Characterization of EMC/LF interfacial fracture toughness using the advanced mixed-mode bending method

Author(s):  
M. Schulz ◽  
H. S. Nabi ◽  
D.-K. Vu ◽  
B. Wunderle ◽  
J. Keller
2019 ◽  
pp. 089270571987486 ◽  
Author(s):  
Abdul Samad Khan ◽  
Aaqib Ali ◽  
Ghulam Hussain ◽  
Muhammad Ilyas

Multimaterial structures made using fused deposition modeling (FDM) offer an attractive prospect for enhancing their mechanical properties and functionality. In this study, the interfacial fracture toughness of a unidirectional hybrid composite fabricated by FDM was studied through mechanical testing. The composite structure comprises acrylonitrile butadiene styrene and carbon fiber-reinforced polylactic acid. Since, de-adhesion or bond failure at the interface can occur under a combination of the different fracture modes, therefore, interfacial fracture toughness, in terms of the critical energy release rate, was characterized using double cantilever beam specimen test for mode I, end-notched flexural specimen test for mode II, and mixed-mode bending specimen test for mixed-mode I/II. Effects of varying process parameters, like printing speed and nozzle temperature, on the interfacial fracture toughness in mode I and II were also investigated. It was found that increasing the nozzle temperature and printing speed enhance the fracture toughness, both in mode I and II, but the effect of increasing nozzle temperature on mode II fracture toughness was quite significant.


Author(s):  
David Manan ◽  
Jeongho Kim ◽  
Renata Marques de Melo ◽  
Yu Zhang

Abstract Dental interfaces are subject to mixed-mode loading. This study provides a practical guidance for determining interfacial fracture toughness of dental ceramic systems. We address interfacial fracture of a composite resin cement sandwiched between two dental ceramic materials. Emphasis is placed on sandwich disc specimens with cracks originating from elliptical-shaped flaws near the center, for which analytical fracture mechanics methods fail to predict. The interaction integral method is used to provide accurate finite element solutions for cracks with elliptical-shaped flaws in a Brazil-nut-sandwich specimen. The developed model was first validated with existing experimental data, and then used to evaluate three most widely used dental ceramic systems: polycrystalline ceramics (zirconia), glass-ceramics (lithium disilicate), and feldspathic ceramics (porcelain). Contrary to disc specimens with ideal cracks, those with cracks emanating from elliptical-shaped flaws do not exhibit a monotonic increase in interfacial toughness. Also, interfacial fracture toughness is seen to have a direct relationship with the aspect ratio of elliptical-shaped flaws and an inverse relationship with the modulus ratio of the constituents. The presence of an elliptical-shaped flaw significantly changes the interfacial fracture behavior of sandwich structures. Semi-empirical design equations are provided for fracture toughness and stress intensity factors for interfacial cracks. The developed design equations provide a practical guidance for determining interfacial fracture toughness of selected dental ceramic material systems. Those equations take into account four critical factors: size of the elliptical flaw, modulus ratio of constituent materials, loading angle and applied load.


2019 ◽  
Author(s):  
Denizhan Yavas ◽  
Ashraf Bastawros ◽  
Bishoy Dawood ◽  
Christopher Giuffre

1989 ◽  
Vol 153 ◽  
Author(s):  
Mark J. Filiaggi ◽  
N. A. Coombs ◽  
R.M. Pilliar

AbstractPlasma sprayed Hydroxyapatite (HA) coatings are applied to metal prostheses to allow for implant fixation through chemical bonding of the coating with surrounding bone tissue. Without a well-adhering coating, this fixation is threatened. Thus, a thorough characterization of the metal / ceramic interface is necessary. This study used a novel composite short bar interfacial fracture toughness technique with high resolution electron spectroscopic imaging to examine Ti-6AI-4V plasma spray coated with 100μm of HA. For this system, an interfacial fracture toughness value of 1.31 +/− 0.08 MPa·m1/2 was obtained, with a corresponding tensile adhesive bond strength of 6.7 +/− 1.5 MPa. High resolution ESI revealed distinct phosphorous segregation to the interface and diffusion into the underlying titanium. A 24-hour post-heat treatment at 960°C greatly increased the bond strength at this interface. Observations from ESI suggested that this effect may be due to enhanced diffusion of both phosphorous and calcium into the metal substrate.


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