X-ray powder diffraction data for high-temperature Al4Re(Ni)

2009 ◽  
Vol 24 (1) ◽  
pp. 29-31 ◽  
Author(s):  
B. Grushko

A monoclinic phase isostructural to Al4W was revealed in Al–Ni–Re close to the Al–Re terminal. It is assumed to be a ternary extension of the high-temperature Al4Re phase usually transforming in binary alloys even by sharp quenching from the existence temperatures. The powder X-ray diffraction pattern of this phase of the Al77Ni2.5Re20.5 composition was indexed for the Cm space group with a=5.1538(12) Å, b=17.410(5) Å, c=5.1546(15) Å, and β=100.548(16)°.

1996 ◽  
Vol 11 (1) ◽  
pp. 26-27 ◽  
Author(s):  
Irena Georgieva ◽  
Ivan Ivanov ◽  
Ognyan Petrov

A new compound—Ba3MnSi2O8 in the system BaO–MnO–SiO2 was synthesized and studied by powder X-ray diffraction. The compound is hexagonal, space group—P6/mmm, a=5.67077 Å, c=7.30529 Å, Z=1, Dx=5.353. The obtained powder X-ray diffractometry (XRD) data were interpreted by the Powder Data Interpretation Package.


2015 ◽  
Vol 30 (3) ◽  
pp. 293-293 ◽  
Author(s):  
Qing Wang ◽  
Ying Xiao ◽  
Jia Wei He ◽  
Hui Li

X-ray powder diffraction data for 3,3-dichloro-1-(4-nitrophenyl)-2-piperidinone, C11H10Cl2N2O3, are reported [a = 11.088(4) Å, b = 11.594(5) Å, c = 12.689(3) Å, α = 118.456(1)°, β = 100.320(3)°, γ = 107.763(3)°, V = 1259.27 Å3, Z = 4 and space group P-1 ]. All measured lines were indexed and are consistent with the P-1 space group. No detectable impurities were observed.


2008 ◽  
Vol 23 (4) ◽  
pp. 356-359 ◽  
Author(s):  
B. Grushko ◽  
D. Pavlyuchkov

Ternary Al–Cu–Ir phases, isostructural to the Al–Cu–Rh ω and C2 phases, were found to be around the Al70Cu20Ir10 and Al60Cu15Ir25 compositions, respectively. Using powder X-ray diffraction, the former was found to have a tetragonal structure (space group P4/mnc) with a=6.4142(9) Å and c=14.842(4) Å, and the latter has a cubic structure (space group Fm3) with a=15.3928(6) Å.


1993 ◽  
Vol 8 (4) ◽  
pp. 249-250 ◽  
Author(s):  
Chan Park ◽  
Robert L. Snyder

The X-ray powder diffraction pattern for a sample of the high-temperature superconducting phase Tl0.5Pb0.5Sr2CaCu2O6.5+δ has been determined. The sample was prepared by a molten salt technique and had a Tc of 96 K.


1997 ◽  
Vol 12 (3) ◽  
pp. 134-135
Author(s):  
Liangqin Nong ◽  
Lingmin Zeng ◽  
Jianmin Hao

The compound DyNiSn has been studied by X-ray powder diffraction. The X-ray diffraction patterns for this compound at room temperature are reported. DyNiSn is orthorhombic with lattice parameters a=7.1018(1) Å, b=7.6599(2) Å, c=4.4461(2) Å, space group Pna21 and 4 formula units of DyNiSn in unit cell. The Smith and Snyder Figure-of-Merit F30 for this powder pattern is 26.7(0.0178,63).


Author(s):  
Michel Fleck ◽  
Ekkehart Tillmanns ◽  
Ladislav Bohatý ◽  
Peter Held

AbstractThe crystal structures of eight different L-malates have been determined and refined from single-crystal X-ray diffraction data. The compounds are the monoclinic (space groupIn addition, for all the compounds, powder diffraction data were collected, analysed and submitted to the powder diffraction file (PDF).


1999 ◽  
Vol 14 (3) ◽  
pp. 231-233 ◽  
Author(s):  
Raj P. Singh ◽  
Michael J. Miller ◽  
Jeffrey N. Dann

(Na0.6H0.4)(Ta0.7Nb0.3)O3 was synthesized by heating a tantalum/niobium scale containing two sodium tantalate/niobate phases :Na14(Ta0.7Nb0.3)12O37·31H2O and NaH2Ta0.7Nb0.3O4. Powder X-ray diffraction data for (Na0.6H0.4)(Ta0.7Nb0.3)O3 indicated it to be a cubic perovskite (ABO3/ReO3 type structure) with unit cell a0=3.894 Å. The compound is analogous to the mineral lueshite (NaNbO3), and to the high temperature forms of NaTaO3 and NaNbO3. Powder diffraction data for (Na0.6H0.4)(Ta0.7Nb0.3)O3 will be useful in the analysis of synthetic tantalum/niobium concentrates.


1994 ◽  
Vol 9 (3) ◽  
pp. 187-188 ◽  
Author(s):  
Hee-Lack Choi ◽  
Naoya Enomoto ◽  
Nobuo Ishizawa ◽  
Zenbe-e Nakagawa

X-ray powder diffraction data for Ti2O2(C2O4)(OH)2·H2O were obtained. The crystal system was determined to be orthorhombic with space group C2221. The unit cell parameters were refined to a = 1.0503(2) nm, b = 1.5509(3) nm, and c = 0.9700(1) nm.


2006 ◽  
Vol 21 (4) ◽  
pp. 318-319
Author(s):  
Mark A. Rodriguez ◽  
David P. Adams

X-ray powder diffraction data for a rhombohedral AlPt phase formed by self-propagating, high-temperature reactions of Al∕Pt bi-layer films are reported. Multilayer Al∕Pt thin film samples, reacted in air or vacuum, transformed into rhombohedral AlPt with space group R-3(148). Indexing and lattice parameter refinement of AlPt powders (generated from thin-film samples) yielded trigonal/hexagonal unit-cell lattice parameters of a=15.623(6) Å and c=5.305(2) Å, Z=39, and V=1121.5 Å3.


2010 ◽  
Vol 25 (1) ◽  
pp. 72-74 ◽  
Author(s):  
H. A. Camargo ◽  
J. A. Henao ◽  
D. F. Amado ◽  
V. V. Kouznetsov

1-N-(4-pyridylmethyl)amino naphtalene was synthesized by means of a reaction of alpha-naphthylamine, 4-pyridylcarboxyaldehyde, in anhydrous ethanol to obtainN-(4-pyridylen)-alpha-naphthylamine and that was reduced with NaBH4 to produce the wanted compound. The X-ray powder diffraction pattern for the new compound 1-N-(4-pyrydylmethyl)amino naphtalene was obtained. This compound crystallizes in a monoclinic system with refined unit cell parameters a=10.375(5) Å, b=17.665(6) Å, c=5.566(2) Å, β=100.11(3), and V=1004.3(5) Å3, with space group P2/m (No. 10).


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