scholarly journals Ultrasonic attenuation in lead

The absorption of longitudinal ultrasonic waves has been studied as a function of transverse magnetic field in pure single crystals of lead at 1.2 °K. The results were found to be generally consistent with the Fermi surface of lead suggested by Gold. In particular a detailed study of the magneto-acoustic oscillations, as a function of sample orientation and field direction, allowed the determination of some of the dimensions of the hole surface in the second Brillouin zone and revealed a number of new electronic orbits on the multiply-connected surface in the third zone. The absolute magnitude of the attenuation and its dependence on propagation direction and on magnetic field was studied and the results interpreted in terms of the general theory of ultrasonic absorption.

1979 ◽  
Vol 15 (3) ◽  
pp. 316-317 ◽  
Author(s):  
V. M. Mel'nikov ◽  
�. A. Putnin'sh ◽  
V. O. Putninya ◽  
V. P. Karlivan

1977 ◽  
Vol 32 (9) ◽  
pp. 946-951
Author(s):  
Erwin Kittinger

AbstractAttenuation and velocity of longitudinal ultrasonic waves have been measured in a-Se in the vicinity of the glass transition. Both quantities are shown to be affected significantly by the stabilization process below the glass transition temperature Tg. Equilibrium values of sound velocity are also reported for the range 25 °C to 45 °C. The decrease (increase) of attenuation (velocity) during stabilization is reversed at higher temperatures. The connection of both quantities is discussed in terms of an effective temperature which allows the approximate determination of equilibrium values of attenuation (and possibly of other structure related properties) from measurements performed in nonequilibrium states.


1971 ◽  
Vol 49 (3) ◽  
pp. 296-301 ◽  
Author(s):  
J. M. Perz ◽  
W. A. Roger

The attenuation due to interaction with conduction electrons of longitudinal sound propagating along [110] in a Ta crystal of resistance ratio 390 has been measured over the frequency range 0.46 to 1.0 GHz. The product of the wave vector q and the electronic mean free path l determined from the frequency dependence of the normal state attenuation ranges over 1.8 < ql < 3.8. The attenuation in the superconducting state in the absence of a magnetic field fits the BCS expression for 1.2 < T < Tc = 4.46 K with 2Δ(0) = 3.62 ± 0.06 kTc. The ultrasonic waves have been generated by thin film CdS transducers, and the conversion efficiency has been found to vary inversely with the active area of the transducer.


1973 ◽  
Vol 51 (1) ◽  
pp. 77-86 ◽  
Author(s):  
J. P. Kalejs ◽  
J. M. Perz

We have measured the frequencies of quantum oscillations in the attenuation of 20 MHz longitudinal ultrasonic waves in tungsten in magnetic fields up to 109 kOe. Our results agree well with the de Haas–van Alphen (dHvA) data of Girvan, Gold, and Phillips (GGP). In addition, we see features predicted by the empirical model developed by GGP but not observed directly in the dHvA studies. Specifically, we find strong evidence of the continuation of the ω branch (GGP notation) for the magnetic field H in the [Formula: see text] plane right to the [110] direction; we also observe splitting of the ξ branch for field directions near [111], but not to the extent predicted by the model. From the temperature dependence of the amplitudes of the quantum oscillations, we have deduced cyclotron masses for some orbits; these agree well with GGP and cyclotron resonance data.


The attenuation of an ultrasonic wave by direct interaction with the conduction electrons in a metal is analyzed without making any special assumptions about the shape of the Fermi surface. The problem is reduced to a calculation of the currents set up in a stationary lattice by forces on the electrons, some real (due to electric fields) and some fictitious to describe the disturbances due to the passage of the wave. The fictitious forces have their origin in the relative motion of different parts of the metal and in the change in shape of the equilibrium form of the Fermi surface as a result of lattice deformation. It is assumed, as is valid for ultrasonic frequencies below about 10 9 c/s, that the electric fields serve to annul any electronic current relative to the lattice. The expressions obtained are qualitatively similar to the earlier results for a free-electron model, in particular the attenuation tends to a con­stant limit as the electronic free path becomes infinite. Only for a pure longitudinal wave is the limit simple in form and there it is determined by the Gaussian curvature and the mean square value of the deformation parameter round that zone of the Fermi surface on which the electrons move parallel to the wave front. The analysis is extended to cover the situation which arises in a transverse magnetic field, in the limit when the free path is long compared with the electronic orbit perimeters. The results are very complicated, but qualitatively similar to the free-electron results in the types of oscillatory behaviour predicted and in the limiting values of the attenuation as the magnetic field increases without limit; if there are open orbits present, however, the limiting behaviour is changed, the attenuation of longitudinal waves for instance tending to infinity as H 2 . Although the oscillatory behaviour may usually be governed by the extreme exten­sions of the Fermi surface in a direction normal to H and to the direction of propagation, it is suggested that this is not likely to hold if the deformation parameter is very variable over the Fermi surface, as is probable in the noble metals, and that the oscillations may then indicate the positions of parts of high deformability.


Materials ◽  
2021 ◽  
Vol 14 (10) ◽  
pp. 2594
Author(s):  
Marta Harničárová ◽  
Jan Valíček ◽  
Milena Kušnerová ◽  
Zuzana Palková ◽  
Ivan Kopal ◽  
...  

The formulation of the Hall–Petch relationship in the early 1950s has raised immense interest in studying the influence of the grain size of solid materials on their properties. Grain refinement can be achieved through extreme deformation. In the presented study, Equal-Channel Angular Pressing (ECAP) was successfully applied to produce an ultrafine-grained microstructure in a pure commercial Cu of 99.9 wt%. Samples were processed by ECAP at 21 °C for six passes via route A. A new equation of equilibrium that allows the exact determination of the number of extrusions and other technological parameters required to achieve the desired final grain size has been developed. The presented research also deals, in a relatively detailed and comparative way, with the use of ultrasound. In this context, a very close correlation between the process functions of extrusion and the speed of longitudinal ultrasonic waves was confirmed.


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