Glass Capillary Gas Chromatography of Secondary Amines in Foods with Flame Photometric Detection after Derivatization with Benzenesulfonyl Chloride

1981 ◽  
Vol 45 (10) ◽  
pp. 2237-2243
Author(s):  
Takashi Hamano ◽  
Yukimasa Mitsuhashi ◽  
Yukio Matsuki
Keyword(s):  
Gas Chromatography ◽  
Capillary Gas Chromatography ◽  
Secondary Amines ◽  
Glass Capillary ◽  
Benzenesulfonyl Chloride ◽  
Photometric Detection ◽  
Flame Photometric Detection

scholarly journals Collection and Analysis of Butyltin Compounds in Air at Nanogram-Per-Cubic-Meter Levels

1996 ◽  
Vol 79 (1) ◽  
pp. 170-174 ◽  
Author(s):  
Kamal Swami ◽  
Rajinder S Narang
Keyword(s):  
Gas Chromatography ◽  
Detection Limit ◽  
Sodium Borohydride ◽  
Analytical Method ◽  
Capillary Gas Chromatography ◽  
Methylene Chloride ◽  
Photometric Detection ◽  
Flame Photometric Detection ◽  
Butyltin Compounds

Abstract An analytical method for determining butyltin chlo rides in air at low nanogram-per-cubic-meter levels was developed. Butyltin chlorides investigated were mono-n-butyltin trichloride (MBTC),di-n-butyltin dichloride (DBTC), and tri-n-butyltin chlo ride (TBTC). These tin chlorides were trapped on cartridges packed with Porapak-N, eluted with methylene chloride containing 0.3% HCI, hy dridized with sodium borohydride, and analyzed by capillary gas chromatography with flame photometric detection. On the basis of a 20 m3 sample, a detection limit of 0.05 ng/m3 can be achieved.

scholarly journals Analysis of sulfur compounds using a water stationary phase in gas chromatography with flame photometric detection

2017 ◽  
Vol 9 (7) ◽  
pp. 1097-1104 ◽  
Author(s):  
Kaylan H. McKelvie ◽  
Kevin B. Thurbide
Keyword(s):  
Gas Chromatography ◽  
Stationary Phase ◽  
Capillary Gas Chromatography ◽  
Sulfur Compounds ◽  
Organic Sulfur ◽  
Flame Photometric Detector ◽  
Organic Sulfur Compounds ◽  
Photometric Detection ◽  
Photometric Detector ◽  
Flame Photometric Detection

The properties of using a water stationary phase for analyzing organic sulfur compounds in capillary gas chromatography (GC) with a flame photometric detector (FPD) are presented.

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