Application of Statistical Solvent Mixture Design in Optimizing the Solid-Liquid Extraction of Phenolic Compounds from Mango Seed Kernels

2021 ◽  
Vol 14 (2) ◽  
Author(s):  
Alden A. Cabajar ◽  
Francis Dave C. Siacor ◽  
Kramer Joseph A. Lim ◽  
Camila Flor Y. Lobarbio ◽  
Evelyn B. Taboada
Keyword(s):  
Phenolic Compounds ◽  
Extraction Process ◽  
Solvent Mixture ◽  
Liquid Extraction ◽  
Mixture Design ◽  
Positive Effects ◽  
Lattice Design ◽  
Solid Liquid Extraction ◽  
Mango Seed ◽  
Solid Liquid

Mango seed kernel (MSK) is a waste material of the mango processing industry and is reported to significantly contain phenolic compounds with anti-oxidative properties. In this work, these compounds are isolated via solid-liquid extraction (SLE) in which solvent mixture design approach was used to evaluate the optimal quaternary solvent ratio in relation to the phenolics content of extracts from MSK. The quaternary solvent is composed of ethanol (E), methanol (M), acetone (A), and water (W). The extraction process was implemented at 40°C for 60 minutes with the ratio between solid and solvent at 1:25. Response surface methodology coupled with simplex lattice design was developed to evaluate the optimal solvent system and their interaction effects on the phenolic compounds content. The linear, two-way, and three-way interaction, except for methanol-acetonewater system, resulted in positive effects on the phenolic compounds content. The response model shows that a quaternary mixture with approximately 3:3:3:1 E:M:A:W ratio provided the highest phenolic content. A Scheffé cubic model sufficiently described the extraction process. The results of this study showed that the extraction of phenolic compounds in MSK via SLE using a mixture of solvents is possible. Higher extraction efficiencies can be achieved by optimizing the SLE process, and the optimum conditions can be applied to produce phenolic extracts with positive antioxidant activity.

scholarly journals Comparison between Two Solid-Liquid Extraction Methods for the Recovery of Steviol Glycosides from Dried Stevia Leaves Applying a Numerical Approach

Processes ◽  
2018 ◽  
Vol 6 (8) ◽  
pp. 105 ◽  
Author(s):  
Monica Gallo ◽  
Andrea Formato ◽  
Gaetano Formato ◽  
Daniele Naviglio
Keyword(s):  
Stevia Rebaudiana ◽  
Value Added ◽  
Numerical Approach ◽  
Extraction Process ◽  
Extraction Methods ◽  
Liquid Extraction ◽  
Steviol Glycosides ◽  
Stevia Rebaudiana Bertoni ◽  
Solid Liquid Extraction ◽  
Solid Liquid

Abstract: Stevia rebaudiana Bertoni is a perennial shrub belonging to the Asteraceae family. The leaves contain a mixture of steviol glycosides with extraordinary sweetening properties, among which the most important are stevioside and rebaudioside A. These components have a high sweetening power, which is about 300 times that of sucrose, and a negligible calorie content. However, their extraction and purification are not easy. In this paper, the extraction technique under cyclic pressure, known as rapid solid-liquid dynamic extraction (RSLDE), was compared using a Naviglio extractor (NE) with conventional maceration. The aim was to identify an efficient and economically viable method for obtaining high amounts of steviol glycosides in a short time. Furthermore, a numerical model was set up for the solid-liquid extraction process of value-added compounds from natural sources. Several parameters must be evaluated in relation to the characteristics of the parts of the plant subjected to extraction. Therefore, since diffusion and osmosis are highly dependent on temperature, it is necessary to control the temperature of the extraction system. On the other hand, the final aim of this work was to provide a scientific and quantitative basis for RSLDE. Therefore, the results obtained from stevia extracts using the corresponding mathematical model allowed hypothesizing the application of this model to the extraction processes of other vegetable matrices.

Application of response surface methodology for optimization of ultrasound‐assisted solid‐liquid extraction of phenolic compounds from Cenostigma macrophyllum

2020 ◽  
Vol 34 (10) ◽  
Author(s):  
Bruno Oliveira Moreira ◽  
Marco Roberto Dourado Barbosa Filho ◽  
Anaildes Lago Carvalho ◽  
Douglas Gonçalves Silva ◽  
Mariluze Peixoto Cruz ◽  
...  
Keyword(s):  
Response Surface Methodology ◽  
Phenolic Compounds ◽  
Response Surface ◽  
Liquid Extraction ◽  
Ultrasound Assisted ◽  
Solid Liquid Extraction ◽  
Solid Liquid

scholarly journals EKSTRAKSI SILIKA DARI ABU SEKAM PADI DENGAN PELARUT KOH

Konversi ◽  
2013 ◽  
Vol 2 (1) ◽  
pp. 28
Author(s):  
Galang Fajar Agung M ◽  
Muhammad Rizal Hanafie Sy ◽  
Primata Mardina
Keyword(s):  
Raw Materials ◽  
Operation Time ◽  
Extraction Process ◽  
Liquid Extraction ◽  
Waste Material ◽  
Alkali Solution ◽  
Rice Husks ◽  
Solid Liquid Extraction ◽  
The One ◽  
Solid Liquid

Sekam padi sebagai limbah yang berlimpah khususnya di negara agraris, adalah salah satu sumber penghasil silika terbesar. Sekam padi mengandung sekitar 90%-98% silika setelah mengalami pembakaran sempurna. Pengambilan silika dari abu sekam padi dilakukan dengan proses ekstraksi padat cair menggunakan larutan alkali sebagai pelarut. Tujuan dari penelitian ini adalah untuk mengetahui pengaruh konsentrasi larutan alkali dan waktu operasi terhadap yield dari silika. Proses ekstraksi dilakukan dalam skala laboratorium. Sepuluh gram abu sekam padi dimasukkan ke dalam 60 mL larutan alkali dengan konsentrasi tertentu (5%w/w, 10% w/w dan 15% w/w) untuk diekstrak kandungan silika dengan waktu operasi tertentu (30, 60 dan 90 menit). Setelah proses ekstraksi selesai, larutan tersebut ditambahkan larutan HCl 1 N untuk mengendapkan silika. Silika yang terbentuk kemudian dipisahkan dari sisa larutan dengan penyaringan. Untuk menghilangkan kelembaban pada silika yang dihasilkan, maka dilanjutkan dengan proses pengeringan. Hasil penelitian menunjukkan yield silika terbesar adalah 50,49% terjadi pada KOH 10% dan waktu ekstraksi 90 menit.  Keywords: abu sekam padi, silika, KOH  Rice husks, the most abundant waste material in agricultural country, is the one of the silica rich raw materials. Rice husks contain about 90%-98% of silica after completed combustion. Recovery silica from ash of  rice husks was done by solid-liquid extraction using alkali solution. Different concentration of alkali solution (5% w/w, 10% w/w and 10% w/w) and different operation time (30, 60 and 90 minutes) were used to investigate their influence on yields of silica. The extraction process was carried out in laboratory scale. After extraction, process was continued by acidic solidification, filtration and drying. The result showed the biggest yield of  silica was 50, 49% at 10% KOH for 90 minutes . Keywords: ash of rice husks, silica, KOH

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