Phase-Vortex Removal for Quantitative X-Ray Nanotomography with Near-Field Ptychography

2020 ◽  
Vol 14 (6) ◽  
Author(s):  
Irene Zanette ◽  
Richard Clare ◽  
David Eastwood ◽  
Charan Venkata ◽  
Franz Pfeiffer ◽  
...  
Keyword(s):  
2015 ◽  
Vol 23 (10) ◽  
pp. 12720 ◽  
Author(s):  
Marco Stockmar ◽  
Maxime Hubert ◽  
Martin Dierolf ◽  
Bjoern Enders ◽  
Richard Clare ◽  
...  
Keyword(s):  

2004 ◽  
Vol 70 (1) ◽  
Author(s):  
F. Staub ◽  
M. Braud ◽  
J. E. Balmer ◽  
J. Nilsen ◽  
S. Bajt
Keyword(s):  
X Ray ◽  

2016 ◽  
Author(s):  
Dakui Lin ◽  
Huoyao Chen ◽  
Stefanie Kroker ◽  
Thomas Käsebier ◽  
Zhengkun Liu ◽  
...  

2020 ◽  
Vol 27 (6) ◽  
pp. 1703-1706
Author(s):  
D. P. Siddons ◽  
A. J. Kuczewski ◽  
A. K. Rumaiz ◽  
R. Tappero ◽  
M. Idir ◽  
...  

The design and construction of an instrument for full-field imaging of the X-ray fluorescence emitted by a fully illuminated sample are presented. The aim is to produce an X-ray microscope with a few micrometers spatial resolution, which does not need to scan the sample. Since the fluorescence from a spatially inhomogeneous sample may contain many fluorescence lines, the optic which will provide the magnification of the emissions must be achromatic, i.e. its optical properties must be energy-independent. The only optics which fulfill this requirement in the X-ray regime are mirrors and pinholes. The throughput of a simple pinhole is very low, so the concept of coded apertures is an attractive extension which improves the throughput by having many pinholes, and retains the achromatic property. Modified uniformly redundant arrays (MURAs) with 10 µm openings and 50% open area have been fabricated using gold in a lithographic technique, fabricated on a 1 µm-thick silicon nitride membrane. The gold is 25 µm thick, offering good contrast up to 20 keV. The silicon nitride is transparent down into the soft X-ray region. MURAs with various orders, from 19 up to 73, as well as their respective negative (a mask where open and closed positions are inversed compared with the original mask), have been made. Having both signs of mask will reduce near-field artifacts and make it possible to correct for any lack of contrast.


2017 ◽  
Vol 50 (3) ◽  
pp. 701-711 ◽  
Author(s):  
Qi Zhong ◽  
Lars Melchior ◽  
Jichang Peng ◽  
Qiushi Huang ◽  
Zhanshan Wang ◽  
...  

Iterative phase retrieval has been used to reconstruct the near-field distribution behind tailored X-ray waveguide arrays, by inversion of the measured far-field pattern recorded under fully coherent conditions. It is thereby shown that multi-waveguide interference can be exploited to control the near-field distribution behind the waveguide exit. This can, for example, serve to create a secondary quasi-focal spot outside the waveguide structure. For this proof of concept, an array of seven planar Ni/C waveguides are used, with precisely varied guiding layer thickness and cladding layer thickness, as fabricated by high-precision magnetron sputtering systems. The controlled thickness variations in the range of 0.2 nm results in a desired phase shift of the different waveguide beams. Two kinds of samples, a one-dimensional waveguide array and periodic waveguide multilayers, were fabricated, each consisting of seven C layers as guiding layers and eight Ni layers as cladding layers. These are shown to yield distinctly different near-field patterns.


2016 ◽  
Vol 72 (2) ◽  
pp. 215-221 ◽  
Author(s):  
Aike Ruhlandt ◽  
Tim Salditt

This paper presents an extension of phase retrieval algorithms for near-field X-ray (propagation) imaging to three dimensions, enhancing the quality of the reconstruction by exploiting previously unused three-dimensional consistency constraints. The approach is based on a novel three-dimensional propagator and is derived for the case of optically weak objects. It can be easily implemented in current phase retrieval architectures, is computationally efficient and reduces the need for restrictive prior assumptions, resulting in superior reconstruction quality.


1997 ◽  
Vol 3 (S2) ◽  
pp. 1185-1186
Author(s):  
J. Maser ◽  
C. Jacobsen ◽  
S. Spector

In far-field microscopes, the spatial resolution is ultimately limited by the wavelength of the radiation used. While near-field and related microscopes can improve upon this, they can only do so with thin specimen regions. Thin specimens can also be studied at atomic resolution using electron microscopes. To achieve improved resolution on micrometer-thick specimens, another alternative is to use significantly shorter photon wavelengths. We discuss here the use of soft x-rays for microscopy and their resolution limits.Image formation requires resolution and contrast. by using soft x-rays with a photon energy between the K absorption edges of carbon and oxygen, one is able to image hydrated biological specimens with high contrast. The contrast is such that no addi-tional staining is required, while efforts are also underway to utilize gold and luminescent probes for selective labeling. In addition, x-ray sources have high spectral resolution and good signal-to-background relative to electron microscopes which allows for elemental and chemical state mapping of major constituents.


2004 ◽  
Author(s):  
Antony J. Bourdillon ◽  
Gwyn P. Williams ◽  
Yuli Vladimirsky ◽  
Chris B. Boothroyd
Keyword(s):  

2014 ◽  
Vol 71 (11) ◽  
pp. 580-585
Author(s):  
Yuya SHINOHARA ◽  
Teruaki YOSHII ◽  
Hiroyuki KISHIMOTO ◽  
Kentaro UESUGI ◽  
Yoshiyuki AMEMIYA
Keyword(s):  
X Ray ◽  

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