scholarly journals The dry ashing - AAS method and the microwave digestion -ICP-MS method for determination of lead in plastic packaging bag

2019 ◽  
Vol 300 ◽  
pp. 052024
Author(s):  
Haipeng Mi ◽  
Xilin Zhou ◽  
Bo Liang ◽  
Zhonghua Su ◽  
Qingqing Huang ◽  
...  
Keyword(s):  
Microwave Digestion ◽  
Plastic Packaging ◽  
Icp Ms ◽  
Dry Ashing ◽  
Aas Method

Microwave digestion with HNO3/H2O2 mixture at high temperatures for determination of trace elements in coal by ICP-OES and ICP-MS

2004 ◽  
Vol 514 (1) ◽  
pp. 115-124 ◽  
Author(s):  
Jie Wang ◽  
Tetsuya Nakazato ◽  
Kinya Sakanishi ◽  
Osamu Yamada ◽  
Hiroaki Tao ◽  
...  
Keyword(s):  
Trace Elements ◽  
High Temperatures ◽  
Microwave Digestion ◽  
Icp Oes ◽  
Icp Ms

scholarly journals A high-resolution ICP-MS method for the determination of 38 inorganic elements in human whole blood, urine, hair and tissues after microwave digestion

Talanta ◽  
2019 ◽  
Vol 199 ◽  
pp. 228-237 ◽  
Author(s):  
Stanislas Grassin-Delyle ◽  
Marie Martin ◽  
Ons Hamzaoui ◽  
Elodie Lamy ◽  
Christophe Jayle ◽  
...  
Keyword(s):  
High Resolution ◽  
Whole Blood ◽  
Microwave Digestion ◽  
Inorganic Elements ◽  
Human Whole Blood ◽  
Icp Ms

Atomic Absorption Spectroscopy of Copper and Iron in Plant Material

1977 ◽  
Vol 60 (5) ◽  
pp. 1170-1174
Author(s):  
Duane R Boline ◽  
W G Schrenk
Keyword(s):  
Atomic Absorption ◽  
Operating Conditions ◽  
Water Mixture ◽  
Alcohol Water ◽  
Dry Ashing ◽  
Cathode Current ◽  
Aas Method ◽  
Significant Interference ◽  
Determination Of Copper

Abstract An atomic absorption spectroscopic (AAS) method is described for the determination of copper and iron by direct aspiration of a solution of an ashed sample in an alcohol-water mixture. The method has been applied to samples containing 2.0–31.9 μg Cu/g and 15.5–196 Fe/g. Operating conditions for using an acetylene-air flame have been established. The hollow cathode current needed to be carefully controlled for the copper analysis. No significant interference was noted from other elements commonly present in plants. Wet and dry ashing procedures provided comparable results. Recovery of added amounts of copper and iron ranged from 92 to 101% and 94 to 104%, respectively; most results were near 100%. The official AOAC colorimetric methods and the AAS method were compared and were comparable in reliability and accuracy. The AAS method is simpler and faster.

Determination of multi-element in abstergent by ICP-MS with microwave digestion

2017 ◽  
Author(s):  
BeiLei Wu ◽  
ZhenXin Wang ◽  
JiaMei Ye ◽  
ZhenXing Lin ◽  
Hao Wang ◽  
...  
Keyword(s):  
Microwave Digestion ◽  
Icp Ms

Simultaneous Determination of 10 Ultratrace Elements in Infant Formula, Adult Nutritionals, and Milk Products by ICP/MS After Pressure Digestion: Single-Laboratory Validation

2015 ◽  
Vol 98 (4) ◽  
pp. 953-961 ◽  
Author(s):  
Stephane Dubascoux ◽  
Marine Nicolas ◽  
Celine Fragniere Rime ◽  
Janique Richoz Payot ◽  
Eric Poitevin
Keyword(s):  
Simultaneous Determination ◽  
Inductively Coupled Plasma ◽  
Microwave Digestion ◽  
Performance Criteria ◽  
Method Performance ◽  
International Regulation ◽  
Icp Ms ◽  
Ultratrace Elements ◽  
Single Laboratory

Abstract A single-laboratory validation (SLV) is presented for the simultaneous determination of 10 ultratrace elements (UTEs) including aluminum (Al), arsenic (As), cadmium (Cd), cobalt (Co), chromium (Cr), mercury (Hg), molybdenum (Mo), lead (Pb), selenium (Se), and tin (Sn) in infant formulas, adult nutritionals, and milk based products by inductively coupled plasma (ICP)/MS after acidic pressure digestion. This robust and routine multielemental method is based on several official methods with modifications of sample preparation using either microwave digestion or high pressure ashing and of analytical conditions using ICP/MS with collision cell technology. This SLV fulfills AOAC method performance criteria in terms of linearity, specificity, sensitivity, precision, and accuracy and fully answers most international regulation limits for trace contaminants and/or recommended nutrient levels established for 10 UTEs in targeted matrixes.

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