Influence of Element Re on Creep Behavior of Single Crystal Nickel-Based Superalloys at Intermediate Temperature

2013 ◽  
Vol 32 (1) ◽  
pp. 7-13
Author(s):  
Sugui Tian ◽  
Xianlin Meng ◽  
Zeng Zeng ◽  
Chao Zhang ◽  
Chen Liu

AbstractBy means of creep curves measurement and microstructure observation, an investigation has been made into the influence of the element Re on creep behaviors of single crystal nickel-base superalloy at intermediate temperature. Results show that, after fully heat treated, microstructure of the alloy consists of the cubic γ′ phase embedded coherent in the γ matrix. Comparing with Re-free superalloy, 4.5% Re alloy displays a better creep resistance and longer creep rupture life in the ranges of the applied stresses and temperatures. After crept for 425 h up to fracture at 760 °C/800 MPa, the γ′ phase in the alloy keeps still the regular cubical configuration, which is attributed to the effect of the element Re decreasing the diffusing rate of other elements during creep. The deformation features of the alloy during creep are that the dislocations move in the γ matrix channels and shear into the γ′ phase, the 〈110〉 super-dislocation shearing into the γ′ phase may be decomposed to form the configuration of (1/3)〈112〉 super-Shockleys partials plus the stacking fault, which may hinder dislocations movement and restrain the cross-slipping of dislocations. This is thought to be the main reason of the alloy having a better creep resistance. In the latter stage of creep, the crack is firstly initiated in the interface of γ′/γ phases and propagated along the interface vertical to the stress axis up to the occurrence of the creep fracture, which is thought to be the fracture mechanism of the alloy during creep.

2015 ◽  
Vol 816 ◽  
pp. 551-556
Author(s):  
Su Gui Tian ◽  
Bao Shuai Wang ◽  
Xin Ding ◽  
De Long Shu ◽  
Jing Wu

Creep behavior of a heat treated single crystal nickel base superalloy containing Re/Ru under the test condition of 1100°C/137MPa high temperatures was investigated. The experimental results showed that the segregation extent of elements in the dendrite and inter-dendrite regions of single crystal superalloy decreases by heat treatment at high temperature. The creep life of the alloy at 1100°C/137MPa was measured to be 321 h displaying a better creep resistance. Wherein, significant amount of fine cubiodal γ′ particles precipitated in the γ matrix channels are considered to be the main reason of the alloy having the better creep resistance. The deformation feature of the alloy during steady state creep is dislocations slipping in the γ matrix and climbing over the rafted γ′ phase. But in the latter stage of creep, the deformation feature of the alloy is dislocations shearing into the rafted γ′ phase. As creep goes on, the main / secondary slipping dislocations in the alloy are alternately activated to result in the initiation and propagation of the cracks along the interface of the rafted γ′/γ phase up to fracture, which is thought to be the fracture mechanism of the alloy during creep.


2007 ◽  
Vol 546-549 ◽  
pp. 1345-1348
Author(s):  
Hong Qiang Du ◽  
Su Gui Tian ◽  
Xing Fu Yu ◽  
Ming Gang Wang ◽  
Fan Lai Meng

By means of pre-compressive stress treated, the cubic γ΄ phase in alloy is transformed into the P-type structure along the direction parallel to the applied stress axis. The influence of the P-type structure on the creep lifetimes of alloy has been investigated by means of the tensile creep testing and microstructure observation. Results show that, compared with the A structure alloy, the P-type γ′ rafted alloy displays a shorter creep lifetimes under the experimental conditions. The microstructure evolution of the P-type structure alloy occurs during tensile creep, in which the p-type γ′ rafted phase is transformed into the N-type structure. The microstructure evolution alloy reduces the creep resistance of the alloy, this is one of the main reasons for reducing the creep resistance of the one.


2005 ◽  
Vol 475-479 ◽  
pp. 673-676
Author(s):  
D.Y. Yang ◽  
Tao Jin ◽  
Na Ru Zhao ◽  
Zhi Wang ◽  
Xiao Feng Sun ◽  
...  

The precipitation behavior during ageing treatment of a single crystal nickel-base superalloy was investigated by SEM and TEM. The results showed that tetragonal needle-like σ phase and blocky -W phase precipitated during low temperature ageing treatment after this testing alloy was completely solution heat treated. σ and -W phases robbed of solid solution strengthening alloying element W、Mo in the matrix and degraded high temperature creep rupture property severely. The creep curve of the crystal tested at 1010 °C and 248 MPa exhibited that the steady state creep rate ε was as high as 9.46 × 10-3/h. The creep-rupture life was only 25 hours. -W phase was not formed by decrease of W content properly. A relatively low level of Co could inhibit σ phase precipitation and improve microstructural stability.


2004 ◽  
Vol 379 (1-2) ◽  
pp. 141-147 ◽  
Author(s):  
Sugui Tian ◽  
Xingfu Yu ◽  
Jinghong Yang ◽  
Nairen Zhao ◽  
Yongbo Xu ◽  
...  

2007 ◽  
Vol 546-549 ◽  
pp. 1225-1228
Author(s):  
Fan Lai Meng ◽  
Su Gui Tian ◽  
Ming Gang Wang ◽  
Xing Fu Yu ◽  
Hong Qiang Du ◽  
...  

By means of tensile and compression creep testing and SEM, TEM observation, an investigation has been made into the microstructure evolution of a single crystal nickel base superalloy during tensile / compression creep. Results show that the cubic γ′ phase in the superalloy is transformed into the N-type meshlike structure along the direction vertical to stress axis during tensile creep. The cubic γ′ phase is transformed into the P-type structure along the direction parallel to stress axis during compression creep. An obvious asymmetry strain of the alloy occurs during tensile and compression creep, the formation of the needle-like γ′ rafts during compression creep is a main reason of the alloy displaying a smaller strain. During compressive creep, the deformation feature of the alloy is the <110> and (1/3) <112> super dislocations shearing into the γ′ rafts. The deformation mechanism of the alloy, in the stage state of tensile creep, is dislocation climb over the γ′ rafts.


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