Base-Promoted Three-Component One-Pot Synthesis of 3- (Thiomethyl)indoles with Paraformaldehyde under Aqueous Conditions

Synlett ◽  
2018 ◽  
Vol 29 (20) ◽  
pp. 2693-2696 ◽  
Author(s):  
Fuhong Xiao ◽  
Guo-Jun Deng ◽  
Shanshan Yuan ◽  
Huawen Huang
Keyword(s):  
Carbon Source ◽  
Environmentally Friendly ◽  
Green Solvent ◽  
One Pot ◽  
One Pot Synthesis ◽  
Low Toxicity ◽  
Aqueous Conditions

An ethylenediamine-promoted three-component synthesis of 3-(thiomethyl)indoles from indoles, thiophenols, and paraformaldehyde has been developed. Water is used as the green solvent in a simple and environmentally friendly procedure. Stable and low-toxicity paraformaldehyde is used as a carbon source.

A Clean One-pot Synthesis of 7-Amino-5-Aryl-6-Cyano-1,5-Dihydro-2H-Pyrano[2,3-d] Pyrimidine-2,4(3H)-Diones in Aqueous Media under Ultrasonic Irradiation

2005 ◽  
Vol 2005 (3) ◽  
pp. 162-163 ◽  
Author(s):  
Tong-Shou Jin ◽  
Li-Bin Liu ◽  
Ying Zhao ◽  
Tong-Shuang Li
Keyword(s):  
Ultrasonic Irradiation ◽  
Aqueous Media ◽  
Environmentally Friendly ◽  
Green Solvent ◽  
One Pot ◽  
One Pot Synthesis ◽  
Novel Approach ◽  
Work Up

A novel approach to the synthesis of 7-amino-5-aryl-6-cyano-1,5-dihydro-2H-pyrano[2,3-d]pyrimidine-2,4(3H)-diones in aqueous media under ultrasonic irradiation without catalyst is described. This method provides several advantages such as being environmentally friendly, simple work-up procedure and milder condition. In addition, water was chosen as a green solvent.

scholarly journals Aqueous one-pot synthesis of well-defined zwitterionic diblock copolymers by RAFT polymerization: an efficient and environmentally-friendly route to a useful dispersant for aqueous pigments

2021 ◽  
Vol 23 (3) ◽  
pp. 1248-1258
Author(s):  
Shannon M. North ◽  
Steven P. Armes
Keyword(s):  
Iron Oxide ◽  
Diblock Copolymers ◽  
Raft Polymerization ◽  
Environmentally Friendly ◽  
Iron Oxide Particles ◽  
One Pot ◽  
One Pot Synthesis ◽  
Highly Effective ◽  
Oxide Particles

An atom-efficient, wholly aqueous one-pot synthesis of zwitterionic diblock copolymers has been devised. Such copolymers can serve as highly effective aqueous dispersants for nano-sized transparent yellow iron oxide particles.

scholarly journals ZnO Nanoparticles: A Highly Effective and Readily Recyclable Catalyst for the One-Pot Synthesis of 1,8-dioxo-decahydroacridine and 1,8-dioxooctahydro-xanthene Derivatives

2017 ◽  
Vol 57 (1) ◽  
Author(s):  
Javad Safaei-Ghomi ◽  
Mohammad Ali Ghasemzadeh ◽  
Safura Zahedi
Keyword(s):  
Zno Nanoparticles ◽  
Environmentally Friendly ◽  
Recyclable Catalyst ◽  
Solvent Free ◽  
One Pot ◽  
One Pot Synthesis ◽  
Solvent Free Conditions ◽  
Xanthene Derivatives ◽  
Highly Effective ◽  
The One

ZnO nanoparticles as a worthwhile and recyclable catalyst have been used for the one-pot synthesis of 1,8-dioxo-decahydroacridines and 1,8-dioxooctahydro-xanthenes via multi-component reactions under solvent-free conditions. The presented method is mild, environmentally friendly, inexpensive and highly effective to give the products in good to excellent yields.

scholarly journals Environmentally Friendly and Regioselective One-Pot Synthesis of Imines and Oxazolidines Serinol Derivatives and Their Use for Rubber Cross-Linking

2020 ◽  
Vol 8 (25) ◽  
pp. 9356-9366
Author(s):  
Vincenzina Barbera ◽  
Gabriella Leonardi ◽  
Antonio Marco Valerio ◽  
Lucia Rubino ◽  
Shuquan Sun ◽  
...  
Keyword(s):  
Environmentally Friendly ◽  
Cross Linking ◽  
One Pot ◽  
One Pot Synthesis

Terminal Alkyne-Assisted One-Pot Synthesis of Arylamidines: Carbon Source of the Amidine Group from Oxime Chlorides

2019 ◽  
Vol 84 (11) ◽  
pp. 6780-6787 ◽  
Author(s):  
Fengping Yi ◽  
Qihui Sun ◽  
Jing Sun ◽  
Chao Fu ◽  
Weiyin Yi
Keyword(s):  
Carbon Source ◽  
Terminal Alkyne ◽  
One Pot ◽  
One Pot Synthesis

Mild, efficient, and environmentally friendly synthesis of symmetrical N,N′-alkylidenebisamides under solvent-free conditions catalyzed by H7[(P2W17O61)FeIII(H2O)]

RSC Advances ◽  
2016 ◽  
Vol 6 (25) ◽  
pp. 20687-20694 ◽  
Author(s):  
R. Tayebee ◽  
B. Maleki ◽  
F. M. Zonoz ◽  
R. M. Kakhki ◽  
T. Kunani
Keyword(s):  
Environmentally Friendly ◽  
Solvent Free ◽  
One Pot ◽  
Effective Catalyst ◽  
One Pot Synthesis ◽  
Solvent Free Conditions ◽  
Noticeable Reduction ◽  
The One

H7[(P2W17O61)FeIII(H2O)] is introduced as an effective catalyst for the one-pot synthesis ofN,N′-alkylidenebisamides. The catalyst could be easily separated without noticeable reduction in activity.

Environmentally Friendly One-Pot Synthesis of α-Alkylated Nitriles Using Hydrotalcite-Supported Metal Species as Multifunctional Solid Catalysts

2006 ◽  
Vol 12 (32) ◽  
pp. 8228-8239 ◽  
Author(s):  
Ken Motokura ◽  
Noriaki Fujita ◽  
Kohsuke Mori ◽  
Tomoo Mizugaki ◽  
Kohki Ebitani ◽  
...  
Keyword(s):  
Environmentally Friendly ◽  
Metal Species ◽  
One Pot ◽  
Solid Catalysts ◽  
One Pot Synthesis ◽  
Supported Metal
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