Sample holder for high-temperature vibrating sample magnetometer

2001 ◽  
Vol 72 (9) ◽  
pp. 3721-3722 ◽  
Author(s):  
M. Mikhov
Keyword(s):  
High Temperature ◽  
Vibrating Sample Magnetometer ◽  
Sample Holder

scholarly journals High-temperature (1500 K) reciprocal space mapping on a laboratory X-ray diffractometer

2007 ◽  
Vol 40 (2) ◽  
pp. 332-337 ◽  
Author(s):  
R. Guinebretière ◽  
A. Boulle ◽  
R. Bachelet ◽  
O. Masson ◽  
P. Thomas
Keyword(s):  
Thin Films ◽  
High Temperature ◽  
Reciprocal Space ◽  
Primary Beam ◽  
Sample Holder ◽  
Reciprocal Space Mapping ◽  
X Ray ◽  
Translation Stage

A laboratory X-ray diffractometer devoted to thein situcharacterization of the microstructure of epitaxic thin films at temperatures up to 1500 K has been developed. The sample holder was built using refractory materials, and a high-accuracy translation stage allows correction of the dilatation of both the sample and the sample holder. The samples are oriented with respect to the primary beam with two orthogonal rotations allowing the registration of symmetric as well as asymmetric reciprocal space maps (RSMs). The association of a monochromatic primary beam and a position-sensitive detector allows the measurement of RSMs in a few minutes for single crystals and in a few hours for imperfect epitaxic thin films. A detailed description of the setup is given and its potential is illustrated by high-temperature RSM experiments performed on yttria-doped zirconia epitaxic thin films grown on sapphire substrates.

Development of an Integrated Thermocouple for the Accurate Sample Temperature Measurement During High Temperature Environmental Scanning Electron Microscopy (HT-ESEM) Experiments

2015 ◽  
Vol 21 (2) ◽  
pp. 307-312 ◽  
Author(s):  
Renaud Podor ◽  
Damien Pailhon ◽  
Johann Ravaux ◽  
Henri-Pierre Brau
Keyword(s):  
High Temperature ◽  
Precise Measurement ◽  
Environmental Scanning Electron Microscopy ◽  
Sample Temperature ◽  
Silicate Melts ◽  
Environmental Scanning ◽  
Gas Composition ◽  
Sample Holder ◽  
Precision Control ◽  
Scanning Electron

AbstractWe have developed two integrated thermocouple (TC) crucible systems that allow precise measurement of sample temperature when using a furnace associated with an environmental scanning electron microscope (ESEM). Sample temperatures measured with these systems are precise (±5°C) and reliable. The TC crucible systems allow working with solids and liquids (silicate melts or ionic liquids), independent of the gas composition and pressure. These sample holder designs will allow end users to perform experiments at high temperature in the ESEM chamber with high precision control of the sample temperature.

3D printed sample holder for in-operando EPR spectroscopy on high temperature polymer electrolyte fuel cells

2016 ◽  
Vol 269 ◽  
pp. 157-161 ◽  
Author(s):  
Arvid Niemöller ◽  
Peter Jakes ◽  
Steffen Kayser ◽  
Yu Lin ◽  
Werner Lehnert ◽  
...  
Keyword(s):  
Fuel Cells ◽  
High Temperature ◽  
Polymer Electrolyte ◽  
Epr Spectroscopy ◽  
Polymer Electrolyte Fuel Cells ◽  
Sample Holder ◽  
3D Printed ◽  
In Operando
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