scholarly journals X-ray in-line holography and holotomography at the NanoMAX beamline

2022 ◽  
Vol 29 (1) ◽  
Author(s):  
Sebastian Kalbfleisch ◽  
Yuhe Zhang ◽  
Maik Kahnt ◽  
Khachiwan Buakor ◽  
Max Langer ◽  
...  
Keyword(s):  
Electron Density ◽  
Low Dose ◽  
Focal Spot ◽  
Chemical Elements ◽  
Imaging Techniques ◽  
High Sensitivity ◽  
X Ray ◽  
X Ray Imaging ◽  
Dose Imaging ◽  
2D And 3D

Coherent X-ray imaging techniques, such as in-line holography, exploit the high brilliance provided by diffraction-limited storage rings to perform imaging sensitive to the electron density through contrast due to the phase shift, rather than conventional attenuation contrast. Thus, coherent X-ray imaging techniques enable high-sensitivity and low-dose imaging, especially for low-atomic-number (Z) chemical elements and materials with similar attenuation contrast. Here, the first implementation of in-line holography at the NanoMAX beamline is presented, which benefits from the exceptional focusing capabilities and the high brilliance provided by MAX IV, the first operational diffraction-limited storage ring up to approximately 300 eV. It is demonstrated that in-line holography at NanoMAX can provide 2D diffraction-limited images, where the achievable resolution is only limited by the 70 nm focal spot at 13 keV X-ray energy. Also, the 3D capabilities of this instrument are demonstrated by performing holotomography on a chalk sample at a mesoscale resolution of around 155 nm. It is foreseen that in-line holography will broaden the spectra of capabilities of MAX IV by providing fast 2D and 3D electron density images from mesoscale down to nanoscale resolution.

Experimental Evaluation of Physical Breast Phantoms for 2D and 3D Breast X-Ray Imaging Techniques

2020 ◽  
pp. 544-552
Author(s):  
Nikolay Dukov ◽  
Kristina Bliznakova ◽  
Tsvetelina Teneva ◽  
Stoyko Marinov ◽  
Predrag Bakic ◽  
...  
Keyword(s):  
Experimental Evaluation ◽  
Imaging Techniques ◽  
X Ray ◽  
X Ray Imaging ◽  
Breast Phantoms ◽  
2D And 3D

Low-dose phase-based X-ray imaging techniques for in situ soft tissue engineering assessments

Biomaterials ◽  
2016 ◽  
Vol 82 ◽  
pp. 151-167 ◽  
Author(s):  
Zohreh Izadifar ◽  
Ali Honaramooz ◽  
Sheldon Wiebe ◽  
George Belev ◽  
Xiongbiao Chen ◽  
...  
Keyword(s):  
Tissue Engineering ◽  
Soft Tissue ◽  
Low Dose ◽  
Imaging Techniques ◽  
X Ray ◽  
X Ray Imaging ◽  
Soft Tissue Engineering

An x-ray microprobe based upon a close-coupled focal-spot / glass capillary arrangement

1992 ◽  
Vol 50 (2) ◽  
pp. 1758-1759
Author(s):  
D. A. Carpenter ◽  
M. A. Taylor
Keyword(s):  
Imaging Techniques ◽  
Fluorescence Analysis ◽  
High Sensitivity ◽  
Specimen Preparation ◽  
X Rays ◽  
Glass Capillary ◽  
Close Coupling ◽  
X Ray ◽  
Point To Point ◽  
Beam Damage

The development of intense sources of x rays has led to renewed interest in the use of microbeams of x rays in x-ray fluorescence analysis. Sparks pointed out that the use of x rays as a probe offered the advantages of high sensitivity, low detection limits, low beam damage, and large penetration depths with minimal specimen preparation or perturbation. In addition, the option of air operation provided special advantages for examination of hydrated systems or for nondestructive microanalysis of large specimens.The disadvantages of synchrotron sources prompted the development of laboratory-based instrumentation with various schemes to maximize the beam flux while maintaining small point-to-point resolution. Nichols and Ryon developed a microprobe using a rotating anode source and a modified microdiffractometer. Cross and Wherry showed that by close-coupling the x-ray source, specimen, and detector, good intensities could be obtained for beam sizes between 30 and 100μm. More importantly, both groups combined specimen scanning with modern imaging techniques for rapid element mapping.

Quantitative nano-characterization of heterogeneous catalysts

1995 ◽  
Vol 53 ◽  
pp. 398-399
Author(s):  
P.A. Crozier ◽  
M. Pan
Keyword(s):  
Heterogeneous Catalysts ◽  
Low Dose ◽  
Imaging Techniques ◽  
Structural Features ◽  
Catalyst Characterization ◽  
New Developments ◽  
Double Phase ◽  
Phase Systems ◽  
Dose Imaging

Heterogeneous catalysts can be of varying complexity ranging from single or double phase systems to complicated mixtures of metals and oxides with additives to help promote chemical reactions, extend the life of the catalysts, prevent poisoning etc. Although catalysis occurs on the surface of most systems, detailed descriptions of the microstructure and chemistry of catalysts can be helpful for developing an understanding of the mechanism by which a catalyst facilitates a reaction. Recent years have seen continued development and improvement of various TEM, STEM and AEM techniques for yielding information on the structure and chemistry of catalysts on the nanometer scale. Here we review some quantitative approaches to catalyst characterization that have resulted from new developments in instrumentation.HREM has been used to examine structural features of catalysts often by employing profile imaging techniques to study atomic details on the surface. Digital recording techniques employing slow-scan CCD cameras have facilitated the use of low-dose imaging in zeolite structure analysis and electron crystallography. Fig. la shows a low-dose image from SSZ-33 zeolite revealing the presence of a stacking fault.

scholarly journals X-Ray Imaging Techniques Appraisal: Pathway to Sustainable Health Status

2021 ◽  
Vol 655 (1) ◽  
pp. 012073
Author(s):  
J. A. Achuka ◽  
M. R. Usikalu ◽  
M. A. Aweda ◽  
O. A. Olowoyeye ◽  
C. A. Enemuwe ◽  
...  
Keyword(s):  
Health Status ◽  
Imaging Techniques ◽  
X Ray ◽  
X Ray Imaging ◽  
Sustainable Health

Dental cone-beam CT reconstruction from limited-angle view data based on compressed-sensing (CS) theory for fast, low-dose X-ray imaging

2014 ◽  
Vol 64 (12) ◽  
pp. 1907-1911
Author(s):  
Uikyu Je ◽  
Hyosung Cho ◽  
Minsik Lee ◽  
Jieun Oh ◽  
Yeonok Park ◽  
...  
Keyword(s):  
Compressed Sensing ◽  
Low Dose ◽  
Cone Beam Ct ◽  
Cone Beam ◽  
Ct Reconstruction ◽  
X Ray ◽  
X Ray Imaging ◽  
Limited Angle

scholarly journals High-sensitivity high-resolution X-ray imaging with soft-sintered metal halide perovskites

2021 ◽  
Vol 4 (9) ◽  
pp. 681-688
Author(s):  
Sarah Deumel ◽  
Albert van Breemen ◽  
Gerwin Gelinck ◽  
Bart Peeters ◽  
Joris Maas ◽  
...  
Keyword(s):  
High Sensitivity ◽  
Metal Halide ◽  
Detector Arrays ◽  
X Ray ◽  
Carrier Lifetimes ◽  
Sintered Metal ◽  
X Ray Imaging ◽  
Imaging Detector ◽  
High Carrier ◽  
Halide Perovskites

AbstractTo realize the potential of artificial intelligence in medical imaging, improvements in imaging capabilities are required, as well as advances in computing power and algorithms. Hybrid inorganic–organic metal halide perovskites, such as methylammonium lead triiodide (MAPbI3), offer strong X-ray absorption, high carrier mobilities (µ) and long carrier lifetimes (τ), and they are promising materials for use in X-ray imaging. However, their incorporation into pixelated sensing arrays remains challenging. Here we show that X-ray flat-panel detector arrays based on microcrystalline MAPbI3 can be created using a two-step manufacturing process. Our approach is based on the mechanical soft sintering of a freestanding absorber layer and the subsequent integration of this layer on a pixelated backplane. Freestanding microcrystalline MAPbI3 wafers exhibit a sensitivity of 9,300 µC Gyair–1 cm–2 with a μτ product of 4 × 10–4 cm2 V–1, and the resulting X-ray imaging detector, which has 508 pixels per inch, combines a high spatial resolution of 6 line pairs per millimetre with a low detection limit of 0.22 nGyair per frame.

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