Miniaturized UV-LED Array Chip Photochemical Vapor Generator Coupled with Point Discharge Optical Emission Spectrometer for Determination of Trace Selenium

2021 ◽  
Author(s):  
Mengtian Li ◽  
Yi Luo ◽  
Zhirong Zou ◽  
Fujian Xu ◽  
Xiaoming Jiang ◽  
...  
Keyword(s):  
Light Emitting Diode ◽  
Optical Emission ◽  
Nano Tio2 ◽  
Light Emitting ◽  
Uv Led ◽  
Led Array ◽  
Point Discharge ◽  
Photochemical Vapor Generation ◽  
Optical Emission Spectrometer

An ultraviolet light emitting diode (UV-LED) array chip as irradiation source for nano-TiO2 catalyzed photochemical vapor generation (PCVG) was combined with a hollow electrode point discharge microplasma optical emission spectrometer...

Hydride generation-point discharge microplasma-optical emission spectrometry for the determination of trace As, Bi, Sb and Sn

2016 ◽  
Vol 31 (12) ◽  
pp. 2427-2433 ◽  
Author(s):  
Mengtian Li ◽  
Yujia Deng ◽  
Chengbin Zheng ◽  
Xiaoming Jiang ◽  
Xiandeng Hou
Keyword(s):  
Hydride Generation ◽  
Optical Emission ◽  
Optical Emission Spectrometry ◽  
Sample Introduction ◽  
Excitation Source ◽  
Emission Spectrometry ◽  
Point Discharge ◽  
Optical Emission Spectrometer

A miniaturized optical emission spectrometer (OES) with point discharge (PD) helium–hydrogen microplasma as an excitation source and hydride generation (HG) for sample introduction was constructed for the determination of trace As, Bi, Sb and Sn.

UV photochemical vapor generation–nitrogen microwave induced plasma optical emission spectrometric determination of nickel

2018 ◽  
Vol 33 (6) ◽  
pp. 1086-1091 ◽  
Author(s):  
Mengtian Li ◽  
Yujia Deng ◽  
Xiaoming Jiang ◽  
Xiandeng Hou
Keyword(s):  
Optical Emission ◽  
Analytical Performance ◽  
Sample Introduction ◽  
Vapor Generation ◽  
Microwave Induced Plasma ◽  
Determination Of Nickel ◽  
Photochemical Vapor Generation ◽  
Gaseous Sample ◽  
Optical Emission Spectrometer

Photochemical vapor generation was utilized for gaseous sample introduction into a nitrogen microwave induced plasma optical emission spectrometer in order to enhance the analytical performance.

scholarly journals Design of a Secondary Freeform Lens of UV LED Mosquito-Trapping Lamp for Enhancing Trapping Efficiency

Crystals ◽  
2018 ◽  
Vol 8 (9) ◽  
pp. 335 ◽  
Author(s):  
Wei-Hsiung Tseng ◽  
Diana Juan ◽  
Wei-Cheng Hsiao ◽  
Cheng-Han Chan ◽  
Hsin-Yi Ma ◽  
...  
Keyword(s):  
Light Intensity ◽  
Intensity Distribution ◽  
Light Emitting Diode ◽  
Trapping Efficiency ◽  
Axially Symmetric ◽  
Light Intensity Distribution ◽  
Light Emitting ◽  
Led Light ◽  
Uv Led ◽  
Freeform Lens

In this study, our proposed ultraviolet light-emitting diode (UV LED) mosquito-trapping lamp is designed to control diseases brought by insects such as mosquitoes. In order to enable the device to efficiently catch mosquitoes in a wider area, a secondary freeform lens (SFL) is designed for UV LED. The lens is mounted on a 3 W UV LED light bar as a mosquito-trapping lamp of the new UV LED light bar module to achieve axially symmetric light intensity distribution. The special SFL is used to enhance the trapping capabilities of the mosquito-trapping lamp. The results show that when the secondary freeform surface lens is applied to the experimental outdoor UV LED mosquito-trapping lamp, the trapping range can be expanded to 100π·m2 and the captured mosquitoes increased by about 300%.

Cross Double Point Discharge as Enhanced Excitation Source for Highly Sensitive Determination of Arsenic, Mercury and Lead by Optical Emission Spectrometry

2021 ◽  
Author(s):  
Lin He ◽  
Peixia Li ◽  
Kai Li ◽  
Tao Lin ◽  
Jin Luo ◽  
...  
Keyword(s):  
Double Point ◽  
Hydride Generation ◽  
Optical Emission ◽  
Sample Introduction ◽  
Excitation Source ◽  
Emission Spectrometry ◽  
Highly Sensitive ◽  
Point Discharge ◽  
Sensitive Determination

A new cross double point discharge (CrossPD) microplasma was designed as an excitation source to construct a miniaturized optical emission spectrometer with hydride generation (HG) for sample introduction. The CrossPD...

scholarly journals THE MATHEMATICAL MODELING OF METALS CONTENT IN PEAT

2015 ◽  
Vol 1 ◽  
pp. 249
Author(s):  
Edmunds Teirumnieks ◽  
Ērika Teirumnieka ◽  
Ilmārs Kangro ◽  
Harijs Kalis
Keyword(s):  
Mathematical Modeling ◽  
Mathematical Model ◽  
Inductively Coupled Plasma ◽  
Optical Emission ◽  
Peat Bog ◽  
Inductively Coupled ◽  
Pollution Loading ◽  
The Mathematical Model ◽  
Optical Emission Spectrometer

Metals deposition in peat can aid to evaluate impact of atmospheric or wastewaters pollution and thus can be a good indicator of recent and historical changes in the pollution loading. For peat using in agriculture, industrial, heat production etc. knowledge of peat metals content is important. Experimental determination of metals in peat is very long and expensive work. Using experimental data the mathematical model for calculation of concentrations of metals in different points for different layers is developed. The values of the metals (Ca, Mg, Fe, Sr, Cu, Zn, Mn, Pb, Cr, Ni, Se, Co, Cd, V, Mo) concentrations in different layers in peat taken from Knavu peat bog from four sites are determined using inductively coupled plasma optical emission spectrometer. Mathematical model for calculation of concentrations of metal has been described in the paper. As an example, mathematical models for calculation of Pb concentrations have been analyzed.

scholarly journals Determination of 3,4,5-Trihydroxybenzoic Acid Exploiting a Visible-Light-Driven Photoelectrochemical Platform: Application in Wine and Tea Samples

2022 ◽  
Author(s):  
Kayni Lima ◽  
Ridvan Fernandes ◽  
Clenilton dos Santos ◽  
Flavio Damos ◽  
Rita de Cássia Luz
Keyword(s):  
Light Emitting Diode ◽  
Glass Slide ◽  
Experimental Conditions ◽  
Amperometric Determination ◽  
Light Emitting ◽  
Promising Tool ◽  
Visible Light Driven ◽  
Photoelectrochemical Method ◽  
Acid Determination

The present work is based on the development and application of a photoelectrochemical method for the amperometric determination of 3,4,5-trihydroxybenzoic acid in different samples. The method is based on the use of a photoelectrochemical platform based on a glass slide coated with fluorine-doped tin oxide, which has been modified with cadmium sulfide and poly(D-glucosamine) and subjected to a light-emitting diode (LED) lamp. The photoelectrochemical platform was sensitive to the increase of the concentration of the antioxidant 3,4,5-trihydroxybenzoic acid in the solution. Under the optimized experimental conditions, the photoelectrochemical method presented a linear response for a 3,4,5-trihydroxybenzoic acid concentration ranging from 0.2 up to 500 μmol L-1. The method was applied to 3,4,5-trihydroxybenzoic acid determination in samples of wines and teas with recoveries between 95.88 and 101.72%. The results obtained suggest that the developed platform is a promising tool for quantifying the 3,4,5-trihydroxybenzoic acid.

scholarly journals Determination of Dental Adhesive Composition throughout Solvent Drying and Polymerization Using ATR–FTIR Spectroscopy

Polymers ◽  
2021 ◽  
Vol 13 (22) ◽  
pp. 3886
Author(s):  
Arwa Almusa ◽  
António H.S. Delgado ◽  
Paul Ashley ◽  
Anne M. Young
Keyword(s):  
Light Exposure ◽  
Light Emitting Diode ◽  
Attenuated Total Reflectance ◽  
Drying Time ◽  
Light Emitting ◽  
Spectral Changes ◽  
One Step ◽  
Urethane Dimethacrylate ◽  
Kinetics Of

The of this study aim was to develop a rapid method to determine the chemical composition, solvent evaporation rates, and polymerization kinetics of dental adhesives. Single-component, acetone-containing adhesives One-Step (OS; Bisco, USA), Optibond Universal (OU; Kerr, USA), and G-Bond (GB; GC, Japan) were studied. Filler levels were determined gravimetrically. Monomers and solvents were quantified by comparing their pure Attenuated Total Reflectance-Fourier Transform Infra-Red (ATR–FTIR) spectra, summed in different ratios, with those of the adhesives. Spectral changes at 37 °C, throughout passive evaporation for 5 min, then polymerisation initiated by 20 s, and blue light emitting diode (LED) (600 mW/cm2) exposure (n = 3) were determined. Evaporation and polymerisation extent versus time and final changes were calculated using acetone (1360 cm−1) and methacrylate (1320 cm−1) peaks. OS, OU, and GB filler contents were 0, 9.6, and 5.3%. FTIR suggested OS and OU were Bis-GMA based, GB was urethane dimethacrylate (UDMA) based, and that each had a different diluent and acidic monomers and possible UDMA/acetone interactions. Furthermore, initial acetone percentages were all 40−50%. After 5 min drying, they were 0% for OS and OU but 10% for GB. Whilst OS had no water, that in OU declined from 18 to 10% and in GB from 25 to 20% upon drying. Evaporation extents were 50% of final levels at 23, 25, and 113 s for OS, OU, and GB, respectively. Polymerisation extents were all 50 and 80% of final levels before 10 and at 20 s of light exposure, respectively. Final monomer polymerisation levels were 68, 69, and 88% for OS, OU, and GB, respectively. An appreciation of initial and final adhesive chemistry is important for understanding the properties. The rates of evaporation and polymerisation provide indications of relative required drying and light cure times. UDMA/acetone interactions might explain the considerably greater drying time of GB.

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