In situ X-ray diffraction investigation of compression behavior in Gd 40 Y 16 Al 24 Co 20 bulk metallic glass under high pressure with synchrotron radiation

2009 ◽  
Vol 33 (11) ◽  
pp. 1028-1032 ◽  
Author(s):  
Xu Tao ◽  
Huang Lei ◽  
Dong Yan-Guo ◽  
Li Gong ◽  
Li Yan-Chun ◽  
...  
Keyword(s):  
High Pressure ◽  
Synchrotron Radiation ◽  
Metallic Glass ◽  
Bulk Metallic Glass ◽  
X Ray Diffraction ◽  
Compression Behavior ◽  
X Ray

Nucleation and growth in bulk metallic glass under high pressure investigated using in situ x-ray diffraction

2003 ◽  
Vol 83 (25) ◽  
pp. 5202-5204 ◽  
Author(s):  
W. H. Wang ◽  
P. Wen ◽  
D. Q. Zhao ◽  
M. X. Pan ◽  
T. Okada ◽  
...  
Keyword(s):  
High Pressure ◽  
Metallic Glass ◽  
Bulk Metallic Glass ◽  
Nucleation And Growth ◽  
X Ray Diffraction ◽  
X Ray

scholarly journals In-situhigh-pressure powder X-ray diffraction study of α-zirconium phosphate

2014 ◽  
Vol 70 (3) ◽  
pp. 510-516
Author(s):  
Jennifer E. Readman ◽  
Alistair Lennie ◽  
Joseph A. Hriljac
Keyword(s):  
High Pressure ◽  
Synchrotron Radiation ◽  
Zirconium Phosphate ◽  
Water Molecules ◽  
X Ray Diffraction ◽  
X Ray ◽  
Additional Water ◽  
Diffraction Patterns ◽  
Layered Phosphate

The high-pressure structural chemistry of α-zirconium phosphate, α-Zr(HPO4)2·H2O, was studied usingin-situhigh-pressure diffraction and synchrotron radiation. The layered phosphate was studied under both hydrostatic and non-hydrostatic conditions and Rietveld refinement carried out on the resulting diffraction patterns. It was found that under hydrostatic conditions no uptake of additional water molecules from the pressure-transmitting medium occurred, contrary to what had previously been observed with some zeolite materials and a layered titanium phosphate. Under hydrostatic conditions the sample remained crystalline up to 10 GPa, but under non-hydrostatic conditions the sample amorphized between 7.3 and 9.5 GPa. The calculated bulk modulus,K0= 15.2 GPa, showed the material to be very compressible with the weak linkages in the structure of the type Zr—O—P.

In situ high-energy x-ray diffraction observation of structural evolution in a Ti-based bulk metallic glass upon heating

2010 ◽  
Vol 25 (12) ◽  
pp. 2271-2277 ◽  
Author(s):  
N. Zheng ◽  
G. Wang ◽  
L.C. Zhang ◽  
M. Calin ◽  
M. Stoica ◽  
...  
Keyword(s):  
Metallic Glass ◽  
Bulk Metallic Glass ◽  
Free Volume ◽  
Structural Relaxation ◽  
Structural Evolution ◽  
High Energy ◽  
Rapid Quenching ◽  
X Ray Diffraction ◽  
X Ray

The structural evolution of the Ti40Zr10Cu34Pd14Sn2 bulk metallic glass (BMG) upon was investigated by means of in situ high-energy x-ray diffraction. The position, width, and intensity of the first peak in diffraction patterns are fitted through Voigt function below 800 K. All the peak position, width, and intensity values show a nearly linear increase with the increasing temperature to the onset temperature of structural relaxation, Tr = 510 K. However, these values start to deviate from the linear behavior between Tr and Tg (the glass transition temperature). The changes in free volume and the coefficient of volume thermal expansion prove that the aforementioned phenomenon is closely related to the structural relaxation releasing excess free volume arrested during rapid quenching of the BMG. Above 800 K, three crystallization events are detected and the first exothermic event is due to the formation of metastable nanocrystals.

Preparation of Zr60Ni21Al19 bulk metallic glass and compression behavior under high pressure

2008 ◽  
Vol 23 (9) ◽  
pp. 2346-2349 ◽  
Author(s):  
G. Li ◽  
Q. Jing ◽  
T. Xu ◽  
L. Huang ◽  
R.P. Liu ◽  
...  
Keyword(s):  
High Pressure ◽  
Metallic Glass ◽  
Bulk Metallic Glass ◽  
High Strength ◽  
Amorphous Structure ◽  
X Ray Diffraction ◽  
Compression Behavior ◽  
Copper Mold Casting ◽  
Mold Casting ◽  
Diamond Anvil

Zr60Ni21Al19 metallic glass rod, with a diameter of 8 mm, is manufactured by copper mold casting. The as-cast bulk metallic glass (BMG) exhibits nearly zero plastic strain, but a high strength of 1.88 GPa. The compression behavior of this new zirconium-base ternary BMG under high pressure at ambient temperature in a diamond-anvil cell instrument has been unraveled using energy dispersive x-ray diffraction with a synchrotron radiation source. The investigation shows that the amorphous structure of Zr60Ni21Al19 is stable under pressures up to 24.5 GPa at room temperature. According to the Bridgman equation of state, the bulk modulus B0 = 96 GPa has been obtained.

scholarly journals The solvothermal synthesis of γ-AlOOH nanoflakes and their compression behaviors under high pressures

RSC Advances ◽  
2017 ◽  
Vol 7 (9) ◽  
pp. 4904-4911 ◽  
Author(s):  
Xudong Zhou ◽  
Jian Zhang ◽  
Yanmei Ma ◽  
Hui Tian ◽  
Yue Wang ◽  
...  
Keyword(s):  
High Pressure ◽  
Synchrotron Radiation ◽  
Solvothermal Synthesis ◽  
High Pressures ◽  
X Ray Diffraction ◽  
X Ray ◽  
Radiation Angle

The compression behaviors of γ-AlOOH nanoflakes were investigated via in situ high pressure synchrotron radiation angle dispersive X-ray diffraction techniques.

scholarly journals Crystallization of Zr41Ti14Cu12.5Ni10Be22.5 bulk metallic glass under high pressure examined byin situsynchrotron radiation x-ray diffraction

2006 ◽  
Vol 99 (2) ◽  
pp. 023525 ◽  
Author(s):  
C. Yang ◽  
W. K. Wang ◽  
R. P. Liu ◽  
Z. J. Zhan ◽  
L. L. Sun ◽  
...  
Keyword(s):  
High Pressure ◽  
Metallic Glass ◽  
Bulk Metallic Glass ◽  
X Ray Diffraction ◽  
X Ray

The stability of B6 octahedron in BaB6 under high pressure

RSC Advances ◽  
2016 ◽  
Vol 6 (22) ◽  
pp. 18077-18081 ◽  
Author(s):  
Xin Li ◽  
Xiaoli Huang ◽  
Defang Duan ◽  
Gang Wu ◽  
Mingkun Liu ◽  
...  
Keyword(s):  
High Pressure ◽  
First Principles ◽  
First Principles Calculations ◽  
X Ray Diffraction ◽  
Compression Behavior ◽  
X Ray ◽  
The Stability

We have performed in situ synchrotron X-ray diffraction and first-principles calculations to explore the compression behavior of barium hexaboride (BaB6) under high pressure.

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