Fabrication of Pt- and Au-coated W Nano Tip with Electroplated Films as a Noble-metal Source toward Viable Application for Long-life Electron Source

An electron source featuring high brightness and long life has been developed for high-resolution video recording. The electron source is of triode type, and incorporates a directly heated and replaceable lanthanum hexaboride (LaB6) emitter.Since the initial work of Lafferty (1) in 1951, LaB6 has been known as a potential long-life emitter material capable of high emission densities. However, a number of drawbacks have prevented widespread application as a cathode material. These include the high reactivity of LaB6 at elevated temperatures with almost all substrate materials, its sensitivity to corrosion by oxygen-containing gases (2), and fabrication problems due to Its brittleness. Successful operation at high emission densities, therefore, has been reported only by Kapitza, et al (3), and by Broers (4). Kapitza soldered an LaB6 cube to a tantalum heater using MoSi2 in vacuo at 2000°C. This system required a heating current of 50 A. Broers brazed an LaB6 rod to a copper heatsink and indirectly heated the tip of the rod by means of a tungsten coil requiring a power input of 60 W.

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A Shelved Structure for the Support of An Electron Optical Column

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100068825 ◽

1970 ◽

Vol 28 ◽

pp. 366-367

Author(s):

P.H. McLaughlin

Keyword(s):

Electron Source ◽

Floating Platform ◽

Supporting Structure

A shelved structure for the support of an electron optical column affords advantages both to the designer and the user. A lens may be removed for cleaning for example, without demounting the remaining lenses. A custom device for another example, may be placed on a shelf, substituting for the standard lens perhaps so that some specialized research may be undertaken. Especially advantageous is a shelved arrangement if the column assembly is designed to hang from a supporting structure such as a gas borne floating platform, as is the case with the system described below.As shown on the schematic, a floating platform (I) supports the electron source apparatus (2) and a U-shaped column support shelf (3). The column support shelf acts as a key for locating and supporting three struts (4) which with nuts (5) support the condenser shelf (6), the objective shelf (7), the upper projector shelf (8), and the lower projector shelf (9).

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Optical Properties of HVEM Accelerators

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100114529 ◽

1975 ◽

Vol 33 ◽

pp. 180-181

Author(s):

A. Strojnik ◽

J.W. Scholl ◽

V. Bevc

Keyword(s):

Optical Properties ◽

Electron Accelerator ◽

Systematic Investigation ◽

Electron Source ◽

High Brightness ◽

The Past ◽

Wide Range ◽

Optical Behavior

The electron accelerator, as inserted between the electron source (injector) and the imaging column of the HVEM, is usually a strong lens and should be optimized in order to ensure high brightness over a wide range of accelerating voltages and illuminating conditions. This is especially true in the case of the STEM where the brightness directly determines the highest resolution attainable. In the past, the optical behavior of accelerators was usually determined for a particular configuration. During the development of the accelerator for the Arizona 1 MEV STEM, systematic investigation was made of the major optical properties for a variety of electrode configurations, number of stages N, accelerating voltages, 1 and 10 MEV, and a range of injection voltages ϕ0 = 1, 3, 10, 30, 100, 300 kV).

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A comparative study on the cold type and thermal type field emission guns used in the same electron microscope

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100107435 ◽

1978 ◽

Vol 36 (1) ◽

pp. 58-59

Author(s):

M. Iwatsuki ◽

Y. Kokubo ◽

Y. Harada

Keyword(s):

Electron Microscope ◽

Field Emission ◽

Signal To Noise Ratio ◽

Electron Source ◽

Resolving Power ◽

Optical Source ◽

Experimental Conditions ◽

High Brightness ◽

Illumination System ◽

Transmission Electron

On accout of its high brightness, small optical source size, and minimal energy spread, the field emission gun (FEG) has the advantage that it provides the conventional transmission electron microscope (TEM) with a highly coherent illumination system and directly improves the resolving power and signal-to-noise ratio of the scanning electron microscope (SEM). The FEG is generally classified into two types; the cold field emission (C-FEG) and thermal field emission gun (T-FEG). The former, in which a field emitter is used at the room temperature, was successfully developed as an electron source for the SEM. The latter, in which the emitter is heated to the temperature range of 1000-1800°K, was also proved to be very suited as an electron source for the TEM, as well as for the SEM. Some characteristics of the two types of the FEG have been studied and reported by many authors. However, the results of the respective types have been obtained separately under different experimental conditions.

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Analytical Electron Microscopy study of two vehicle-aged automotive exhaust catalysts having dissimilar activities

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100153336 ◽

1989 ◽

Vol 47 ◽

pp. 272-273

Author(s):

Sooho Kim ◽

M. J. D’Aniello

Keyword(s):

Electron Microscopy ◽

Particle Size ◽

Noble Metal ◽

Catalyst Deactivation ◽

Analytical Electron Microscopy ◽

Microscopy Study ◽

Metal Particles ◽

Automotive Exhaust ◽

Exhaust Catalysts ◽

Analytical Electron

Automotive catalysts generally lose-agtivity during vehicle operation due to several well-known deactivation mechanisms. To gain a more fundamental understanding of catalyst deactivation, the microscopic details of fresh and vehicle-aged commercial pelleted automotive exhaust catalysts containing Pt, Pd and Rh were studied by employing Analytical Electron Microscopy (AEM). Two different vehicle-aged samples containing similar poison levels but having different catalytic activities (denoted better and poorer) were selected for this study.The general microstructure of the supports and the noble metal particles of the two catalysts looks similar; the noble metal particles were generally found to be spherical and often faceted. However, the average noble metal particle size on the poorer catalyst (21 nm) was larger than that on the better catalyst (16 nm). These sizes represent a significant increase over that found on the fresh catalyst (8 nm). The activity of these catalysts decreases as the observed particle size increases.

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Interlayer confinement synthesis of Ir nanodots/dual carbon as an electrocatalyst for overall water splitting

Journal of Materials Chemistry A ◽

10.1039/d0ta09358k ◽

2020 ◽

Author(s):

Yaru Li ◽

Yu-Quan Zhu ◽

Weili Xin ◽

Song Hong ◽

Xiaoying Zhao ◽

...

Keyword(s):

Water Splitting ◽

Noble Metal ◽

High Efficiency ◽

Overall Water Splitting ◽

Highly Dispersed

Rationally designing low-content and high-efficiency noble metal nanodots offers opportunities to enhance electrocatalytic performances for water splitting. However, the preparation of highly dispersed nanodots electrocatalysts remains a challenge. Herein, we...

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