X‐Ray Powder Diffraction and Spectral Studies of Transition Metal Complexes Using Novel Tetradentate Macrocyclic Ligand

2005 ◽  
Vol 35 (9) ◽  
pp. 683-688 ◽  
Author(s):  
Sulekh Chandra ◽  
Rachna Gupta ◽  
Nidhi Gupta ◽  
S. S. Bawa
Keyword(s):  
Transition Metal ◽  
Metal Complexes ◽  
Transition Metal Complexes ◽  
Powder Diffraction ◽  
Macrocyclic Ligand ◽  
Spectral Studies ◽  
X Ray

X-ray crystallographic and 2D HETCOR NMR studies of 2-acetylthiophene-o-aminobenzoylhydrazone: synthesis and spectral studies of its transition metal complexes

2006 ◽  
Vol 788 (1-3) ◽  
pp. 22-29 ◽  
Author(s):  
Kalagouda B. Gudasi ◽  
Rashmi V. Shenoy ◽  
Ramesh S. Vadavi ◽  
Siddappa A. Patil ◽  
Munirathinam Nethaji
Keyword(s):  
Transition Metal ◽  
Metal Complexes ◽  
Transition Metal Complexes ◽  
Spectral Studies ◽  
Nmr Studies ◽  
X Ray

scholarly journals Ultrafast inter-ionic charge transfer of transition-metal complexes mapped by femtosecond x-ray powder diffraction

2013 ◽  
Vol 41 ◽  
pp. 05046
Author(s):  
F. Zamponi ◽  
B. Freyer ◽  
V. Juvé ◽  
J. Stingl ◽  
M. Woerner ◽  
...  
Keyword(s):  
Charge Transfer ◽  
Transition Metal ◽  
Metal Complexes ◽  
Transition Metal Complexes ◽  
Powder Diffraction ◽  
Ionic Charge ◽  
X Ray

scholarly journals Ultrafast inter-ionic charge transfer of transition-metal complexes mapped by femtosecond X-ray powder diffraction

2013 ◽  
Vol 138 (14) ◽  
pp. 144504 ◽  
Author(s):  
Benjamin Freyer ◽  
Flavio Zamponi ◽  
Vincent Juvé ◽  
Johannes Stingl ◽  
Michael Woerner ◽  
...  
Keyword(s):  
Charge Transfer ◽  
Transition Metal ◽  
Metal Complexes ◽  
Transition Metal Complexes ◽  
Powder Diffraction ◽  
Ionic Charge ◽  
X Ray

Preparation, properties and structure of some intermediate nido- and arachno-monocarbaboranes

1981 ◽  
Vol 46 (10) ◽  
pp. 2345-2353 ◽  
Author(s):  
Karel Baše ◽  
Bohumil Štíbr ◽  
Jiří Dolanský ◽  
Josef Duben
Keyword(s):  
Transition Metal ◽  
Metal Complexes ◽  
Transition Metal Complexes ◽  
Nmr Spectra ◽  
Liquid Ammonia ◽  
X Ray Diffraction ◽  
X Ray ◽  
H Nmr ◽  
Starting Compound

The 6-N(CH3)3-6-CB9H11 carbaborane reacts with sodium in liquid ammonia with the formation of 6-CB9H12- which was used as a starting compound for preparing the 4-CB8H14, 9-L-6-CB9H13 (L = (CH3)2S, CH3CN and P(C6H5)3), 1-(η5-C5H5)-1,2-FeCB9H10-, and 2,3-(η5-C5H5)2-2,31-Co2CB9H10- carboranes. The 4-CB8H14 compound was dehydrogenated at 623 K to give 4-(7)-CB8H12 carborane. Base degradation of 6-N(CH3)3-6-CB9H11 in methanol resulted in the formation of 3,4-μ-N(CH3)3CH-B5H10. The structure of all compounds was proposed on the basis of their 11B and 1H NMR spectra and X-ray diffraction was used in the case of the transition metal complexes.

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