The Cu-doped cryptomelane-type octahedral molecular sieve manganese oxide synthesized by sol-gel for the degradation of methylene blue

Author(s):  
Amir Awaluddin ◽  
Lia Astuti ◽  
Amilia Linggawati ◽  
Siti Saidah Siregar ◽  
Prasetya Prasetya ◽  
...  
2019 ◽  
Vol 276 ◽  
pp. 06005 ◽  
Author(s):  
Amir Awaluddin ◽  
Riska Anggraini ◽  
Siti Saidah Siregar ◽  
Muhdarina ◽  
Prasetya

The Fe-doped octahedral molecular sieve manganese oxides have been successfully synthesized by one-pot synthesis of the reaction between KMnO4 and glucose using sol-gel methods. The oxide products are then characterized by various techniques such as X-ray diffraction, scanning electron microscopy, atomic absorption spectroscopy and average oxidation state (AOS) of manganese in manganese oxides. The as-synthesized manganese oxide and Fe-doped manganese oxides are used as catalysts for the degradation of methylene blue dye using hydrogen peroxide as oxidants. The results indicated that the Fe-doped manganese oxide catalyst displayed much enhanced catalytic activities compared to undoped manganese oxide for methylene blue degradation. The differences in catalytic activities have been correlated with the difference in surface properties and crystallinity.


2019 ◽  
Vol 56 ◽  
pp. 152-157 ◽  
Author(s):  
Abdelouahab Noua ◽  
Hichem Farh ◽  
Rebai Guemini ◽  
Oussama Zaoui ◽  
Tarek Diab Ounis ◽  
...  

Nickel oxide (NiO) thin films were successfully deposited by sol-gel dip-coating method on glass substrates. The structural, morphological and optical properties in addition to the photocatalytic activity of the prepared films were investigated. The results show that the films have a polycrystalline NiO cubic structure with dense NiO grains and average optical transmittance in the visible region. The photocatalytic properties of the films were studied through the degradation of methylene blue and 89% of degradation was achieved for 4.5h of solar light irradiation exposure which indicates the capability of NiO photocatalytic activity.


2017 ◽  
Vol 422 ◽  
pp. 754-762 ◽  
Author(s):  
Jun Li ◽  
Peng Ye ◽  
Jia Fang ◽  
Manye Wang ◽  
Deming Wu ◽  
...  

2013 ◽  
Vol 668 ◽  
pp. 13-16
Author(s):  
Qing Shan Li ◽  
Biao Zhan ◽  
Wei Hong ◽  
Guang Zhong Xing

Opal as a carrier, tetrabutyl titanate as a titanium source, TiO2 loaded on opal was prepared by sol-gel technique. The photocatalysts were characterized by XRD, TEM and UV-VIS absorption spectrum. Their photocatalytic activities were examined by the photocatalytic decolorization of methylene blue solution under UV light irradiation. The effects of calcination temperature, the amount of TiO2 loading and pH on photocatalytic activities were discussed. The results show that TiO2 supported on opal induced enhancement of photocatalytic decolorization rant and TiO2 doping is about 30 wt. % with 92.15% of decolorization rate at 700°C.


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