Fracture Surface Characterization of Dentin-bonded Interfacial Fracture Toughness Specimens

1994 ◽  
Vol 73 (3) ◽  
pp. 607-619 ◽  
Author(s):  
L.E. Tam ◽  
R.M. Pilliar
2019 ◽  
Author(s):  
Denizhan Yavas ◽  
Ashraf Bastawros ◽  
Bishoy Dawood ◽  
Christopher Giuffre

1989 ◽  
Vol 153 ◽  
Author(s):  
Mark J. Filiaggi ◽  
N. A. Coombs ◽  
R.M. Pilliar

AbstractPlasma sprayed Hydroxyapatite (HA) coatings are applied to metal prostheses to allow for implant fixation through chemical bonding of the coating with surrounding bone tissue. Without a well-adhering coating, this fixation is threatened. Thus, a thorough characterization of the metal / ceramic interface is necessary. This study used a novel composite short bar interfacial fracture toughness technique with high resolution electron spectroscopic imaging to examine Ti-6AI-4V plasma spray coated with 100μm of HA. For this system, an interfacial fracture toughness value of 1.31 +/− 0.08 MPa·m1/2 was obtained, with a corresponding tensile adhesive bond strength of 6.7 +/− 1.5 MPa. High resolution ESI revealed distinct phosphorous segregation to the interface and diffusion into the underlying titanium. A 24-hour post-heat treatment at 960°C greatly increased the bond strength at this interface. Observations from ESI suggested that this effect may be due to enhanced diffusion of both phosphorous and calcium into the metal substrate.


2007 ◽  
Vol 73 (735) ◽  
pp. 1266-1272 ◽  
Author(s):  
Yoshiaki NOMURA ◽  
Masaki NAGAI ◽  
Toru IKEDA ◽  
Noriyuki MIYAZAKI

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