scholarly journals Advanced miniature mixed mode bending setup for in-situ interface delamination characterization

Author(s):  
M. Kolluri ◽  
M. H. L. Thissen ◽  
J. P. M. Hoefnagels ◽  
J. A. W. van Dommelen ◽  
M. G. D. Geers
2009 ◽  
Vol 158 (2) ◽  
pp. 183-195 ◽  
Author(s):  
M. Kolluri ◽  
M. H. L. Thissen ◽  
J. P. M. Hoefnagels ◽  
J. A. W. Dommelen ◽  
M. G. D. Geers

Author(s):  
Chenglin Wu ◽  
Congjie Wei ◽  
Yanxiao Li

In-situ nanoindentation experiment has been widely adopted to characterize material behaviors of microelectronic devices. This work introduces the latest developments of nanoindentation experiment in characterizing nonlinear material properties of 3D integrated microelectronic devices with through-silicon-vias (TSVs). The elastic, plastic, and interfacial fracture behavior of the copper via and matrix-via interface have been characterized using small scale specimens prepared with focused-ion-beam (FIB) and nanoindentation experiment. A brittle interfacial fracture was found at the Cu/Si interface under mixed-mode loading with a phase angle ranging from 16.7 to 83.7 degrees. The mixed-mode fracture strengths were extracted using the linear elastic fracture mechanics (LEFM) analysis and a fracture criterion was obtained by fitting the extracted data with the power-law function. The vectorial interfacial strength and toughness were found to be independent with mode-mix.


Science ◽  
2020 ◽  
Vol 369 (6504) ◽  
pp. 689-694
Author(s):  
Gianluca Roscioli ◽  
Seyedeh Mohadeseh Taheri-Mousavi ◽  
Cemal Cem Tasan

Steels for sharp edges or tools typically have martensitic microstructures, high carbide contents, and various coatings to exhibit high hardness and wear resistance. Yet they become practically unusable upon cutting much softer materials such as human hair, cheese, or potatoes. Despite this being an everyday observation, the underlying physical micromechanisms are poorly understood because of the structural complexity of the interacting materials and the complex boundary conditions of their co-deformation. To unravel this complexity, we carried out interrupted tests and in situ electron microscopy cutting experiments with two micromechanical testing setups. We investigated the findings analytically and numerically, revealing that the spatial variation of lath martensite structure plays the key role leading to a mixed-mode II-III cracking phenomenon before appreciable wear.


Author(s):  
Saeid Ghouli ◽  
Majid R. Ayatollahi ◽  
Bahador Bahrami ◽  
Jamaloddin Jamali

2000 ◽  
Vol 634 ◽  
Author(s):  
Donald E. Kramer ◽  
Tim Foecke

ABSTRACTNanolaminate materials exhibit increases in hardness and yield strength beyond those expected according to rule of mixtures calculations. Several models have been proposed to explain this enhancement of strength, but conclusive experimental verification is hindered by the complex interaction between ingrown defects, in-plane microstructure and compositional modulation. In this study, mechanisms of plastic deformation in nanolaminates are investigated by in situ TEM straining of epitaxial Cu/Ni nanolaminates grown on Cu (001) single crystal substrates. Two distinct types of deformation are observed. Initial plastic deformation is accommodated by motion of “Orowan” and threading dislocations in a uniform and random fashion. As the stress levels increase, fracture occurs creating a mixed mode crack. Subsequent observations suggest that intense plastic deformation occurs over many bilayers in the direction of crack growth, but is contained to within one or two bilayers in a direction normal to the crack faces.


1991 ◽  
Vol 6 (2) ◽  
pp. 314-323 ◽  
Author(s):  
H. Zhang ◽  
A.H. King ◽  
R. Thomson

The elastic interactions of dislocations and intergranular cracks in isotropic materials have been studied. In the first part of the paper, a model based on the Rice–Thomson theory is established under which the conditions for dislocation emission and crack propagation can be described in terms of an emission surface, cleavage surface, and loading line in the local k-space associated with a mixed mode intergranular crack. For a given crack, the local k-field changes with the emission of dislocations from the crack tip, which alters the balance of cleavage and emission. In the second part, we present experimental results of in situ TEM observations of intergranular cracks in molybdenum. Alternating brittle crack propagation and dislocation emission is observed. The number of emitted dislocations corresponding to each crack propagation is in good agreement with the calculated values.


2013 ◽  
Vol 185 (1-2) ◽  
pp. 77-95 ◽  
Author(s):  
M. Kolluri ◽  
J. P. M. Hoefnagels ◽  
J. A. W. Dommelen ◽  
M. G. D. Geers

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