Crystal structure and Hirshfeld surface analysis of 3-octyl-4-oxo-2,6-bis(3,4,5-trimethoxyphenyl)piperidinium chloride
2018 ◽
Vol 74
(7)
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pp. 931-934
Keyword(s):
One Pot
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The title compound, C31H46NO7 +·Cl−, was synthesized by a one-pot Mannich condensation reaction. In the molecule, the piperidinone ring adopts a chair conformation, and the trimethoxy-substituted benzene rings and octyl chain are arranged equatorially. In the crystal, centrosymmetric dimers are linked into layers parallel to (011) by N—H...Cl and C—H...Cl hydrogen bonds. A Hirshfeld surface analysis indicates that the most important contributions for the crystal packing are O...H (20.5%) interactions followed by C...H (7.8%), Cl...H (5.5%), C...C (1.2%), C...O (0.5%) and Cl...O (0.4%) interactions.
2022 ◽
Vol 78
(1)
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2021 ◽
Vol 77
(5)
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pp. 512-515
2020 ◽
Vol 76
(7)
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pp. 1007-1011
2020 ◽
Vol 76
(10)
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pp. 1557-1561
Keyword(s):
2017 ◽
Vol 73
(5)
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pp. 763-766
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2020 ◽
Vol 76
(5)
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pp. 605-610
2020 ◽
Vol 76
(7)
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pp. 1146-1149
2019 ◽
Vol 75
(12)
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pp. 1934-1939
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2017 ◽
Vol 73
(4)
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pp. 524-527
2019 ◽
Vol 75
(2)
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pp. 237-241
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Keyword(s):