cu lead-free solder on a Cu substrate which was achieved for the first time by synchrotron X-ray imaging. Reactions between liquid solder and Cu substrate during a soldering process were able to be recorded in real-time. Individual stages of the soldering process consisted of flux activation in removal of Cu oxide, solder melting and contact with the Cu substrate (wetting) and intermetallic compound (IMC) and void formation between the solder and Cu substrate. The technique development which includes experimental setup with calculated optimum beam energy in the range of 20 – 30 keV appears to result in a clear observation of real-time X-ray imaging of the soldering process. This technique provides a key method to understand the mechanism of formation of micro-electronic inter-connects for future electronic packaging applications.

Formation of silica–surfactant mesophases studied by real-time in situ X-ray powder diffraction

1995 ◽  
pp. 2423-2424 ◽  
Author(s):  
Stephen O'Brien ◽  
Robin J. Francis ◽  
Stephen J. Price ◽  
Dermot O'Hare ◽  
Simon M. Clark ◽  
...  
Keyword(s):  
Real Time ◽  
Powder Diffraction ◽  
X Ray

Real-Time Investigation of the Structural Evolution of Electrodes in a Lithium-Ion Battery Containing V-Added LiFePO4Cathode Using In-Situ Synchrotron X-Ray Powder Diffraction

PRICM ◽  
2013 ◽  
pp. 3505-3512
Author(s):  
Chih-Wei Hu ◽  
Kai-Sheng Shih ◽  
Ching-Yu Chiang ◽  
Hui-Chia Su ◽  
Bor-Yuan Shew ◽  
...  
Keyword(s):  
Lithium Ion Battery ◽  
Real Time ◽  
Powder Diffraction ◽  
Structural Evolution ◽  
Lithium Ion ◽  
X Ray

Manipulating the dynamics of mechanochemical ternary cocrystal formation

2019 ◽  
Vol 55 (66) ◽  
pp. 9793-9796 ◽  
Author(s):  
Hannes Kulla ◽  
Adam A. L. Michalchuk ◽  
Franziska Emmerling
Keyword(s):  
Raman Spectroscopy ◽  
Real Time ◽  
Powder Diffraction ◽  
X Ray

In situ real-time X-ray powder diffraction and Raman spectroscopy reveal formation pathways of ternary co-crystals by mechanochemistry.

In-situ and real-time monitoring of MOCVD growth of III-nitrides by simultaneous multi-wavelength-ellipsometry and X-ray-diffraction

2006 ◽  
Vol 203 (7) ◽  
pp. 1704-1707 ◽  
Author(s):  
C. Simbrunner ◽  
K. Schmidegg ◽  
A. Bonanni ◽  
A. Kharchenko ◽  
J. Bethke ◽  
...  
Keyword(s):  
Real Time ◽  
X Ray Diffraction ◽  
Real Time Monitoring ◽  
X Ray ◽  
Mocvd Growth ◽  
Multi Wavelength
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